GB783666A - Improvements in method of cleaning equipment fouled with latex coagulum - Google Patents
Improvements in method of cleaning equipment fouled with latex coagulumInfo
- Publication number
- GB783666A GB783666A GB33985/55A GB3398555A GB783666A GB 783666 A GB783666 A GB 783666A GB 33985/55 A GB33985/55 A GB 33985/55A GB 3398555 A GB3398555 A GB 3398555A GB 783666 A GB783666 A GB 783666A
- Authority
- GB
- United Kingdom
- Prior art keywords
- rubber
- tower
- solution
- coagulum
- vessel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08C—TREATMENT OR CHEMICAL MODIFICATION OF RUBBERS
- C08C1/00—Treatment of rubber latex
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Cleaning By Liquid Or Steam (AREA)
- Detergent Compositions (AREA)
Abstract
783,666. Cleaning rubber latex equipment: rubber solvents. UNITED STATES RUBBER CO. Nov. 28, 1955 [Feb. 17, 1955], No. 33985/55. Class 70. Equipment used for handling or processing rubber latex and which has become coated with a rubber coagulum, is cleaned by subjecting the coagulum to the action of a rubber solvent containing a small amount of a prooxidant softener for rubber in the presence of available oxygen, at an elevated temperature. In the apparatus shown, rubber latex containing ammonia as a preservative flows from a source 11 down a tower 10 against an upward current of moisture-saturated air or other suitable gas flowing via pipes 12 and 13, said air or gas sweeping the ammonia out of the latex so that deammoniated latex may be stored in a vessel 15. In due course two distinct forms of rubber are deposited in the tower, one of which is of soft buttery consistency and is easily removable and the other of which is of tough, stringy agglomerates that are difficult to remove. At frequent intervals the process is stopped and the buttery deposits in the tower 10 are removed by introducing a dilute aqueous solution of an aqueous alkali through an inlet 18 ; and delivering it by a pump 19 through a pipe 20 and heater 26 to the top of the tower 10. The alkali flows down the tower to loosen and dissolve said buttery deposits, the solution being then recirculated or discharged to waste through the line 21. At less frequent intervals, the more difficult to remove coagulum of rubber is treated with a chemical softener for rubber contained in a rubber solvent, the treatment being made in the presence of available oxygen and preferably at an elevated temperature as well as with mechanical agitation. The softener may be a pre-oxidant or an oxidation catalyst such as one of the mercaptans of which phenylhydrazine is preferred. The amount of softener used is from about 0À5 to about 5 per cent on the weight of the solvent. The solvents employable include all solvents for rubber and their mixtures. A trace of oxygen is supplied in the form of air or gaseous oxygen or in the form of a peroxy compound. The temperature should preferably be between 40‹ and 200‹C. Mechanical agitation may be caused by (a) refluxing the solution in which case the reflux leaches the coagulum, or (b) filling the tower with the solution and bubbling in air from the bottom of the tower, or (c) pumping the solution continuously from the bottom to the top of the tower, and (d) stirring, in the case of autoclaves or tanks. When the volume of cleaning liquid is large, the system preferably includes a solution vessel 28 connected to the cleaning liquid return line 24 by a line 29 and at its lower portion to the inlet side of the pump 19 by a line 30. The circulating cleaning liquid passes through the vessel 28 and chunks of coagulum loosened from the tower 10 settle at the bottom of the vessel 28. A breather line 31 which is open to the atmosphere is also connected to the top of the solution vessel 28. A reflux condenser 32 may be included in the breather line. Specification 775,536 is referred to.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US783666XA | 1955-02-17 | 1955-02-17 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB783666A true GB783666A (en) | 1957-09-25 |
Family
ID=22143590
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB33985/55A Expired GB783666A (en) | 1955-02-17 | 1956-11-28 | Improvements in method of cleaning equipment fouled with latex coagulum |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB783666A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3410805A (en) * | 1964-03-09 | 1968-11-12 | Purex Corp Ltd | Paint stripper composition |
-
1956
- 1956-11-28 GB GB33985/55A patent/GB783666A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3410805A (en) * | 1964-03-09 | 1968-11-12 | Purex Corp Ltd | Paint stripper composition |
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