GB1548334A - Carbamate derivatives - Google Patents
Carbamate derivativesInfo
- Publication number
- GB1548334A GB1548334A GB257777A GB257777A GB1548334A GB 1548334 A GB1548334 A GB 1548334A GB 257777 A GB257777 A GB 257777A GB 257777 A GB257777 A GB 257777A GB 1548334 A GB1548334 A GB 1548334A
- Authority
- GB
- United Kingdom
- Prior art keywords
- carbamate derivatives
- dihydroxymethylpyridine
- methylcarbamate
- recrystallisation
- hydrochloride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/24—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D213/28—Radicals substituted by singly-bound oxygen or sulphur atoms
- C07D213/30—Oxygen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pyridine Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
2,6-Dihydroxymethylpyridine-bis-(N-methylcarbamate) in the gamma 2 modification is obtained from 2,6-dihydroxymethylpyridine hydrochloride using methyl isocyanate, the purification being effected by recrystallisation from an alcohol-water mixture and the drying being carried out at 50-100 DEG C. The product thus obtained, which is employed in the therapy of vascular diseases, can easily be made into tablets.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
HU76RI584A HU171664B (en) | 1976-01-24 | 1976-01-24 | Process for preparing 2,6-dihydroxymethyl-pyridine-bis/n-methyl-carbamate / in gamma 2 crystal form for direct tablet compression |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1548334A true GB1548334A (en) | 1979-07-11 |
Family
ID=11000992
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB257777A Expired GB1548334A (en) | 1976-01-24 | 1977-01-21 | Carbamate derivatives |
Country Status (10)
Country | Link |
---|---|
JP (1) | JPS5291870A (en) |
AT (1) | AT347968B (en) |
CH (1) | CH638496A5 (en) |
CS (1) | CS215094B2 (en) |
DD (1) | DD129213A5 (en) |
DE (1) | DE2702772A1 (en) |
GB (1) | GB1548334A (en) |
HU (1) | HU171664B (en) |
PL (1) | PL106095B1 (en) |
SU (2) | SU689619A3 (en) |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL126013C (en) * | 1963-04-13 | 1900-01-01 | ||
AT258954B (en) * | 1963-04-13 | 1967-12-27 | Michiro Inoue | Process for the preparation of new bis (hydroxymethyl) pyridinedicarbamate derivatives |
AT258953B (en) * | 1963-04-13 | 1967-12-27 | Michiro Inoue | Process for the preparation of new bis (hydroxymethyl) pyridinedicarbamate derivatives |
AT258955B (en) * | 1965-11-08 | 1967-12-27 | Michiro Inoue | Process for the preparation of new bis (hydroxymethyl) pyridinedicarbamate derivatives |
ES377775A1 (en) * | 1970-03-21 | 1973-06-01 | Prodes Sa | Procedure for the obtaining of ester bis- (N-meticarbamico) of 2,6-piridindimetanol. (Machine-translation by Google Translate, not legally binding) |
JPS497286A (en) * | 1972-05-24 | 1974-01-22 |
-
1976
- 1976-01-24 HU HU76RI584A patent/HU171664B/en not_active IP Right Cessation
- 1976-12-31 CS CS889776A patent/CS215094B2/en unknown
-
1977
- 1977-01-03 CH CH1177A patent/CH638496A5/en not_active IP Right Cessation
- 1977-01-17 AT AT22277A patent/AT347968B/en not_active IP Right Cessation
- 1977-01-21 DD DD19703377A patent/DD129213A5/en unknown
- 1977-01-21 GB GB257777A patent/GB1548334A/en not_active Expired
- 1977-01-22 PL PL19550577A patent/PL106095B1/en unknown
- 1977-01-22 JP JP544277A patent/JPS5291870A/en active Granted
- 1977-01-24 DE DE19772702772 patent/DE2702772A1/en active Granted
- 1977-01-24 SU SU772446201A patent/SU689619A3/en active
- 1977-12-29 SU SU772559952A patent/SU697051A3/en active
Also Published As
Publication number | Publication date |
---|---|
CS215094B2 (en) | 1982-07-30 |
CH638496A5 (en) | 1983-09-30 |
HU171664B (en) | 1978-02-28 |
SU689619A3 (en) | 1979-09-30 |
DE2702772A1 (en) | 1977-07-28 |
DE2702772C2 (en) | 1988-01-21 |
JPS6135984B2 (en) | 1986-08-15 |
PL106095B1 (en) | 1979-11-30 |
ATA22277A (en) | 1978-06-15 |
JPS5291870A (en) | 1977-08-02 |
AT347968B (en) | 1979-01-25 |
SU697051A3 (en) | 1979-11-05 |
DD129213A5 (en) | 1978-01-04 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PCNP | Patent ceased through non-payment of renewal fee |
Effective date: 19940121 |