GB315700A - Production of di-ammonium phosphate - Google Patents
Production of di-ammonium phosphateInfo
- Publication number
- GB315700A GB315700A GB19006/29A GB1900629A GB315700A GB 315700 A GB315700 A GB 315700A GB 19006/29 A GB19006/29 A GB 19006/29A GB 1900629 A GB1900629 A GB 1900629A GB 315700 A GB315700 A GB 315700A
- Authority
- GB
- United Kingdom
- Prior art keywords
- ammonia
- ammonium phosphate
- crystals
- admitted
- mother liquor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/28—Ammonium phosphates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/38—Condensed phosphates
- C01B25/40—Polyphosphates
- C01B25/405—Polyphosphates of ammonium
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Fertilizers (AREA)
Abstract
315,700. Federal Phosphorus Co., (Assignees of Klugh, B. G., and Seyfried, W. R.). July 16, 1928, [Convention date]. Ammonium phosphate. - In preparing di-ammonium phosphate in crystals of uniform size from concentrated phosphoric acid and gaseous ammonia, the heat generated by the neutralization is used to effect evaporation of water from the product. Phosphoric acid of 60-80 per cent strength is mixed with mother liquor from the process to reduce its viscositv and is treated in an insulated acid-proof tank Š with gaseous ammonia admitted through pipes 4. The liquid is agitated by a stirrer 3. Water vapour passes away through an outlet 6. After partial neutralization a further admixture with mother liquor is made, and the mixture is passed into a horizontal rotary cylindrical vessel B, from which air is removed either by a vacuum pump or by displacement by steam or ammonia. Ammonia is admitted through a pipe 15 in quantity sufficient to form di-ammonium phosphate. The solution which first becomes heated to about 100‹ C. is cooled and maintained at about 80‹ C. by water sprayed from a pipe 17. After admission of the ammonia is completed, the solution is allowed to cool slowly to atmospheric temperature, the vessel B being continuously rotated. The slurry is discharged into a filter or centrifuge. The crystals are dried at a temperature below 65‹ C.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US315700XA | 1928-07-16 | 1928-07-16 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB315700A true GB315700A (en) | 1930-06-12 |
Family
ID=21860187
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB19006/29A Expired GB315700A (en) | 1928-07-16 | 1929-06-20 | Production of di-ammonium phosphate |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB315700A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4185075A (en) | 1967-11-20 | 1980-01-22 | Occidental Research and Engineering Ltd. | Phosphoric acid ammoniation apparatus with water quench |
EP0161704A2 (en) * | 1984-04-18 | 1985-11-21 | ENICHEM AGRICOLTURA S.p.A. | Process for the production of water soluble ammonium phosphates |
-
1929
- 1929-06-20 GB GB19006/29A patent/GB315700A/en not_active Expired
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4185075A (en) | 1967-11-20 | 1980-01-22 | Occidental Research and Engineering Ltd. | Phosphoric acid ammoniation apparatus with water quench |
EP0161704A2 (en) * | 1984-04-18 | 1985-11-21 | ENICHEM AGRICOLTURA S.p.A. | Process for the production of water soluble ammonium phosphates |
EP0161704A3 (en) * | 1984-04-18 | 1988-06-22 | Enichem Agricoltura S.P.A. | Process for the production of water soluble ammonium phosphates |
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