GB2285067A - Gland packing yarn - Google Patents

Gland packing yarn Download PDF

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Publication number
GB2285067A
GB2285067A GB9326165A GB9326165A GB2285067A GB 2285067 A GB2285067 A GB 2285067A GB 9326165 A GB9326165 A GB 9326165A GB 9326165 A GB9326165 A GB 9326165A GB 2285067 A GB2285067 A GB 2285067A
Authority
GB
United Kingdom
Prior art keywords
fibres
yarn
core
gland packing
another
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
GB9326165A
Other versions
GB9326165D0 (en
GB2285067B (en
Inventor
Alan William Atkinson
Melanie Jane Walsh
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Federal Mogul Technology Ltd
Original Assignee
T&N Technology Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by T&N Technology Ltd filed Critical T&N Technology Ltd
Priority to GB9326165A priority Critical patent/GB2285067B/en
Publication of GB9326165D0 publication Critical patent/GB9326165D0/en
Publication of GB2285067A publication Critical patent/GB2285067A/en
Application granted granted Critical
Publication of GB2285067B publication Critical patent/GB2285067B/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16JPISTONS; CYLINDERS; SEALINGS
    • F16J15/00Sealings
    • F16J15/16Sealings between relatively-moving surfaces
    • F16J15/18Sealings between relatively-moving surfaces with stuffing-boxes for elastic or plastic packings
    • F16J15/20Packing materials therefor
    • F16J15/22Packing materials therefor shaped as strands, ropes, threads, ribbons, or the like
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K3/00Materials not provided for elsewhere
    • C09K3/10Materials in mouldable or extrudable form for sealing or packing joints or covers
    • C09K3/1025Materials in mouldable or extrudable form for sealing or packing joints or covers characterised by non-chemical features of one or more of its constituents
    • C09K3/1028Fibres
    • DTEXTILES; PAPER
    • D02YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02GCRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
    • D02G3/00Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
    • D02G3/02Yarns or threads characterised by the material or by the materials from which they are made
    • D02G3/06Threads formed from strip material other than paper
    • DTEXTILES; PAPER
    • D02YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02GCRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
    • D02G3/00Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
    • D02G3/22Yarns or threads characterised by constructional features, e.g. blending, filament/fibre
    • D02G3/32Elastic yarns or threads ; Production of plied or cored yarns, one of which is elastic
    • D02G3/328Elastic yarns or threads ; Production of plied or cored yarns, one of which is elastic containing elastane
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K2200/00Chemical nature of materials in mouldable or extrudable form for sealing or packing joints or covers
    • C09K2200/02Inorganic compounds
    • C09K2200/0204Elements
    • C09K2200/0208Carbon
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K2200/00Chemical nature of materials in mouldable or extrudable form for sealing or packing joints or covers
    • C09K2200/02Inorganic compounds
    • C09K2200/0278Fibres
    • C09K2200/0282Carbon fibres

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Textile Engineering (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Sealing Devices (AREA)

Abstract

A gland packing yarn (10) comprises an elongated resilient core (12) and at least one layer of extrusion-inhibiting fibres (18). The core (12) comprises at least one strip of flexible graphite foil (14) and the fibres (18) which may be or carbon are arranged to extend parallel to one another and are adjacent to one another, either axis-parallel or helically. The yarn may be formed by adhesively laminating sheets of graphite foil and of carbon fibres to form layers (14, 18), cutting the laminate into separate yarn-forming strips and rolling the strip to form a round yarn (10). Alternatively a single layer of graphite foil and one of fibres may be joined together and then folded over to form a yarn. Yarns may be braided to form a packing. <IMAGE>

