GB201223095D0 - Method of processing polycrystalline diamond material - Google Patents
Method of processing polycrystalline diamond materialInfo
- Publication number
- GB201223095D0 GB201223095D0 GBGB1223095.9A GB201223095A GB201223095D0 GB 201223095 D0 GB201223095 D0 GB 201223095D0 GB 201223095 A GB201223095 A GB 201223095A GB 201223095 D0 GB201223095 D0 GB 201223095D0
- Authority
- GB
- United Kingdom
- Prior art keywords
- leaching
- acid
- diamond
- leaching mixture
- polycrystalline diamond
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 229910003460 diamond Inorganic materials 0.000 title abstract 5
- 239000010432 diamond Substances 0.000 title abstract 5
- 239000000463 material Substances 0.000 title abstract 5
- 238000000034 method Methods 0.000 title abstract 2
- 238000002386 leaching Methods 0.000 abstract 7
- 239000000203 mixture Substances 0.000 abstract 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 4
- 239000002253 acid Substances 0.000 abstract 3
- 150000007513 acids Chemical class 0.000 abstract 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract 2
- 239000011707 mineral Substances 0.000 abstract 2
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical compound OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 229910017604 nitric acid Inorganic materials 0.000 abstract 1
- 239000001117 sulphuric acid Substances 0.000 abstract 1
- 235000011149 sulphuric acid Nutrition 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24D—TOOLS FOR GRINDING, BUFFING OR SHARPENING
- B24D99/00—Subject matter not provided for in other groups of this subclass
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/91—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics involving the removal of part of the materials of the treated articles, e.g. etching
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/52—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbon, e.g. graphite
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F1/00—Etching metallic material by chemical means
- C23F1/02—Local etching
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F1/00—Etching metallic material by chemical means
- C23F1/10—Etching compositions
- C23F1/14—Aqueous compositions
- C23F1/16—Acidic compositions
- C23F1/28—Acidic compositions for etching iron group metals
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/42—Non metallic elements added as constituents or additives, e.g. sulfur, phosphor, selenium or tellurium
- C04B2235/422—Carbon
- C04B2235/427—Diamond
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Structural Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Metallurgy (AREA)
- Earth Drilling (AREA)
- Carbon And Carbon Compounds (AREA)
Abstract
A method of processing a polycrystalline diamond (PCD) material having a non-diamond phase comprising a diamond catalyst/solvent material is disclosed which comprises leaching an amount of the diamond catalyst/solvent from the PCD material by exposing at least a portion of the PCD material to a leaching mixture. The leaching mixture comprises hydrochloric acid and one or more additional mineral acids, the molar concentration of the hydrochloric acid being greater than the molar concentration of the one or more additional mineral acids in the leaching mixture. The additional acids may be sulphuric acid, phosphoric acid, perchloric acid or nitric acid. The leaching may be carried out by heating the leaching mixture to a temperature at or grater to the boiling temperature of the leaching mixture.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201161581214P | 2011-12-29 | 2011-12-29 | |
GBGB1122434.2A GB201122434D0 (en) | 2011-12-29 | 2011-12-29 | Method of processing polycrystalline diamond material |
Publications (2)
Publication Number | Publication Date |
---|---|
GB201223095D0 true GB201223095D0 (en) | 2013-02-06 |
GB2499299A GB2499299A (en) | 2013-08-14 |
Family
ID=45695062
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GBGB1122434.2A Ceased GB201122434D0 (en) | 2011-12-29 | 2011-12-29 | Method of processing polycrystalline diamond material |
GB1223095.9A Withdrawn GB2499299A (en) | 2011-12-29 | 2012-12-20 | A method of processing a polycrystalline diamond material |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GBGB1122434.2A Ceased GB201122434D0 (en) | 2011-12-29 | 2011-12-29 | Method of processing polycrystalline diamond material |
