GB327885A - - Google Patents

Info

Publication number
GB327885A
GB327885A GB14049/29A GB1404929A GB327885A GB 327885 A GB327885 A GB 327885A GB 14049/29 A GB14049/29 A GB 14049/29A GB 1404929 A GB1404929 A GB 1404929A GB 327885 A GB327885 A GB 327885A
Authority
GB
United Kingdom
Prior art keywords
monophosphate
acid
potassium
acid salt
liquor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB14049/29A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kali Forschungs Anstalt GmbH
Original Assignee
Kali Forschungs Anstalt GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kali Forschungs Anstalt GmbH filed Critical Kali Forschungs Anstalt GmbH
Publication of GB327885A publication Critical patent/GB327885A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00Phosphorus; Compounds thereof
    • C01B25/16Oxyacids of phosphorus; Salts thereof
    • C01B25/26Phosphates
    • C01B25/30Alkali metal phosphates
    • C01B25/301Preparation from liquid orthophosphoric acid or from an acid solution or suspension of orthophosphates

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)

Abstract

327,885. Kali-Forschungs - Anstalt Ges. Nov. 19, 1928, [Convention date]. Potassium monophosphate is obtaiend by heating potassium chloride with an excess of phosphoric acid of over 30 per cent strength at about 130‹ C., until the chlorine is driven off as hydrochloric acid, this being accelerated by working under reduced pressure. The acid salt. KH2PO4.H3PO4 crystallizes on cooling, and after separation, is treated with sufficient potassium monophosphate solution or water to precipitate potassium monophosphate, and leave a supernatant liquor saturated with the acid and monophosphate. This liquor and the mother liquor from the crystallization of the acid salt are used, with a further addition of phosphoric acid, for the conversion of further quantities of potassium chloride. The precipitated monophosphate is treated with water, and the mother liquor therefrom is again used to decompose the acid salt. Alternatively, the hot solution from the reaction with phosphoric acid may be treated with sufficient potassium monophosphate solution or water to produce, after cooling to precipitate potassium monophosphate, a liquor corresponding in composition to the liquod obtained above in the first described method of splitting the acid salt.
GB14049/29A 1928-11-19 1929-05-06 Expired GB327885A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE327885T 1928-11-19

Publications (1)

Publication Number Publication Date
GB327885A true GB327885A (en) 1930-04-17

Family

ID=31894840

Family Applications (1)

Application Number Title Priority Date Filing Date
GB14049/29A Expired GB327885A (en) 1928-11-19 1929-05-06

Country Status (1)

Country Link
GB (1) GB327885A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113072047A (en) * 2021-05-25 2021-07-06 贵州川恒化工股份有限公司 Production process for continuously preparing monopotassium phosphate

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113072047A (en) * 2021-05-25 2021-07-06 贵州川恒化工股份有限公司 Production process for continuously preparing monopotassium phosphate

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