Description

Gland Packing Yarn This invention is concerned with gland packing yarn and with a method of manufacturing such gland packing yarn.
In fluid handling systems, such as valves or pumps, where a moving shaft extends through a fluid-containing wall, a seal is required arcund said shaft. Such seals are often provided by packing a resilient gland packing material, made from a plurality of lengths of yarn braided or pleated together, around the shaft. The parking material is contained in a chamber known as a "stuffing box". The gland packing material must form a tight seal around the shaft while presenting a low-friction surface to the moving shaft. Additionally, the gland packing material must also be stable in the operating environment.
The most common resilient materials used in the gland packings are asbestos and flexible graphite (also known as exfoliated graphite or expanded graphite). Flexible graphite has good resilience, good formability and good temperature resistance. It is also chemically resistant to many fluids encountered by gland packings in practice and is inherently a low-friction material. However, flexible graphite has the disadvantage that it tends to be extruded into the space between the shaft and the opening into the stuffing box through which the shaft passes. The flexible graphite may also build up as a deposit on the shaft.
These problems can be reduced by cladding the flexible graphite core of a gland packing with a knitted or braided sleeve of carbon fibres (see US patent number 4,705,722).
However, the provision of such a knitted or braided sleeve does not prevent extrusion occurring through the spaces between the fibres in such a sleeve. Furthermore, it is not easy to provide a knitted or braided sleeve of sufficiently small dimensions and providing such a small diameter sleeve is expensive.
It is an object of the present invention to provide a yarn which allows a gland packing to be made which has a more efficient barrier to extrusion of flexible graphite forming a core of the yarn.
The invention provides a gland packing yarn comprising an elongated resilient core and at least one layer of extrusion-inhibiting fibres secured to an outer surface of the core, the core comprising at least one strip of flexible graphite foil, wherein the fibres are arranged so that they extend parallel to one another and are adjacent to one another.
It is found that in a gland packing yarn according to the invention, the fibres provide a more efficient barrier against extrusion of the flexible graphite and such a layer is easier to provide than a knitted or braided sleeve.
Furthermore, such a barrier represents a more efficient use of the relatively expensive fibres.
The core of a gland packing yarn according to the invention may comprise a plurality of strips of flexible graphite foil overlying one another and secured together by adhesive.
The extrusion-inhibiting fibres may be carbon fibres which can be secured to the core by adhesive.
The invention also provides a gland packing formed from a plurality of lengths of yarn according to the invention. The lengths of yarn can be braided, plaited or otherwise combined to form the packing.
The invention also provides a method of manufacturing a gland packing yarn comprising securing at least one layer of extrusion-inhibiting fibres to one or more surfaces of an elongated resilient core comprising at least one strip of flexible graphite foil so that the fibres extend parallel to one another- and are adjacent to one another, the method also comprising folding or coiling the core so that the fibres are formed into a layer around the core.
Said fibres may be secured to a sheet of flexible graphite foil eg by adhesive, which is then slit into strips which are first coiled or folded to form the gland packing yarn.
The invention also provides a method of manufacturing a gland packing by manufacturing yarn by a method in accordance with the invention and braiding or plaiting lengths of the yarn together.
There now follows a detailed description, to be read with reference to the accompanying drawings, of five illustrative gland packing yarns in accordance with the invention and also of an illustrative method of manufacturing said yarns.
In the drawings: Figure 1 is a diagrammatic perspective view of various stages in the illustrative method; Figure 2 is a diagrammatic perspective view of further stages in the illustrative method; Figures 3 to 6 are diagrammatic views of the second to fifth illustrative gland packing yarns; and Figure 7 is a diagrammatic perspective view of a gland packing made from the yarn shown in Figure 3.
The illustrative method is for making a gland packing yarn 10 which is illustrated in Figure 2. The yarn 10 comprises an elongated resilient core 12 which is generally cylindrical in shape and comprises three strips 14 of flexible graphite foil which are overlying one another and secured together by adhesive 16. The yarn 10 also comprises a layer of extrusion-inhibiting carbon fibres 18 secured to an outer surface of the core 12. The fibres 18 are arranged so that they extend parallel to one another and are adjacent to one another.
The first illustrative yarn 10 is manufactured by the method illustrated in the Figures 1 and 2. Figure 1 shows the apparatus used in a first stage of the illustrative method. This apparatus comprises a series of reels 30 each of which has a supply of carbon fibre thereon. The reels 30 are arranged in a bank so that a plurality of carbon fibres can be supplied therefrom with the fibres extending parallel to one another and adjacent to one another. These fibres 18 are supplied to the nip between two rollers 32.
The apparatus also comprises three feed rolls 34, 36 and 38 each of which supplies a sheet of flexible graphite foil, 40, 42 and 44 respectively. These sheets of flexible graphite are also supplied to the nip between the rollers 32. The sheet 40 has adhesive on its upper surface which at the nip engages the fibres 18 from the reels 30 so that this adhesive secures the fibres to the top of the sheet 40. The sheet 42 has adhesive on the upper surface thereof so that the sheet 42 is secured to the sheet 40. The sheet 44 has adhesive on both the upper and lower surfaces thereof. The adhesive on the upper surface secures the sheet 44 to the sheet 42 and the adhesive on the lower surface secures further fibres 18 supplied from a further bank of reels 46 to the foil sheet 44.Thus, the rollers 32, which may be heated and which apply pressure to the stack comprising the three sheets 40, 42 and 44 and two layers of fibres 18, serve to compress the stack into a composite sheet 50 which passes away from the rollers 32.
This composite sheet 50 is slit by slitting wheels 52 located downstream of the rollers 32 into a series of strips 56, one of which is shown in Figure 2.
The remainder of the method of making the first illustrative yarn 10 is shown in Figure 2. In this part of the method, each strip 56 which is of rectangular transverse cross-section, is deformed by deforming rollers 58 to have a circular transverse cross-section. This causes the two layers of carbon fibres 18 to form a continuous cylindrical layer around the core 12 which is made up from the three strips of flexible graphite foil.
Lengths of yarn 10 are then braided to form a gland packing 59 a shown in Figure 7.
The second illustrative gland packing yarn 60 shown in Figure 3 is of similar construction to the first illustrative yarn 10 but has been subjected to a longitudinal twisting operation so that the fibres 18 extend parallel to one another helically along the length of the yarn 60. The second illustrative yarn 60 is manufactured by a similar method to the first illustrative yarn 10 but with an additional twisting operation after the operation shown in Figure 2.
Figures 4, 5 and 6 show the third illustrative gland packing yarn 70, the fourth illustrative gland packing yarn 80 and the fifth illustrative gland packing yarn 90, respectively. The yarns 70, 80 and 90 are manufactured by securing parallel and adjacent carbon fibres 18 to one surface of a strip of flexible graphite 72, 82 and 92 respectively. These strips are wider than the strips 14 described above but form the core of the yarns. In the case of the yarn 70, the strip 72 is covered entirely with fibres 18 on one surface thereof and the strip 72 is then folded in half and the two halves secured together by adhesive. This means that the layer of fibres 18 covers all the outer surface of the yarn 70 except for the two edges of the strip 72. In the case of the yarn 80 the strip 82 is covered entirely on one side with parallel and adjacent fibres 18 and the strip 82 is then folded into a small spiral. In the case of the yarn 90, the fibres 18 cover one surface of the strip 92 except for edge portions of said strip. These edge portions are folded over and the strip is then folded in half so that the core formed by the strip 92 has the shape of a "U" with the two upper edges of the arms folded inwardly towards the base of the U. This means that the fibres 18 form a substantially continuous layer around the yarn 90.

