GB803477A - Process for the preparation of 2-ethyl-2-sec-butyl-1, 3-propanediol dicarbamate - Google Patents
Process for the preparation of 2-ethyl-2-sec-butyl-1, 3-propanediol dicarbamateInfo
- Publication number
- GB803477A GB803477A GB1225/57A GB122557A GB803477A GB 803477 A GB803477 A GB 803477A GB 1225/57 A GB1225/57 A GB 1225/57A GB 122557 A GB122557 A GB 122557A GB 803477 A GB803477 A GB 803477A
- Authority
- GB
- United Kingdom
- Prior art keywords
- ethyl
- sec
- butyl
- preparation
- dicarbamate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C271/00—Derivatives of carbamic acids, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups
- C07C271/06—Esters of carbamic acids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
2 - Ethyl - 2 - sec. - butyl - 1:3 - propanediol dicarbamate is prepared by ester interchange between 2 - ethyl - 2 - sec. - butyl - 1:3 - propanediol and a carbamate of an alcohol, said alcohol containing not more than 4 carbon atoms. In an example alcohol is distilled as an azeotrope with toluene from a mixture of the diol and ethyl urethane in toluene containing a catalytic amount of aluminium isopropylate and the residue is worked up to give the required dicarbamate. Specification 798,848 is referred to.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US803477XA | 1956-01-13 | 1956-01-13 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB803477A true GB803477A (en) | 1958-10-29 |
Family
ID=22156812
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1225/57A Expired GB803477A (en) | 1956-01-13 | 1957-01-11 | Process for the preparation of 2-ethyl-2-sec-butyl-1, 3-propanediol dicarbamate |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB803477A (en) |
-
1957
- 1957-01-11 GB GB1225/57A patent/GB803477A/en not_active Expired
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