GB2243528A - Method for producing kimchi-fermented sausage - Google Patents
Method for producing kimchi-fermented sausage Download PDFInfo
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- GB2243528A GB2243528A GB9103503A GB9103503A GB2243528A GB 2243528 A GB2243528 A GB 2243528A GB 9103503 A GB9103503 A GB 9103503A GB 9103503 A GB9103503 A GB 9103503A GB 2243528 A GB2243528 A GB 2243528A
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- GB
- United Kingdom
- Prior art keywords
- kimchi
- meat
- sausage
- mixture
- fermented
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B4/00—General methods for preserving meat, sausages, fish or fish products
- A23B4/044—Smoking; Smoking devices
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/60—Comminuted or emulsified meat products, e.g. sausages; Reformed meat from comminuted meat product
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/60—Comminuted or emulsified meat products, e.g. sausages; Reformed meat from comminuted meat product
- A23L13/65—Sausages
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Storage Of Fruits Or Vegetables (AREA)
- Meat, Egg Or Seafood Products (AREA)
Abstract
Kimchi-fermented sausages are produced by fermenting kimchi, containing for example 3.5 to 8.0% salt, to produce acidification, separating kimchi solids containing kimchi-fermenting bacteria for example by centrifugation at 8,000 to 12,000 rpm, and mixing the kimchi solids with meat to form a mixture containing for example 3 to 20% of kimchi by weight of the meat, then fermenting the mixture and if desired drying the fermented mixture. Kimchee is a fermented vegetable food.
Description
- 1 4 METHOD FOR PRODUCING KIMCHI-FERMENTED SAUSAGE The present invention
relates to a method for producing kimchi-fer - mented sausages, which are produced by mixing kimchi containing 1.3% acidity with meat at the rateof 3-20%, and then fermenting the first and second fermenting process of the KIMCHI-meat mixture firstly at 15 C-20"C and secondly at 27"C-3f C,respectively.
The kimchi is a traditional Korean fermented vegetable food made by mixing the salted vegetables such as cabbages or radishes with vari -ous seasonings and then naturally maturing. In the fermenting and maturing of the kimchi, a lot of number of micro-organisms act on the fermentation and maturity of the kimchi. Among them, fungi are acid-vulnerable aerobic micro-organisms that th -rive at temperatures 20-3e C, and yeasts are aerobic micro-organisms that thrive at temperatures 270C-26C, give unique fragrance and taste of matured kimchi and also form thin layers on th kimchi in the postmaturity period of the kimchi.
Accordingly, primary micro-organisms involved in the fermentation of the kimchi are bacteria derived from raw materials such as cabbage, 4 4 the seasonings and other materials during preparation of the kimchi.
In the maturing process of the kimchi, aerobic bacteria, such as achromobacter, flavobacterium, 6acillus and pseudomonas groups, which are not associated with lactic acid fermentation grow at the beginning of fermentation and then acid-enduring anaerobic bacteria, such as lactobacillus Planetarium and leuconostoc ze-senteroides grow proceeding the lactic acid fermentation. After the maturity period, yeasts, suchas, sacchromyces, torulopsis, candida, hansenula, debaryomy -ces, pichia and rhodotorula, grow by use of lactic acid.
As the fermentation goes on, the number of aerobic bacteria are reduced andorganic acids like the lactic acid are gradually generated and accordingly pH goes down and acid-enduring bacteria start to grow. As theacidenduring bacteria grow up producing lactic acid, malic acid, acetic acid and oxalic acid, the PH of the kimchi is dramatically dro -pped, content of reduced sugar is decreased, acidity is increased, and therefore the fermenting and maturing process is proceeded. if the kimchi is fermented and matured in low temperature, it is leuconostoc mesenteroides that is a bacterium which continues to multiply in numbers from the beginning until the maturity period of the kim chi where it reaches a maximum in numbers. While the leuconostoc Mesente -roides is not much as able other acid-producIng bacteria in Pro - ducingacid, it is a bacteria that plays important role in giving uni -que tastes and flavors up to a degree of being capable of maturing i 4 the kimchiby itself. This bacteria grows more actively when it is given a lowerdegree of salt concentration. This bacteria also grow mor -erapidly at cooler temperatures than a normal temperature, thriving up to 32% of the entire population of various bacteria. The leuconosioc me-senteroides is a representative lactic acid bacteria that give the kimchi not only sour taste but also pleasant taste by producing or -ganic acid group such as the lactic acid, ethanol and carbon bioxide gas. The environment of the kimchi changes eventually from aerobic to anaerobicby taste products. Therefore, most of aerobic bacteria that do not contribute to fermentation of the kimchi is slowed down in growth or die away. When the kimchi is matured at room temperature.
lactobacillus planetarium grows more actively than leuconostoc mesente -roides and gets to 32% of the entire bacteria-pqpulation. The lactobacillus: planetarium is a representative lactic-fermenting lactic bacteria that in-creases acidity by lactic acid producing.