Claims (8)

1A gland packing yarn comprising an elongated resilient core and at least one layer of extrusion-inhibiting fibres secured to an outer surface of the core, the core comprising at least one strip of flexible graphite foil, wherein the fibres are arranged so that they extend parallel to one another and are adjacent to one another.
2 A yarn according to Claim 1, wherein the core comprising a plurality of strips of flexible graphite foil overlying one another and secured together by adhesive.
3 A yarn according to either one of claims 1 end 2, wherein the fibres are carbon fibres.
4 A yarn substantially as hereinbefore described with reference to, and as shown in, any one of Figures 2 to
6 of the accompanying drawings.
5 A gland packing formed from a plurality of lengths of yarn according to any one of claims 1 to 4.
6 A method of manufacturing a gland packing yarn comprising securing at least one layer of extrusion inhibiting fibres to one or more surfaces of an elongated resilient core comprising at least one strip of flexible graphite foil so that the fibres extend parallel to one another and are adjacent to one another, the method also comprising folding or coiling the core so that the fibres are formed into a layer around the core.
7 A method according to Claim 6, wherein the said fibres are secured to a sheet of flexible graphite foil which is then slit into strips.
8 A method of manufacturing a gland packing substantially as hereinbefore described with reference to the accompanying drawings.
GB9326165A 1993-12-22 1993-12-22 Gland packing yarn Expired - Fee Related GB2285067B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB9326165A GB2285067B (en) 1993-12-22 1993-12-22 Gland packing yarn

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB9326165A GB2285067B (en) 1993-12-22 1993-12-22 Gland packing yarn

Publications (3)

Publication Number Publication Date
GB9326165D0 GB9326165D0 (en) 1994-02-23
GB2285067A true GB2285067A (en) 1995-06-28
GB2285067B GB2285067B (en) 1997-06-04

Family

ID=10747013

Family Applications (1)

