GB1513196A - Process for the digestion of the hemi-celluloses of xylan-containing natural products to obtain xylose therefrom - Google Patents
Process for the digestion of the hemi-celluloses of xylan-containing natural products to obtain xylose therefromInfo
- Publication number
- GB1513196A GB1513196A GB41050/76A GB4105076A GB1513196A GB 1513196 A GB1513196 A GB 1513196A GB 41050/76 A GB41050/76 A GB 41050/76A GB 4105076 A GB4105076 A GB 4105076A GB 1513196 A GB1513196 A GB 1513196A
- Authority
- GB
- United Kingdom
- Prior art keywords
- stage
- solution
- extracting
- xylan
- xylose
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- SRBFZHDQGSBBOR-IOVATXLUSA-N D-xylopyranose Chemical compound O[C@@H]1COC(O)[C@H](O)[C@H]1O SRBFZHDQGSBBOR-IOVATXLUSA-N 0.000 title abstract 8
- PYMYPHUHKUWMLA-UHFFFAOYSA-N arabinose Natural products OCC(O)C(O)C(O)C=O PYMYPHUHKUWMLA-UHFFFAOYSA-N 0.000 title abstract 4
- SRBFZHDQGSBBOR-UHFFFAOYSA-N beta-D-Pyranose-Lyxose Natural products OC1COC(O)C(O)C1O SRBFZHDQGSBBOR-UHFFFAOYSA-N 0.000 title abstract 4
- 229920002488 Hemicellulose Polymers 0.000 title abstract 2
- 230000029087 digestion Effects 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 229930014626 natural product Natural products 0.000 title abstract 2
- 229920001221 xylan Polymers 0.000 title abstract 2
- 150000004823 xylans Chemical class 0.000 title abstract 2
- 239000000243 solution Substances 0.000 abstract 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 3
- 238000001914 filtration Methods 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 2
- 238000011084 recovery Methods 0.000 abstract 2
- 239000007858 starting material Substances 0.000 abstract 2
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 238000010306 acid treatment Methods 0.000 abstract 1
- 229910001854 alkali hydroxide Inorganic materials 0.000 abstract 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract 1
- 239000012670 alkaline solution Substances 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 229920005610 lignin Polymers 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 abstract 1
- 150000007524 organic acids Chemical class 0.000 abstract 1
- 235000005985 organic acids Nutrition 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 abstract 1
- 229960002675 xylitol Drugs 0.000 abstract 1
- 235000010447 xylitol Nutrition 0.000 abstract 1
- 239000000811 xylitol Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
- C13K13/002—Xylose
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Abstract
1513196 Extracting xylose from xylancontaining material SUD-CHEMIE AG 4 Oct 1976 [8 Oct 1975] 41050/76 Heading C2S A process for the two-stage digestion of hemicelluloses of xylan-containing natural products to obtain xylose comprises (i) treating the starting material in a first stage at standard pressure or elevated pressure and elevated temperature with an alkali hydroxide solution in sufficient amount to split off and neutralize the acetic acid linked in the starting material, filtering off the alkaline solution from the reaction vessel, (ii) extracting the residue whilst in the same vessel at 20-120 C. with at least one liquid surge and (iii) subjecting the solid residue to an acid treatment in a second stage in the same vessel at elevated pressure and temperature, filtering off the acid solution from the reaction vessel and extracting the residue obtained with at least one liquid surge and processing the solution and extract from stage (iii) for the recovery of xylose and xylitol and optionally processing the solution and extract from the first stage for the recovery of organic acids and lignin.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2545110A DE2545110C3 (en) | 1975-10-08 | 1975-10-08 | Process for the two-stage digestion of the hemicelluloses of xylan-containing natural products for the purpose of obtaining xylose |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1513196A true GB1513196A (en) | 1978-06-07 |
Family
ID=5958664
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB41050/76A Expired GB1513196A (en) | 1975-10-08 | 1976-10-04 | Process for the digestion of the hemi-celluloses of xylan-containing natural products to obtain xylose therefrom |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US4072538A (en) |
| JP (1) | JPS5248700A (en) |
| AT (1) | AT349033B (en) |
| BE (1) | BE847080A (en) |
| CH (1) | CH626405A5 (en) |
| DE (1) | DE2545110C3 (en) |
| FI (1) | FI60236C (en) |