Fermented sausages originate from the Middle Ages and are known to be produced by filling salted fresh meat into intestines and drying. Italian salami of today is considered to be the origin.
Traditionally, most of fermented sausages including the salami and fermented hams known as uncooked ham or raw ham were produced mainly in Mediterranean coastal areas. They had its slightly different brand name, shape and processing methods in each area. Recently, it was discovered that natural fermentation is caused by bac i A -teria so that fermented sausages and hams could be artificially pro - duced by applying lactic acid bacteria as starter culture. As Cesari tried applying yeast in 1919, Kurk used micrococci in 1921, Drake used bacilli and sprilli in 1928, Jesen and Paddock used lactobacilli in 1940, the technology of producing the fermented sausages and hams was gradually developed. The technology has continually been improved as summer sausage was developed in U.S.A. in 1957 by developing freezingdried pediococus cerevisiae. Racovita developed a method of spraying penicillium on the surface of dried sausage in 1968, Eilberg and Liepe developed a method of bringing streptomycetes into a mixed lactic bacteria(streptococci and lactobacilli) in 1977, and Bartholomew and Blumer developed a method of applying pediococcus cerevisiae to country ham in 1977.
As in the foregoing, mi cro-organ isms, such as bacteria, fung-I and yeast, can be used in meat fermentation but most popularly applied mic roorganisms used as starter micro-organisms are salt-enduring lactic bacteria, such as micrococci, streptococcl, pediococci and lactobacil N 1 The invention provides a first aspect a method for producing a kimchifermented sausage, which method comprises:
(a) fermenting kimchi to produce acidification thereof and separating kimchi solids containing kimchifermenting bacteria; and (b) mixing the kimchi solids with meat such that the kimchi solids are 3 to 20 by weight of meat, fermenting the mixture of kimchi and meat by performing a first fermentation at 15 to 200C and fermentation at 27 to 320C, and then drying the fermented mixture.
In a second aspect, the invention provides a mould for producing kimchifermented sausage, which method comprises:- (a) fermenting kimchi containing from 3.5 to 8% by weight of salt at from 15 to 300C to produce acidification and separating kimchi solids containing kimchi-fermenting bacteria; and (b) mixing the kimchi solids with meat and fermenting the kimchi-meat mixture.
The invention includes a method for producing a kimchi-fermented sausage comprising mixing fermented kimchi solids containing fermentation bacteria with meat and fermenting the kimchi-meat mixture.
In the illustrative embodiments hereinafter described the kimchi fermentation period is controlled by adjusting temperature until lactic bacteria, which are most adaptive to fermenting meat, are most active in the kimchi, and substances of the kimchi and the bacteria therein are obtained by using a centrifugal method and then the kimchi substances already having flavour and taste are applied to the meat, thus the meat is fermented by re-fermentation of the kimchi thereafter. Therefore, natural lactic acid bacteria with matured kimchi can use instead of starter culture and avoid a danger of vacteriphage.
4 -6 In addition, temperature control is provided in a way that can improve fermentation process of the meat in which the micro-organisms of the kimchi acts as fermentation agent.
And in general processes, such as method of slicing and mixing the kimchi and the raw material meat, filling the mixture of kimchi and the meat into a casing, and then salting, fermenting, smoking and drying operations, prior technology has been employed.
In order to use the kimchi as a starter culture effectively, each process is specifically conditioned so that fermenting and maturing can be better performed.
7 v V BRIEF DESCRIPTION OF THE ATTACHED DRAWING
For a better understanding of the invention and to show how the same may be carried into effect reference will now be made, by way of example, to the accompanied diagrammatic drawing, in which:
FIG 1 is a process diagram illustrating processes of producing kim chifermented sausage.
DETAILED DESCRIPTION OF THE INVENTION
As shown in FIG 1, the producing of the kimchi-fermented sausage comprises following four processes.