Application Number Title Priority Date Filing Date
GB9326165A Expired - Fee Related GB2285067B (en) 1993-12-22 1993-12-22 Gland packing yarn

Country Status (1)

Country Link
GB (1) GB2285067B (en)

Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2310868A (en) * 1996-03-06 1997-09-10 Flexitallic Sealing Materials Seal material
EP0967423A2 (en) 1998-06-27 1999-12-29 Sgl Technik Gmbh Packing yarn of graphite and plastic sheet
EP0967422A2 (en) 1998-06-27 1999-12-29 Sgl Technik Gmbh Packing yarn of graphite and plastic sheet
US6020276A (en) * 1996-03-06 2000-02-01 Flexitallic Investments, Inc. Seal material
EP1179698A1 (en) * 1999-12-27 2002-02-13 Nippon Pillar Packing Co., Ltd. Expanded graphite-made knitting yarn
EP1179697A1 (en) * 1999-12-27 2002-02-13 Nippon Pillar Packing Co., Ltd. Expanded graphite-made knitting yarn
EP1193428A1 (en) * 1999-12-27 2002-04-03 Nippon Pillar Packing Co., Ltd. Gland packing
EP1193427A1 (en) * 1999-12-27 2002-04-03 Nippon Pillar Packing Co., Ltd. Gland packing
WO2004025151A1 (en) * 2002-09-11 2004-03-25 Nippon Pillar Packing Co., Ltd. Material for gland packing and the gland packing
WO2004025150A1 (en) * 2002-09-11 2004-03-25 Nippon Pillar Packing Co., Ltd. Material for gland packing and the gland packing
WO2004025149A1 (en) * 2002-09-11 2004-03-25 Nippon Pillar Packing Co., Ltd. Material for gland packing and the gland packing
US6777086B2 (en) 2001-08-31 2004-08-17 Julian Norley Laminates prepared from impregnated flexible graphite sheets
JP2007170674A (en) * 2007-02-05 2007-07-05 Nippon Pillar Packing Co Ltd Expanded graphite knitting yarn
JP2011140743A (en) * 2011-02-09 2011-07-21 Nippon Pillar Packing Co Ltd Knitting yarn made of expanded graphite
JP2011144929A (en) * 2011-02-09 2011-07-28 Nippon Pillar Packing Co Ltd Gland packing

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB298766A (en) * 1927-10-07 1928-10-18 Gordon Fraser Method of and apparatus for the production of braiding
US4705722A (en) * 1986-06-18 1987-11-10 Nippon Pillar Packing Co., Ltd. Gland packing
EP0340303A1 (en) * 1986-11-25 1989-11-08 Nippon Pillar Packing Co., Ltd. Packing material and packing made of the same
GB2243883A (en) * 1990-05-08 1991-11-13 Kempchen & Co Gmbh Braided sealing cord
US5225262A (en) * 1991-04-29 1993-07-06 A. W. Chesterton Co. Braided high-temperature packing comprising a core of folded flexible graphite sheet

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB298766A (en) * 1927-10-07 1928-10-18 Gordon Fraser Method of and apparatus for the production of braiding
US4705722A (en) * 1986-06-18 1987-11-10 Nippon Pillar Packing Co., Ltd. Gland packing
EP0340303A1 (en) * 1986-11-25 1989-11-08 Nippon Pillar Packing Co., Ltd. Packing material and packing made of the same
GB2243883A (en) * 1990-05-08 1991-11-13 Kempchen & Co Gmbh Braided sealing cord
US5225262A (en) * 1991-04-29 1993-07-06 A. W. Chesterton Co. Braided high-temperature packing comprising a core of folded flexible graphite sheet