Country Status (4)
Country | Link |
---|---|
US (1) | US20140352228A1 (en) |
CN (1) | CN104136641A (en) |
GB (2) | GB201122434D0 (en) |
WO (1) | WO2013098217A1 (en) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US10718166B2 (en) | 2014-06-20 | 2020-07-21 | Halliburton Energy Services, Inc. | Laser-leached polycrystalline diamond and laser-leaching methods and devices |
US11766761B1 (en) | 2014-10-10 | 2023-09-26 | Us Synthetic Corporation | Group II metal salts in electrolytic leaching of superabrasive materials |
US10011000B1 (en) * | 2014-10-10 | 2018-07-03 | Us Synthetic Corporation | Leached superabrasive elements and systems, methods and assemblies for processing superabrasive materials |
CA2965343C (en) | 2014-11-24 | 2019-05-28 | Halliburton Energy Services, Inc. | Determining the leaching profile of a cutter on a drilling tool |
US11794290B2 (en) * | 2021-01-24 | 2023-10-24 | Cnpc Usa Corporation | Method for forming cutters |
Family Cites Families (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4288248A (en) * | 1978-03-28 | 1981-09-08 | General Electric Company | Temperature resistant abrasive compact and method for making same |
DE602006005844D1 (en) * | 2005-10-14 | 2009-04-30 | Element Six Production Pty Ltd | METHOD FOR PRODUCING A MODIFIED GRINDING BOD PRESSURE |
US20070169419A1 (en) * | 2006-01-26 | 2007-07-26 | Ulterra Drilling Technologies, Inc. | Sonochemical leaching of polycrystalline diamond |
US8066087B2 (en) * | 2006-05-09 | 2011-11-29 | Smith International, Inc. | Thermally stable ultra-hard material compact constructions |
US8080074B2 (en) * | 2006-11-20 | 2011-12-20 | Us Synthetic Corporation | Polycrystalline diamond compacts, and related methods and applications |
US8028771B2 (en) * | 2007-02-06 | 2011-10-04 | Smith International, Inc. | Polycrystalline diamond constructions having improved thermal stability |
US20100012389A1 (en) * | 2008-07-17 | 2010-01-21 | Smith International, Inc. | Methods of forming polycrystalline diamond cutters |
US7757792B2 (en) * | 2008-07-18 | 2010-07-20 | Omni Ip Ltd | Method and apparatus for selectively leaching portions of PDC cutters already mounted in drill bits |
EP2379256B1 (en) * | 2009-01-16 | 2020-07-15 | Baker Hughes Holdings LLC | Methods of forming polycrystalline diamond cutting elements |
US7971663B1 (en) * | 2009-02-09 | 2011-07-05 | Us Synthetic Corporation | Polycrystalline diamond compact including thermally-stable polycrystalline diamond body held in barrier receptacle and applications therefor |
US8069937B2 (en) * | 2009-02-26 | 2011-12-06 | Us Synthetic Corporation | Polycrystalline diamond compact including a cemented tungsten carbide substrate that is substantially free of tungsten carbide grains exhibiting abnormal grain growth and applications therefor |
US7972395B1 (en) * | 2009-04-06 | 2011-07-05 | Us Synthetic Corporation | Superabrasive articles and methods for removing interstitial materials from superabrasive materials |
GB0922695D0 (en) * | 2009-12-30 | 2010-02-17 | Element Six Production Pty Ltd | Enhanced acid leaching by direct heating of PCD |
US8974562B2 (en) * | 2010-04-14 | 2015-03-10 | Baker Hughes Incorporated | Method of making a diamond particle suspension and method of making a polycrystalline diamond article therefrom |
CN102059341A (en) * | 2011-01-27 | 2011-05-18 | 成都比拓超硬材料有限公司 | Treatment method for improving high temperature resistance of polycrystalline diamond composite material |
-
2011
- 2011-12-29 GB GBGB1122434.2A patent/GB201122434D0/en not_active Ceased
-
2012
- 2012-12-20 GB GB1223095.9A patent/GB2499299A/en not_active Withdrawn
- 2012-12-20 WO PCT/EP2012/076520 patent/WO2013098217A1/en active Application Filing
- 2012-12-20 CN CN201280070378.8A patent/CN104136641A/en active Pending
- 2012-12-20 US US14/368,705 patent/US20140352228A1/en not_active Abandoned
Also Published As
Publication number | Publication date |
---|---|
GB201122434D0 (en) | 2012-02-08 |
WO2013098217A1 (en) | 2013-07-04 |
CN104136641A (en) | 2014-11-05 |
GB2499299A (en) | 2013-08-14 |
US20140352228A1 (en) | 2014-12-04 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
WAP | Application withdrawn, taken to be withdrawn or refused ** after publication under section 16(1) |