GB1469352A - Process for the preparation of sodium percarbonate - Google Patents

Process for the preparation of sodium percarbonate

Info

Publication number
GB1469352A
GB1469352A GB2518174A GB2518174A GB1469352A GB 1469352 A GB1469352 A GB 1469352A GB 2518174 A GB2518174 A GB 2518174A GB 2518174 A GB2518174 A GB 2518174A GB 1469352 A GB1469352 A GB 1469352A
Authority
GB
United Kingdom
Prior art keywords
product
sodium
solution
sodium percarbonate
litre
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2518174A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
United Initiators GmbH and Co KG
Original Assignee
United Initiators GmbH and Co KG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by United Initiators GmbH and Co KG filed Critical United Initiators GmbH and Co KG
Publication of GB1469352A publication Critical patent/GB1469352A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B15/00Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
    • C01B15/055Peroxyhydrates; Peroxyacids or salts thereof
    • C01B15/10Peroxyhydrates; Peroxyacids or salts thereof containing carbon
    • C01B15/103Peroxyhydrates; Peroxyacids or salts thereof containing carbon containing only alkali metals as metals

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Detergent Compositions (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)

Abstract

1469352 Sodium percarbonate PEROXIDECHEMIE GmbH 6 June 1974 [6 June 1973] 25181/74 Heading C1A Sodium percarbonate is prepared by reacting a H 2 O 2 solution which contains 2À95-10 g./litre at Mg<SP>++</SP> ions in the form of a magnesium salt (other than the silicate), with a Na 2 CO 3 solution or suspension containing 2-8 g./litre of sodium hexametaphosphate or a sodium polyacrylate of a temperature of 10-30‹ C.; crystals of the product are precipitated and separated. The product has a spherulitic crystal habit and has a high resistance to abrasion. Optionally, sodium chloride may be added to the reaction system to increase the yield of the precipitated product, while water glass solution may be added in order to stabilize the product towards loss of active oxygen.
GB2518174A 1973-06-06 1974-06-06 Process for the preparation of sodium percarbonate Expired GB1469352A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19732328803 DE2328803C3 (en) 1973-06-06 1973-06-06 Process for the production of an abrasion-resistant, coarse-grained sodium percarbonate

Publications (1)

Publication Number Publication Date
GB1469352A true GB1469352A (en) 1977-04-06

Family

ID=5883208

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2518174A Expired GB1469352A (en) 1973-06-06 1974-06-06 Process for the preparation of sodium percarbonate

Country Status (7)

Country Link
BE (1) BE815864A (en)
DE (1) DE2328803C3 (en)
ES (1) ES426733A1 (en)
FR (1) FR2232508B1 (en)
GB (1) GB1469352A (en)
IT (1) IT1014827B (en)
NL (1) NL7407414A (en)

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4428914A (en) 1977-12-23 1984-01-31 Interox Process for making sodium percarbonate granules
JPH04227693A (en) * 1990-04-09 1992-08-17 Unilever Nv Granular bleaching detergent composition
US5346680A (en) * 1992-10-16 1994-09-13 Solvay Interox Gmbh Sodium percarbonate stabilized by coating
US5478488A (en) * 1993-05-08 1995-12-26 Solvay Interox Gmbh Detergent composition containing alkali metal peroxysalt stabilized with alkali metal sulfate and chloride
US5560896A (en) * 1993-08-31 1996-10-01 Degussa Aktiengesellschaft Method for producing granulated sodium percarbonate
EP0748764A1 (en) * 1995-06-08 1996-12-18 AUSIMONT S.p.A. Process for producing sodium percarbonate in granular form
EP0796817A2 (en) * 1996-03-19 1997-09-24 Elf Atochem S.A. Sodium percarbonate and process for its production
WO1997035806A1 (en) * 1996-03-27 1997-10-02 Solvay Interox (Societe Anonyme) Process for producing a percarbonate
US6231828B1 (en) * 1997-03-26 2001-05-15 Solvay Interox Sa Process for producing sodium percarbonate
KR100541269B1 (en) * 1996-03-27 2006-04-12 솔베이인터록스(소시에떼아노님) Method of manufacturing percarbonate