Cited By (35)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6020276A (en) * 1996-03-06 2000-02-01 Flexitallic Investments, Inc. Seal material
GB2310868B (en) * 1996-03-06 1999-11-10 Flexitallic Sealing Materials Seal material
GB2310868A (en) * 1996-03-06 1997-09-10 Flexitallic Sealing Materials Seal material
AU723319B2 (en) * 1996-03-06 2000-08-24 Flexitallic Investments, Inc Seal material
US6270083B1 (en) 1998-06-27 2001-08-07 Sgl Technik Gmbh Packing yarn made of graphite foil and plastic foil and method of manufacturing a packing yarn
EP0967422A2 (en) 1998-06-27 1999-12-29 Sgl Technik Gmbh Packing yarn of graphite and plastic sheet
EP0967423A3 (en) * 1998-06-27 2000-09-13 Sgl Technik Gmbh Packing yarn of graphite and plastic sheet
EP0967422A3 (en) * 1998-06-27 2000-09-13 Sgl Technik Gmbh Packing yarn of graphite and plastic sheet
EP0967423A2 (en) 1998-06-27 1999-12-29 Sgl Technik Gmbh Packing yarn of graphite and plastic sheet
US6385956B1 (en) 1998-06-27 2002-05-14 Sgl Technik Gmbh Packing yarn made of graphite foil and metal foil and method of manufacturing a packing yarn
EP1193428A1 (en) * 1999-12-27 2002-04-03 Nippon Pillar Packing Co., Ltd. Gland packing
EP1179697A1 (en) * 1999-12-27 2002-02-13 Nippon Pillar Packing Co., Ltd. Expanded graphite-made knitting yarn
EP1193427A1 (en) * 1999-12-27 2002-04-03 Nippon Pillar Packing Co., Ltd. Gland packing
EP1179698A1 (en) * 1999-12-27 2002-02-13 Nippon Pillar Packing Co., Ltd. Expanded graphite-made knitting yarn
EP1193428A4 (en) * 1999-12-27 2005-08-03 Nippon Pillar Packing Gland packing
EP1179698A4 (en) * 1999-12-27 2005-08-03 Nippon Pillar Packing Expanded graphite-made knitting yarn
EP1179697A4 (en) * 1999-12-27 2005-08-03 Nippon Pillar Packing Expanded graphite-made knitting yarn
EP1193427A4 (en) * 1999-12-27 2005-08-03 Nippon Pillar Packing Gland packing
US6777086B2 (en) 2001-08-31 2004-08-17 Julian Norley Laminates prepared from impregnated flexible graphite sheets
WO2004025149A1 (en) * 2002-09-11 2004-03-25 Nippon Pillar Packing Co., Ltd. Material for gland packing and the gland packing
KR100681889B1 (en) * 2002-09-11 2007-02-12 니폰 필라고교 가부시키가이샤 Material for gland packing and the gland packing
WO2004025150A1 (en) * 2002-09-11 2004-03-25 Nippon Pillar Packing Co., Ltd. Material for gland packing and the gland packing
WO2004025151A1 (en) * 2002-09-11 2004-03-25 Nippon Pillar Packing Co., Ltd. Material for gland packing and the gland packing
EP1541909A4 (en) * 2002-09-11 2006-03-08 Nippon Pillar Packing Material for gland packing and the gland packing
US7140171B2 (en) 2002-09-11 2006-11-28 Nippon Pillar Packing Co., Ltd. Material for gland packing and the gland packing
US7155892B2 (en) 2002-09-11 2007-01-02 Nippon Pillar Packing Co., Ltd. Material for gland packing and the gland packing
EP1541909A1 (en) * 2002-09-11 2005-06-15 Nippon Pillar Packing Co., Ltd. Material for gland packing and the gland packing
KR100681867B1 (en) * 2002-09-11 2007-02-12 니폰 필라고교 가부시키가이샤 Material for gland packing and the gland packing
CN100429439C (en) * 2002-09-11 2008-10-29 日本皮拉工业株式会社 Material for gland packing and the gland packing
US7353645B2 (en) 2002-09-11 2008-04-08 Nippon Pillar Packing Co., Ltd. Material for gland packing and the gland packing
CN100380025C (en) * 2002-09-11 2008-04-09 日本皮拉工业株式会社 Material for gland packing and the gland packing
CN100380024C (en) * 2002-09-11 2008-04-09 日本皮拉工业株式会社 Material for gland packing and the gland packing
JP2007170674A (en) * 2007-02-05 2007-07-05 Nippon Pillar Packing Co Ltd Expanded graphite knitting yarn
JP2011140743A (en) * 2011-02-09 2011-07-21 Nippon Pillar Packing Co Ltd Knitting yarn made of expanded graphite
JP2011144929A (en) * 2011-02-09 2011-07-28 Nippon Pillar Packing Co Ltd Gland packing

Also Published As

Publication number Publication date
GB9326165D0 (en) 1994-02-23
GB2285067B (en) 1997-06-04

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Legal Events

Date Code Title Description
732E Amendments to the register in respect of changes of name or changes affecting rights (sect. 32/1977)
PCNP Patent ceased through non-payment of renewal fee

Effective date: 19971222