GB450053A - An improved method of purifying zircon - Google Patents
An improved method of purifying zirconInfo
- Publication number
- GB450053A GB450053A GB1969535A GB1969535A GB450053A GB 450053 A GB450053 A GB 450053A GB 1969535 A GB1969535 A GB 1969535A GB 1969535 A GB1969535 A GB 1969535A GB 450053 A GB450053 A GB 450053A
- Authority
- GB
- United Kingdom
- Prior art keywords
- per cent
- carbon
- chlorine
- halogen
- lamp black
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229910052845 zircon Inorganic materials 0.000 title abstract 2
- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 title abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 8
- 229910052799 carbon Inorganic materials 0.000 abstract 4
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 3
- 229910052801 chlorine Inorganic materials 0.000 abstract 3
- 239000000460 chlorine Substances 0.000 abstract 3
- 229910052736 halogen Inorganic materials 0.000 abstract 3
- 150000002367 halogens Chemical class 0.000 abstract 3
- 239000006233 lamp black Substances 0.000 abstract 3
- 239000000463 material Substances 0.000 abstract 3
- 241000416162 Astragalus gummifer Species 0.000 abstract 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 abstract 2
- 229920001615 Tragacanth Polymers 0.000 abstract 2
- 239000011230 binding agent Substances 0.000 abstract 2
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 abstract 2
- 229910052794 bromium Inorganic materials 0.000 abstract 2
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 abstract 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract 1
- 229920001353 Dextrin Polymers 0.000 abstract 1
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 abstract 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 abstract 1
- 229910002091 carbon monoxide Inorganic materials 0.000 abstract 1
- 239000011233 carbonaceous binding agent Substances 0.000 abstract 1
- 239000003245 coal Substances 0.000 abstract 1
- FYGDTMLNYKFZSV-MRCIVHHJSA-N dextrin Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)OC1O[C@@H]1[C@@H](CO)OC(O[C@@H]2[C@H](O[C@H](O)[C@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O FYGDTMLNYKFZSV-MRCIVHHJSA-N 0.000 abstract 1
- 239000007789 gas Substances 0.000 abstract 1
- 239000003292 glue Substances 0.000 abstract 1
- 229910002804 graphite Inorganic materials 0.000 abstract 1
- 239000010439 graphite Substances 0.000 abstract 1
- 150000004820 halides Chemical class 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 229910052740 iodine Inorganic materials 0.000 abstract 1
- 239000011630 iodine Substances 0.000 abstract 1
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 abstract 1
- 239000002006 petroleum coke Substances 0.000 abstract 1
- 239000000843 powder Substances 0.000 abstract 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B1/00—Preliminary treatment of ores or scrap
- C22B1/02—Roasting processes
- C22B1/08—Chloridising roasting
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Geochemistry & Mineralogy (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
Zircon-containing material which has previously been purified, say to a residual content of 0,20 per cent titanium oxide and 0,10 per cent ferric oxide, is treated with a halogen in the absence of air and in the presence of not more than 1 per cent carbon at say 950 DEG C. to form and volatilize halides of the remaining impurities. Chlorine is the preferred halogen, but bromine or iodine may also be used. Preferably, the initial material, which may be the product obtained by the process described in Specification 444,285, is finely milled and formed into nodules after being mixed with carbon and a binder. As carbon, lamp black, graphite, petroleum coke, or soft coal may be used, and as binders, gum tragacanth, dextrine, sugar, or glue. The carbon requirement may also be supplied by using sufficient of the carbonaceous binding agent, or by using gases such as carbonyl chloride or a mixture of carbon monoxide and chlorine. In examples using chlorine or bromine as the halogen 0,2--0,3 per cent lamp black and 0,05--0,10 per cent gum tragacanth are generally used, but in one example a less finely milled initial material is treated in powder form with addition of lamp black.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB1969535A GB450053A (en) | 1935-07-10 | 1935-07-10 | An improved method of purifying zircon |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB1969535A GB450053A (en) | 1935-07-10 | 1935-07-10 | An improved method of purifying zircon |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB450053A true GB450053A (en) | 1936-07-09 |
Family
ID=10133665
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB1969535A Expired GB450053A (en) | 1935-07-10 | 1935-07-10 | An improved method of purifying zircon |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB450053A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3515508A (en) * | 1968-05-06 | 1970-06-02 | American Cyanamid Co | Synthesis of single crystals of zrsio4 and hfsio4 by a halogen transport reaction |
| US4361542A (en) * | 1981-11-23 | 1982-11-30 | General Electric Company | Zircon retrieval |
| US4840774A (en) * | 1984-08-01 | 1989-06-20 | Tam Ceramics Inc. | Process for the production of zirconium tetrachloride from dissociated zircon |
| US5688477A (en) * | 1994-01-31 | 1997-11-18 | Atomic Energy Corporation Of South Africa Limited | Process for reacting dissociated zircon with gaseous hydrogen fluoride |
-
1935
- 1935-07-10 GB GB1969535A patent/GB450053A/en not_active Expired
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3515508A (en) * | 1968-05-06 | 1970-06-02 | American Cyanamid Co | Synthesis of single crystals of zrsio4 and hfsio4 by a halogen transport reaction |
| US4361542A (en) * | 1981-11-23 | 1982-11-30 | General Electric Company | Zircon retrieval |
| US4840774A (en) * | 1984-08-01 | 1989-06-20 | Tam Ceramics Inc. | Process for the production of zirconium tetrachloride from dissociated zircon |
| US5688477A (en) * | 1994-01-31 | 1997-11-18 | Atomic Energy Corporation Of South Africa Limited | Process for reacting dissociated zircon with gaseous hydrogen fluoride |
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