First process, which is Kimchi Preparation process, wherein cabbages are salted In salty water of 7-15% concentration, and dehydrated until the salt concentration reaches 3.5-8%; seasonings, such as pepper powder, raw garlic, ginger, and sugar and so on are mixed with the salted cabbages; the salted and seasonings-mixed cabbages are matured at temperatures of 15-30' C for 4-30 days so that pediococci and lactobacilli can grow well; and when the lactic bacteria grow until total acidity reaches 1.3%, fermen -tation is stopped and now, the cabbage has become kimchi that contain -s a lot of micro-organism, so the kimchi is put into centrifugal oper k 4 -ation at 7,000-15,000rpm for fifteen minutes, and only the precipita tion of the kimchi containing bacteria, which is to be'used as starte -r micro-organism, is obtained. Second process, which is Mixing and Filling process, wherein fresh meat stored at -3 to -I' C and backfat of pig are plated two times with diameters of 0.8 cm and 0.3cm, respectively the ground meat is mixed with the kimchi material, which is 3-20% of the ground meat quantity, for 5-10 minutes and this mixture of the kimchi and the ground meat are filled into a flex! -6le fiber-type casing, stored at 5 C for 12-24 hours in a dark room, so that stabilization of microorganisms of the kimchi and salting can be achieved. Third process, which is Fermentation and Smoking process, wherein: after the second process, a first fermentation and smoking are per -formed at 15-2dC for 12-15 hours at the same time, and then a second fermentation and smoking are performed at 27-3Z C is performed until the mixture reaches to pH5.2-4.8. Fourth process, which is Drying process. wherein: after the third process, the mixture is heated up until internal temperatures of the mixture reache 68-7Z C; or the mixture is put into a container, which provides constant temperature and humidity, and the mixture is dried up by applying gradual decrease from RH95% down to RH a 9 - 65% at d C and the wind velocity of 10m per minute for 3-12 weeks.
Now, some exemplaries of the present invention are presented hereinafter.
EXAMPLE 1
As shown in TABLE 1, after cabbage kimch! of 3.5% salt concentration is prepared, the kimchi is matured at 15 C for 20-30 days until the kimchi gets an acidity level of 1.3%. This kimchi is sliced by go -ing through plates with diameters of 0.8cm amd 0.3cm, respectively. And then the kimchi is put into a centrifugal operation at 8000-12000 rpm for 15 minutes and only kimchi material is obtained by removing supernatant, and the precipitation is ready to be used as starter micro-organisms (First process) i TABLE 1 Composition of Kimchi Mixture 41 Items Quantity(g) cabbage powdered pepper green onion garlic ginger sugar alt S 3.0 2.0 0.7 0.7 0.7 3.5-7.0 Fresh meat and fat as raw materials of fermented-sausage are ones that have been stored at -3 to -fC and plated with diameters of 0.8cm and 0. 3cm respectively. The first mixing is performed by mixing the ground meat with seasonings as listed in TABLE 2 into a mixer, The second mixing is performed by mixing the ground fat into mixture of the fresh meat and seasonings, and finally the third mixing Is performed by mixing 108-2" of the kimchi material that is prepared in first pro -cess and has starter micro-organisms. The final mixture is put Into fibrous casing that has a diameter of 1.0 - 5.Ocm and then is stored at 5 0 C in a dark room for 18 hours for 4 equ-ibilization(Second Process).
After equibilization is completed, fermentation and smoking are perfor -med at the same time.
In an early period of the fermentation, the sausage is kept at 15-2jC for 12 hours to promote growth of leuconosioc mesenteroides and mic rococcl groups which generate aromatic products. And then the tempe rature is raised up to 277C at which lactic acid is generated by drama tic increase of lactic bacteria, and the fermentation is stopped when pH of the meat is dropped down to 5.0. For smoking, it is recommenda -ble to use sawdust of wood that is aromatic and has no resin(Third Process).
After the fermentation and smoking have been completed, the sausage is put into a humidity chamber, and the sausage is dried up by applying gradual decrease of relative humidity from 95X down to 65X at 10 C and in the wind velocity of 10m per minute for 3-12 weeks(Fourth Process).
1.
