GB765947A - Process for the preparation of lubricating greases - Google Patents
Process for the preparation of lubricating greasesInfo
- Publication number
- GB765947A GB765947A GB1630/55A GB163055A GB765947A GB 765947 A GB765947 A GB 765947A GB 1630/55 A GB1630/55 A GB 1630/55A GB 163055 A GB163055 A GB 163055A GB 765947 A GB765947 A GB 765947A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acid
- clay
- ammonium
- bromide
- lubricating oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M5/00—Solid or semi-solid compositions containing as the essential lubricating ingredient mineral lubricating oils or fatty oils and their use
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- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/08—Inorganic acids or salts thereof
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- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/08—Inorganic acids or salts thereof
- C10M2201/081—Inorganic acids or salts thereof containing halogen
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- C10M2201/08—Inorganic acids or salts thereof
- C10M2201/082—Inorganic acids or salts thereof containing nitrogen
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- C10M2201/083—Inorganic acids or salts thereof containing nitrogen nitrites
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- Lubricants (AREA)
Abstract
Lubricating greases are obtained by dispersing a clay in water to form a hydrosol in which the concentration of the clay is between 0.3 and 0.9 per cent by weight or, if the water contains between 5 and 30 ppm. of alkali metal ions, between 0.1 and 0.9 per cent by weight adding to this hydrosol a surface-active agent and a lubricating oil consisting of silicone fluids such as polymeric dimethyl silicone or methylphenyl silicone or organo silicates such as tetrakis (2-ethyl hexyl) silicate, the surface-active agent being added prior to, or together with the lubricating oil, and dehydrating the mixture the proportion of clay and lubricating oil employed being such that the latter is thickened to a greasy consistency. The clay may be bentonite, hectorite, saponite, nontronite, or attapulgite, or talc or mica. The slumping properties of the clay are improved by adding a critical amount of a water-soluble acid having a dissociation constant greater than 1.5 X 10-5 at 25 DEG C. such as phosphoric acid, boric acid, hydrochloric acid, sulphuric acid hydrofluoric acid, acetic acid, propionic acid, lactic acid or citric acid. The desirable ions may be produced by adding alkali metal salts to the water used such as sodium, potassium or lithium or thiocyanates, citrates, chlorides, bromides, acetates, sulphates or phosphates or halides. The surface-active agent may be a cationic, anionic or nonionic agent such as ammonium, phosphonium, sulphonium, arsonium and stibonium salts. Specified compounds are octadecadienyl ammonium chloride or bromide, tetraethanol ammonium chloride, lauryl dimethyl ammonium bromide, didecyl ammonium chloride, dicyclohexyl-ammonium bromide, triphenyl lauryl phosphonium bromide and dimethyl dicetyl ammonium bromide and aluminium stearate and non-ionic surface active agents such as those known under the Registered Trade Marks "Spans" and "Tweens". Antioxidants such as phenyl - alpha - naphthylamine, 2,6 - di-tertiary butyl - 4 - methyl phenol, methylenedicyclohexananoic acid and the corresponding ethylene and propylene isomers; corrosion-inhibiting agents such as the calcium salts of petroleum sulphonic acids and ammonium and sodium nitrites; and stabilizers such as polyethylene, polyisobutylene or the reaction products of chlorinated naphthalene with sodium ethyl xanthate or the corresponding propyl, butyl, pentyl and hexyl compounds may also be added. Specifications 672,650, [Group III], 706,772; 709,663, 727,353 and 728,779, [all in Group III], are referred to.ALSO:Lubricating greases are obtained by dispersing a clay in water to form a hydrosol in which the concentration of the clay is between 0.3 and 0.9 per cent by weight or, if the water contains between 5 and 30 ppm. of alkali metal ions, between 0.1 and 0.9 per cent by weight adding to this hydrosol a surface-active agent and a lubricating oil, the surface-active agent being added prior to, or together with the lubricating oil, and dehydrating the mixture the proportion of clay and lubricating oil employed being such that the latter is thickened to a greasy consistency. The oil may be a mineral lubricating oil or a synthetic oil such as bis (2-ethylhexyl) sebacate, esters of acids of phosphorous, such as organophosphates, phosphonates and phosphinates such as tricresyl phosphate, trioctyl phosphate and mixtures, copolymers of ethylene oxide and 1,2-propylene oxide, and fluorocarbons and halogenated aromatics. The clay may be bentonite, hectorite, seponite, nontronite, or attapulgite, or talc or mica. The slumping properties of the clay are improved by adding a critical amount of a water-soluble acid having a dissociation constant greater than 1.5 X 10-5 at 25 DEG C. such as phosphoric acid, boric acid, hydrochloric acid, sulphuric acid, hydrofluoric acid, acetic acid, propionic acid, lactic acid or citric acid. The desirable ions may be produced by adding alkali metal salts to the water used such as sodium, potassium or lithium; or thiocyanates, citrates, chlorides, bromides, acetates, sulphates or phosphates or halides. The surface-active agent may be a cationic, anionic or non-ionic agent such as ammonium, phosphonium, sulphonium, arsonium and stibonium salts. Specified compounds are octadecadienyl ammonium chloride or bromide, tetraethanol ammonium chloride, lauryl dimethyl ammonium bromide, didecyl ammonium chloride, dicyclohexyl-ammonium bromide, triphenyl lauryl phosphonium bromide and dimethyl dicetyl ammonium bromide and aluminium stearate and non-ionic surface active agents such as those known under the Registered Trade Marks "Spans" and "Tweens." Antioxidants such as phenyl-alpha-naphthylamine, 2,6-ditertiary butyl-4-methyl phenol, methylene-dicyclohexananoic acid and the corresponding ethylene and propylene isomers; corrosion-inhibiting agents such as the calcium salts of petroleum sulphonic acids and ammonium and sodium nitrites; and stabilizers such as polyethylene, polyisobutylene or the reaction products of chlorinated naphthalene with sodium ethyl xanthate or the corresponding propyl, butyl, pentyl and hexyl compounds may also be added. Specifications 672,650, 706,772, 709,663, 727,353 and 728,779 are referred to.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US765947XA | 1954-01-21 | 1954-01-21 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB765947A true GB765947A (en) | 1957-01-16 |
Family
ID=22133026
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1630/55A Expired GB765947A (en) | 1954-01-21 | 1955-01-19 | Process for the preparation of lubricating greases |
Country Status (3)
Country | Link |
---|---|
DE (1) | DE958416C (en) |
FR (1) | FR1120562A (en) |
GB (1) | GB765947A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1186680A2 (en) * | 2000-09-06 | 2002-03-13 | General Electric Company | Process for applying and aluminum-containing coating using an inorganic slurry mix |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL239497A (en) * | 1958-05-27 |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BE500080A (en) * | 1949-12-19 | |||
BE504196A (en) * | 1950-06-24 |
-
1955
- 1955-01-19 GB GB1630/55A patent/GB765947A/en not_active Expired
- 1955-01-19 FR FR1120562D patent/FR1120562A/en not_active Expired
- 1955-01-20 DE DEN10081A patent/DE958416C/en not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1186680A2 (en) * | 2000-09-06 | 2002-03-13 | General Electric Company | Process for applying and aluminum-containing coating using an inorganic slurry mix |
EP1186680A3 (en) * | 2000-09-06 | 2003-10-22 | General Electric Company | Process for applying and aluminum-containing coating using an inorganic slurry mix |
Also Published As
Publication number | Publication date |
---|---|
FR1120562A (en) | 1956-07-09 |
DE958416C (en) | 1957-02-21 |
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