GB576505A - Spray crystallizing apparatus and process - Google Patents

Spray crystallizing apparatus and process

Info

Publication number
GB576505A
GB576505A GB18898/43A GB1889843A GB576505A GB 576505 A GB576505 A GB 576505A GB 18898/43 A GB18898/43 A GB 18898/43A GB 1889843 A GB1889843 A GB 1889843A GB 576505 A GB576505 A GB 576505A
Authority
GB
United Kingdom
Prior art keywords
crystallizing apparatus
crystals
nitroguanidine
spray
spray crystallizing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB18898/43A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wyeth Holdings LLC
Original Assignee
American Cyanamid Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by American Cyanamid Co filed Critical American Cyanamid Co
Publication of GB576505A publication Critical patent/GB576505A/en
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0004Crystallisation cooling by heat exchange
    • B01D9/0009Crystallisation cooling by heat exchange by direct heat exchange with added cooling fluid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/16Evaporating by spraying
    • B01D1/18Evaporating by spraying to obtain dry solids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The improvement in the method of crystallising nitroguanidine described in the parent Specification comprises dispersing the nitroguanidine solution into and countercurrent to a current of air which is caused to impinge upon a deflecting surface on which the crystals are deposited, the crystals being recovered by washing them from the surface and filtering the slurry thus obtained.
GB18898/43A 1941-06-27 1943-11-12 Spray crystallizing apparatus and process Expired GB576505A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US571527XA 1941-06-27 1941-06-27
US260847XA 1942-12-10 1942-12-10

Publications (1)

Publication Number Publication Date
GB576505A true GB576505A (en) 1946-04-08

Family

ID=26700758

Family Applications (2)

Application Number Title Priority Date Filing Date
GB7487/42A Expired GB571527A (en) 1941-06-27 1942-06-02 Improvements in or relating to the production of crystalline nitroguanidine in an extremely fine state of subdivision
GB18898/43A Expired GB576505A (en) 1941-06-27 1943-11-12 Spray crystallizing apparatus and process

Family Applications Before (1)

Application Number Title Priority Date Filing Date
GB7487/42A Expired GB571527A (en) 1941-06-27 1942-06-02 Improvements in or relating to the production of crystalline nitroguanidine in an extremely fine state of subdivision

Country Status (2)

Country Link
CH (1) CH260847A (en)
GB (2) GB571527A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2179562A (en) * 1985-09-03 1987-03-11 Nestle Sa Dryer and drying method
EP0332067A1 (en) * 1988-03-08 1989-09-13 Röhm Gmbh Process for the preparation of spray-dried emulsion polymers
CN110204461A (en) * 2019-05-15 2019-09-06 西安万德能源化学股份有限公司 The microchannel crystallization processes and device of a kind of nitroguanidine crystal and nitroguanidine

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1004090B (en) * 1955-10-22 1957-03-07 Chemisches Werk Lowi G M B H Process for the production of nitroguanidine with a high specific surface
CN114288703B (en) * 2022-01-25 2023-08-25 南京吉才汇科技有限公司 Crystallization separation equipment for boric acid production

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2179562A (en) * 1985-09-03 1987-03-11 Nestle Sa Dryer and drying method
GB2179562B (en) * 1985-09-03 1989-08-31 Nestle Sa Dryer and drying method
EP0332067A1 (en) * 1988-03-08 1989-09-13 Röhm Gmbh Process for the preparation of spray-dried emulsion polymers
CN110204461A (en) * 2019-05-15 2019-09-06 西安万德能源化学股份有限公司 The microchannel crystallization processes and device of a kind of nitroguanidine crystal and nitroguanidine
CN110204461B (en) * 2019-05-15 2022-04-05 西安万德能源化学股份有限公司 Nitroguanidine crystal and microchannel crystallization process and device of nitroguanidine

Also Published As

Publication number Publication date
CH260847A (en) 1949-04-15
GB571527A (en) 1945-08-29

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