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
LU75466A1 (en) * 1976-07-27 1978-02-08
DE2644148C3 (en) * 1976-09-30 1983-05-11 Degussa Ag, 6000 Frankfurt Continuous process for the production of a compact, coarse-grained sodium percarbonate
DE2644147C3 (en) * 1976-09-30 1983-05-19 Degussa Ag, 6000 Frankfurt Process for the production of a compact, coarse-grained sodium percarbonate
AT356627B (en) * 1976-10-22 1980-05-12 Treibacher Chemische Werke Ag METHOD FOR PRODUCING SODIUM PERCARBONATE
DE2800760C2 (en) * 1978-01-09 1983-01-27 Degussa Ag, 6000 Frankfurt Process for the production of sodium percarbonate from a soda solution or suspension
DE4338401A1 (en) * 1993-11-10 1995-05-11 Degussa Process for the production of abrasion-resistant sodium percarbonate with high dissolving speed

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB549841A (en) * 1941-09-12 1942-12-09 Laporte Ltd B Manufacture of sodium percarbonate
BE463513A (en) * 1943-08-09

Cited By (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4428914A (en) 1977-12-23 1984-01-31 Interox Process for making sodium percarbonate granules
JPH04227693A (en) * 1990-04-09 1992-08-17 Unilever Nv Granular bleaching detergent composition
US5346680A (en) * 1992-10-16 1994-09-13 Solvay Interox Gmbh Sodium percarbonate stabilized by coating
US5478488A (en) * 1993-05-08 1995-12-26 Solvay Interox Gmbh Detergent composition containing alkali metal peroxysalt stabilized with alkali metal sulfate and chloride
US5560896A (en) * 1993-08-31 1996-10-01 Degussa Aktiengesellschaft Method for producing granulated sodium percarbonate
EP0748764A1 (en) * 1995-06-08 1996-12-18 AUSIMONT S.p.A. Process for producing sodium percarbonate in granular form
US6340452B1 (en) 1996-03-19 2002-01-22 Solvay Sodium percarbonate and process for producing it
EP0796817A2 (en) * 1996-03-19 1997-09-24 Elf Atochem S.A. Sodium percarbonate and process for its production
EP0796817A3 (en) * 1996-03-19 1997-10-01 Elf Atochem S.A. Sodium percarbonate and process for its production
AU714881B2 (en) * 1996-03-19 2000-01-13 Solvay (Societe Anonyme) Novel sodium percarbonate and process for producing it
KR100244785B1 (en) * 1996-03-19 2000-02-15 엘프 아토켐 소시에떼아노님 Novel sodium percarbonate and process for producing it
CN1055448C (en) * 1996-03-19 2000-08-16 索尔维公司 Novel sodium percarbonate and process for producing it
WO1997035806A1 (en) * 1996-03-27 1997-10-02 Solvay Interox (Societe Anonyme) Process for producing a percarbonate
AU733834B2 (en) * 1996-03-27 2001-05-24 Solvay Interox (Societe Anonyme) Process for producing a percarbonate
US6482385B2 (en) * 1996-03-27 2002-11-19 Solvay Interox (Societe Anonyme) Sodium percarbonate and process for producing sodium percarbonate
KR100541269B1 (en) * 1996-03-27 2006-04-12 솔베이인터록스(소시에떼아노님) Method of manufacturing percarbonate
US6231828B1 (en) * 1997-03-26 2001-05-15 Solvay Interox Sa Process for producing sodium percarbonate

Also Published As

Publication number Publication date
FR2232508B1 (en) 1980-04-11
DE2328803C3 (en) 1982-11-25
DE2328803B2 (en) 1978-06-22
FR2232508A1 (en) 1975-01-03
BE815864A (en) 1974-12-04
ES426733A1 (en) 1976-07-01
IT1014827B (en) 1977-04-30
NL7407414A (en) 1974-12-10
DE2328803A1 (en) 1975-01-09

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Legal Events

Date Code Title Description
PS Patent sealed
429A Application made for amendment of specification (sect. 29/1949)
429H Application (made) for amendment of specification now open to opposition (sect. 29/1949)
429D Case decided by the comptroller ** specification amended (sect. 29/1949)
SP Amendment (slips) printed
PCNP Patent ceased through non-payment of renewal fee

Effective date: 19930606