TABLE 2 Composition of Kimchi- Fermented Sausag Items Weight(g) MEAT meat(pork) meat(beef) backfat SALTING AGENTS SEASONINGS Sodium Nitrate(HaNO3) Sodium Nitrite(NaNOz) Sodium Ascorbate(C6H700a) Salt Garl l c black pepper mustard powdered pepper ginger grape sugar matured kimchi 1350 1350 900 0.58 0.29 3.2 60.0 36 7.2 1.26 36 18 32.4 108-720 1 1 f 1 EXAMPLE 2
The kimchi is prepared with 5% salt concentration as shown in Table 1, fermented and matured at 25-30 C for 4-10 days where total acidity becomes 1.3%, and then ground twice as shown in EXAMPLE 1 (First Proce -ss) Fresh meat and fat ground as in the EXAMPLE 1 are mixed as in EXAMPLE 1, and 360-7209 of the ground kimchi is mixed. this mixture is put in to a fiber-type casing, which' has diameter of 3-7cm and kept therein for 6-12 hours at IJ C for performing salting operation and stabilization of starter micro-organisms (Second Process).
The mixture is fermented and smoked at the same time, first for 12 hours at 15 C and then at temperatures of 28-d C until pH of the mixture is dropped down to 4.8 at which level the fermentation and smoking operation is stopped (Third Process).
The sausage which the fermentation is completed is heated up to a poin -t where temperature of inner center of the sausage reaches 7i Wour -th Process).
i - 14 TABLE 3 Characteristics of Kimchi-Fermented Sausage Characteristics EXAMPLE I EXAMPLE2 (dry-type) (semi-dry-type) PH 5.0 4.8 moisture(%) 28-43 52 moisture/protein 1.7-2.3: 1 3.2 1 free amino 47-40 32 nitrogen(mg%) total number of 6.2 x 107 - 2.5 x 106 4.6 x 103 bacteria(cells/9) number of lactic 8.9 X 106 - 1.4 x 106 2.3 x 103 bacteria(cells/9) taste and flavor mild taste strongly sour taste Products produced according to foregoing methods can be classified as dry- type kimchi-fermented sausage(EXAMPLE 1) and Semi-dry-type kimchifermented sausage(EXAMPLE 2) as shown in TABLE 3. The EXAMPLE 1 is dry-type sausage which contains low moisture and shows relatively high in pH due to long drying period, so that it is hard and has mild taste. On the other hand, the EXAMPLE 2 is Semi-dry-type sausage which shows relatively low in pH, and contains high moisture,so that it has strong sour taste.
1 1 k t
Claims (15)
- CLAIMS 1. A method for producing a kimchi-fermented sausage, which methodcomprises:(a) fermenting kimchi to produce acidification thereof and separating kimchi solids containing kimchifermenting bacteria; and (b) mixing the kimchi solids with meat such that the kimchi solids are 3 to 20% by weight of meat, fermenting the mixture of kimchi and meat by performing a first fermentation at 15 to 200C and a second fermentation at 27 to 320C, and then drying the fermented mixture.
- 2. A method as claimed in Claim 1, wherein the fermenting kimchi in step (a) contains from
- 3.5 to 8% by weight of salt.-15 3. A method as claimed in Claim 1 or Claim 2, wherein step (a) is conducted at a temperature of from 15 to 3WC.
- 4. A method as claimed in any one of Claims 1 to 3, wherein said fermentation step (a) is continued until the total acid content of the ferment reaches 1.3% by weight.
- 5. A method as claimed in any one of Claims 1 to 4, wherein said kimchi solids are separated by centrifugation.
- 6. A method as claimed in Claim 5, wherein said centrifugation is conducted at 8,000 to 12,000 rpm.
- 7. A method for producing kimchi-fermented sausage, which method comprises:(a) fermenting kimchi containing from 3.5 to 8 by weight of salt at from 15 to 30C to produce acidification and separating kimchi solids containing kimchi-fermenting bacteria; and (b) mixing the kimchi solids with meat and fermenting the kimchi-meat mixture.
- 8. A method as claimed in any preceding claim, including the step of forming the kimchi meat mixture into a sausage.
- 9. A method as claimed in Claim 8, wherein said mixture is formed into a sausage prior to drying said mixture.
- 10. A method as claimed in any preceding claim, wherein:the fermented mixture in the form of a sausage is put into a humidity chamber, and dried by applying a gradual decrease of relative humidity from RH95 to RH65 at about 100C and at a wind velocity of about 10m per minute for 3 to 12 weeks, so as to produce a dry-type sausage.
- 11. A method for producing kimchi-fermented sausage as claimed in Claim 1, wherein:the fermented mixture in the form of a sausage is heated up to a point where inside temperature of the sausage reaches 68 to 72C, so as to produce a semi-dry type sausage.