| FR (1) | FR2327314A1 (en) |
| GB (1) | GB1513196A (en) |
| IT (1) | IT1069832B (en) |
| SE (1) | SE434278B (en) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4201596A (en) * | 1979-01-12 | 1980-05-06 | American Can Company | Continuous process for cellulose saccharification |
| US4205673A (en) * | 1979-02-05 | 1980-06-03 | Mine Safety Appliances Company | Breathing apparatus with an automatic firing mechanism |
| US4370172A (en) * | 1981-03-17 | 1983-01-25 | Compagnie De Construction Mecanique Sulzer, French Societe Anonyme | Controlled vortex pump feed for supplying cellulose-containing material to reaction vessel |
| FR2668165A1 (en) * | 1990-10-23 | 1992-04-24 | Toulouse Inst Nat Polytech | PROCESS AND PLANT FOR PREPARING CONCENTRATED JUICE OF PENTOSIS AND / OR HEXOSES FROM HEMICELLULOSE - RICH VEGETABLE MATERIAL. |
| US5125977A (en) * | 1991-04-08 | 1992-06-30 | The United States Of America As Represented By The United States Department Of Energy | Two-stage dilute acid prehydrolysis of biomass |
| US7812153B2 (en) * | 2004-03-11 | 2010-10-12 | Rayonier Products And Financial Services Company | Process for manufacturing high purity xylose |
| US7815741B2 (en) * | 2006-11-03 | 2010-10-19 | Olson David A | Reactor pump for catalyzed hydrolytic splitting of cellulose |
| US7815876B2 (en) * | 2006-11-03 | 2010-10-19 | Olson David A | Reactor pump for catalyzed hydrolytic splitting of cellulose |
| KR101657100B1 (en) * | 2008-10-29 | 2016-09-19 | 삼성전자주식회사 | Method and Apparatus for Fractionating Lignocellulose-based Biomass |
| CA2739707A1 (en) * | 2008-11-20 | 2010-05-27 | E.I. Du Pont De Nemours And Company | Sugar production by decrystallization and hydrolysis of polysaccharide enriched biomass |
| US8524474B2 (en) * | 2008-11-20 | 2013-09-03 | E I Du Pont De Nemours And Company | Process for producing a concentrated sugar solution by enzymatic saccharification of polysaccharide enriched biomass |
| WO2010059796A2 (en) * | 2008-11-20 | 2010-05-27 | E. I. Du Pont De Nemours And Company | Process for producing a sugar solution by combined chemical and enzymatic saccharification of polysaccharide enriched biomass |
| CN103842524A (en) * | 2011-07-07 | 2014-06-04 | 波特研究公司 | Systems and methods for acid recycle |
| CN111996296A (en) * | 2020-09-15 | 2020-11-27 | 无锡绿色分离应用技术研究所有限公司 | Environment-friendly method for extracting xylose from hemicellulose |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3565687A (en) * | 1968-02-26 | 1971-02-23 | Okamura Oil Mill | Manufacturing method of xylose with cottonseed hulls as material |
| IT1025544B (en) * | 1973-11-23 | 1978-08-30 | Sued Chemie Ag | PROCESS FOR BREAKING DOWN WOOD OF DAISIES |
| IT1025347B (en) * | 1973-11-23 | 1978-08-10 | Sued Chemie Ag | PROCESS FOR THE BREAKDOWN OF OAT SHELLS |
| FI51371C (en) * | 1974-10-04 | 1976-12-10 | Rosenlew Ab Oy W | Method for decomposing a polysaccharide-containing raw material by acid hydrolysis. |
| US3990904A (en) * | 1976-05-11 | 1976-11-09 | Sud-Chemie Ag | Method for the preparation of xylose solutions |
-
1975
- 1975-10-08 DE DE2545110A patent/DE2545110C3/en not_active Expired
-
1976
- 1976-09-16 CH CH1176076A patent/CH626405A5/de not_active IP Right Cessation
- 1976-09-17 FI FI762664A patent/FI60236C/en not_active IP Right Cessation
- 1976-09-17 AT AT689976A patent/AT349033B/en not_active IP Right Cessation
- 1976-10-04 US US05/729,058 patent/US4072538A/en not_active Expired - Lifetime
- 1976-10-04 GB GB41050/76A patent/GB1513196A/en not_active Expired
- 1976-10-06 SE SE7611093A patent/SE434278B/en not_active IP Right Cessation
- 1976-10-06 IT IT51604/76A patent/IT1069832B/en active
- 1976-10-07 FR FR7630166A patent/FR2327314A1/en active Granted
- 1976-10-07 JP JP51119893A patent/JPS5248700A/en active Pending
- 1976-10-08 BE BE171343A patent/BE847080A/en not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| FI60236B (en) | 1981-08-31 |
| DE2545110A1 (en) | 1977-04-28 |
| DE2545110C3 (en) | 1981-09-10 |
| JPS5248700A (en) | 1977-04-18 |
| AT349033B (en) | 1979-03-12 |
| FR2327314A1 (en) | 1977-05-06 |
| SE7611093L (en) | 1977-04-09 |
| FI60236C (en) | 1981-12-10 |
| US4072538A (en) | 1978-02-07 |
| CH626405A5 (en) | 1981-11-13 |
| ATA689976A (en) | 1978-08-15 |
| DE2545110B2 (en) | 1980-01-03 |
| BE847080A (en) | 1977-01-31 |
| SE434278B (en) | 1984-07-16 |
| FR2327314B1 (en) | 1981-01-09 |
| IT1069832B (en) | 1985-03-25 |
| FI762664A (en) | 1977-04-09 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |