GB2107704A - Process for the preparation of urea - Google Patents
Process for the preparation of urea Download PDFInfo
- Publication number
- GB2107704A GB2107704A GB08224952A GB8224952A GB2107704A GB 2107704 A GB2107704 A GB 2107704A GB 08224952 A GB08224952 A GB 08224952A GB 8224952 A GB8224952 A GB 8224952A GB 2107704 A GB2107704 A GB 2107704A
- Authority
- GB
- United Kingdom
- Prior art keywords
- urea
- reaction zone
- zone
- stripping
- pressure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000006243 chemical reaction Methods 0.000 claims abstract description 137
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 136
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 126
- 239000004202 carbamide Substances 0.000 claims abstract description 122
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 118
- 229910021529 ammonia Inorganic materials 0.000 claims abstract description 67
- BVCZEBOGSOYJJT-UHFFFAOYSA-N ammonium carbamate Chemical compound [NH4+].NC([O-])=O BVCZEBOGSOYJJT-UHFFFAOYSA-N 0.000 claims abstract description 64
- KXDHJXZQYSOELW-UHFFFAOYSA-N carbonic acid monoamide Natural products NC(O)=O KXDHJXZQYSOELW-UHFFFAOYSA-N 0.000 claims abstract description 64
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 63
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 61
- 238000000034 method Methods 0.000 claims abstract description 43
- 230000015572 biosynthetic process Effects 0.000 claims abstract description 30
- 238000002360 preparation method Methods 0.000 claims abstract description 8
- 239000000203 mixture Substances 0.000 claims description 55
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 claims description 42
- 238000010438 heat treatment Methods 0.000 claims description 4
- 229960000510 ammonia Drugs 0.000 description 59
- 239000007789 gas Substances 0.000 description 53
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 35
- 229910001868 water Inorganic materials 0.000 description 28
- 238000003786 synthesis reaction Methods 0.000 description 25
- 239000000047 product Substances 0.000 description 19
- 239000011261 inert gas Substances 0.000 description 14
- 238000000354 decomposition reaction Methods 0.000 description 13
- 239000007788 liquid Substances 0.000 description 11
- 238000009833 condensation Methods 0.000 description 10
- 230000005494 condensation Effects 0.000 description 10
- 238000004519 manufacturing process Methods 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 150000003672 ureas Chemical class 0.000 description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 229920006395 saturated elastomer Polymers 0.000 description 2
- 238000007086 side reaction Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000013589 supplement Substances 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000003467 diminishing effect Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000002706 hydrostatic effect Effects 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- VUZPPFZMUPKLLV-UHFFFAOYSA-N methane;hydrate Chemical compound C.O VUZPPFZMUPKLLV-UHFFFAOYSA-N 0.000 description 1
- 229910000069 nitrogen hydride Inorganic materials 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000003134 recirculating effect Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000005201 scrubbing Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
- C07C273/04—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds from carbon dioxide and ammonia
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
- C07C273/08—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds from ammoniacal liquor
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Saccharide Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL8104039A NL8104039A (nl) | 1981-09-01 | 1981-09-01 | Werkwijze voor de bereiding van ureum. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB2107704A true GB2107704A (en) | 1983-05-05 |
Family
ID=19837995
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB08224952A Withdrawn GB2107704A (en) | 1981-09-01 | 1982-09-01 | Process for the preparation of urea |
Country Status (15)
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL8303424A (nl) * | 1983-10-06 | 1985-05-01 | Unie Van Kunstmestfab Bv | Werkwijze voor de bereiding van ureum. |
| IT1290423B1 (it) * | 1996-10-17 | 1998-12-03 | Eurotecnica Contractors And En | Procedimento per la sintesi di urea da anidride carbonica e ammoniaca |
| RU2529462C1 (ru) * | 2013-05-15 | 2014-09-27 | Открытое акционерное общество "Научно-исследовательский и проектный институт карбамида и продуктов органического синтеза" (ОАО "НИИК") | Способ получения карбамида |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1147734A (en) * | 1966-03-29 | 1969-04-02 | Sumitomo Chemical Co | Method for the preparation of urea |
| CH468356A (de) * | 1966-04-05 | 1969-02-15 | Inventa Ag | Verfahren zur Aufarbeitung des bei der Synthese von Harnstoff aus Ammoniak und Kohlendioxyd in einem Synthesereaktor bei erhöhtem Druck und erhöhter Temperatur erhaltenen Synthesegemisches |
| NL168506C (nl) * | 1970-12-31 | 1982-04-16 | Stamicarbon | Werkwijze voor de bereiding van ureum. |
| BE787832A (fr) * | 1971-09-02 | 1973-02-22 | Stamicarbon | Procede pour la preparation d'uree |
| NL7307036A (enrdf_load_stackoverflow) * | 1973-05-21 | 1974-11-25 |
-
1981
- 1981-09-01 NL NL8104039A patent/NL8104039A/nl not_active Application Discontinuation
-
1982
- 1982-08-10 ZA ZA825789A patent/ZA825789B/xx unknown
- 1982-08-30 GR GR69157A patent/GR76909B/el unknown
- 1982-08-30 DD DD82242880A patent/DD204250A5/de unknown
- 1982-08-30 IT IT49046/82A patent/IT1149070B/it active
- 1982-08-31 PL PL23809382A patent/PL238093A1/xx unknown
- 1982-08-31 EP EP82902529A patent/EP0086804A1/en not_active Withdrawn
- 1982-08-31 WO PCT/EP1982/000187 patent/WO1983000861A1/en not_active Application Discontinuation
- 1982-08-31 ES ES515378A patent/ES8306104A1/es not_active Expired
- 1982-08-31 BR BR8207840A patent/BR8207840A/pt unknown
- 1982-08-31 JP JP57502599A patent/JPS58501374A/ja active Pending
- 1982-08-31 KR KR1019820003930A patent/KR840001132A/ko not_active Withdrawn
- 1982-09-01 GB GB08224952A patent/GB2107704A/en not_active Withdrawn
- 1982-09-01 OA OA57793A patent/OA07201A/xx unknown
-
1983
- 1983-04-29 NO NO831532A patent/NO831532L/no unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DD204250A5 (de) | 1983-11-23 |
| GR76909B (enrdf_load_stackoverflow) | 1984-09-04 |
| BR8207840A (pt) | 1983-09-06 |
| JPS58501374A (ja) | 1983-08-18 |
| ES515378A0 (es) | 1983-05-01 |
| EP0086804A1 (en) | 1983-08-31 |
| ZA825789B (en) | 1983-06-29 |
| IT1149070B (it) | 1986-12-03 |
| IT8249046A0 (it) | 1982-08-30 |
| ES8306104A1 (es) | 1983-05-01 |
| NO831532L (no) | 1983-04-29 |
| WO1983000861A1 (en) | 1983-03-17 |
| PL238093A1 (en) | 1983-03-28 |
| OA07201A (fr) | 1984-04-30 |
| NL8104039A (nl) | 1983-04-05 |
| KR840001132A (ko) | 1984-03-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| WAP | Application withdrawn, taken to be withdrawn or refused ** after publication under section 16(1) |