- 12. A method as claimed in any preceding claim, wherein:after the kimchi solids are mixed with the meat, the mixture is put into a casing, is stored in a dark room for 6 to 12 hours, and is then fermented two times.
- 13. A method for producing a kimchi- fermented sausage substantially as hereinbefore described in Example 1 or Example 2.
- 14. A method for producing a kimchi-fermented sausage comprising mixing fermented kimchi solids containing fermentation bacteria with meat and fermenting the kimchimeat mixture.
- 15. A method for producing a kimchi-fermented sausage, method comprising the processes of (a) fermenting kimchi, wherein 3.5 to 8.0 salt is contained, at 15 to 300C until total acid content reaches 1.3 and then obtaining kimchi precipitation containing kimchi-fermenting bacteria by putting the kimchi into a 30 centrifugal operation at 8,000 to 12,000 rpm; and (b) mixing the kimchi precipitation with meat being 3 to 20 of meat, fermenting a mixture of kimchi and meat, performing a first fermentation at 15 to 200C and fermentation at 27 to 32C, and then drying the fermented mixture.Published 1991 at The Patent Office, Concept House, Cardiff Road. Newport, Gwent NP9 I RH. Further copies may be obtained from Sales BranclL Unit 6. Nine Mile Point. Cwmielinfach. Cross Keys. Newport. NPI 7HZ Printed by Multiplex techniques lid, St Mary Cray. Kent.4 t
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1019900005894A KR920003050B1 (en) | 1990-04-26 | 1990-04-26 | Method for making fermented kimchi sausage |
Publications (3)
Publication Number | Publication Date |
---|---|
GB9103503D0 GB9103503D0 (en) | 1991-04-10 |
GB2243528A true GB2243528A (en) | 1991-11-06 |
GB2243528B GB2243528B (en) | 1994-04-20 |
Family
ID=19298400
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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GB9103503A Expired - Fee Related GB2243528B (en) | 1990-04-26 | 1991-02-20 | Method for producing kimchi-fermented sausage |
Country Status (3)
Country | Link |
---|---|
KR (1) | KR920003050B1 (en) |
DE (1) | DE4104710A1 (en) |
GB (1) | GB2243528B (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6689403B1 (en) * | 1999-03-25 | 2004-02-10 | Karl Muller Gmbh & Co. | Mixture for reddening meat products |
US8075933B2 (en) | 2003-10-17 | 2011-12-13 | Creta Farm Societe Anonyme Industrial And Commercial | Method for the preparation of fermented dry or semi-dried meat products, with partial substitution of the animal fat and direct incorporation of olive oil |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102007015816B4 (en) * | 2007-03-30 | 2008-11-20 | Böklunder Plumrose GmbH & Co. KG | Process for the production of packaged and smoked spreadable raw sausages |
KR101353119B1 (en) * | 2011-12-29 | 2014-01-17 | 오인숙 | The manufacturing method of fermentation sausages additional herb |
KR101703075B1 (en) * | 2014-12-11 | 2017-02-27 | 사회복지법인 평화의 마을 | Lactic acid bacteria salami and manufacturing method thereof |
CN104905301A (en) * | 2015-06-12 | 2015-09-16 | 郭锡铎 | Natural enzyme sausage and making method thereof |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH02154666A (en) * | 1988-12-05 | 1990-06-14 | Tetsunosuke Yoshimura | Sausage seasoned with soybean paste |
-
1990
- 1990-04-26 KR KR1019900005894A patent/KR920003050B1/en not_active IP Right Cessation
-
1991
- 1991-02-15 DE DE4104710A patent/DE4104710A1/en active Granted
- 1991-02-20 GB GB9103503A patent/GB2243528B/en not_active Expired - Fee Related
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6689403B1 (en) * | 1999-03-25 | 2004-02-10 | Karl Muller Gmbh & Co. | Mixture for reddening meat products |
US8075933B2 (en) | 2003-10-17 | 2011-12-13 | Creta Farm Societe Anonyme Industrial And Commercial | Method for the preparation of fermented dry or semi-dried meat products, with partial substitution of the animal fat and direct incorporation of olive oil |
Also Published As
Publication number | Publication date |
---|---|
GB9103503D0 (en) | 1991-04-10 |
DE4104710C2 (en) | 1992-11-12 |
KR910017956A (en) | 1991-11-30 |
KR920003050B1 (en) | 1992-04-13 |
GB2243528B (en) | 1994-04-20 |
DE4104710A1 (en) | 1991-10-31 |
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Effective date: 20000220 |