GB1469352A - Process for the preparation of sodium percarbonate - Google Patents
Process for the preparation of sodium percarbonateInfo
- Publication number
- GB1469352A GB1469352A GB2518174A GB2518174A GB1469352A GB 1469352 A GB1469352 A GB 1469352A GB 2518174 A GB2518174 A GB 2518174A GB 2518174 A GB2518174 A GB 2518174A GB 1469352 A GB1469352 A GB 1469352A
- Authority
- GB
- United Kingdom
- Prior art keywords
- product
- sodium
- solution
- sodium percarbonate
- litre
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/055—Peroxyhydrates; Peroxyacids or salts thereof
- C01B15/10—Peroxyhydrates; Peroxyacids or salts thereof containing carbon
- C01B15/103—Peroxyhydrates; Peroxyacids or salts thereof containing carbon containing only alkali metals as metals
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
Abstract
1469352 Sodium percarbonate PEROXIDECHEMIE GmbH 6 June 1974 [6 June 1973] 25181/74 Heading C1A Sodium percarbonate is prepared by reacting a H 2 O 2 solution which contains 2À95-10 g./litre at Mg<SP>++</SP> ions in the form of a magnesium salt (other than the silicate), with a Na 2 CO 3 solution or suspension containing 2-8 g./litre of sodium hexametaphosphate or a sodium polyacrylate of a temperature of 10-30‹ C.; crystals of the product are precipitated and separated. The product has a spherulitic crystal habit and has a high resistance to abrasion. Optionally, sodium chloride may be added to the reaction system to increase the yield of the precipitated product, while water glass solution may be added in order to stabilize the product towards loss of active oxygen.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19732328803 DE2328803C3 (en) | 1973-06-06 | 1973-06-06 | Process for the production of an abrasion-resistant, coarse-grained sodium percarbonate |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1469352A true GB1469352A (en) | 1977-04-06 |
Family
ID=5883208
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB2518174A Expired GB1469352A (en) | 1973-06-06 | 1974-06-06 | Process for the preparation of sodium percarbonate |
Country Status (7)
Country | Link |
---|---|
BE (1) | BE815864A (en) |
DE (1) | DE2328803C3 (en) |
ES (1) | ES426733A1 (en) |
FR (1) | FR2232508B1 (en) |
GB (1) | GB1469352A (en) |
IT (1) | IT1014827B (en) |
NL (1) | NL7407414A (en) |
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4428914A (en) | 1977-12-23 | 1984-01-31 | Interox | Process for making sodium percarbonate granules |
JPH04227693A (en) * | 1990-04-09 | 1992-08-17 | Unilever Nv | Granular bleaching detergent composition |
US5346680A (en) * | 1992-10-16 | 1994-09-13 | Solvay Interox Gmbh | Sodium percarbonate stabilized by coating |
US5478488A (en) * | 1993-05-08 | 1995-12-26 | Solvay Interox Gmbh | Detergent composition containing alkali metal peroxysalt stabilized with alkali metal sulfate and chloride |
US5560896A (en) * | 1993-08-31 | 1996-10-01 | Degussa Aktiengesellschaft | Method for producing granulated sodium percarbonate |
EP0748764A1 (en) * | 1995-06-08 | 1996-12-18 | AUSIMONT S.p.A. | Process for producing sodium percarbonate in granular form |
EP0796817A2 (en) * | 1996-03-19 | 1997-09-24 | Elf Atochem S.A. | Sodium percarbonate and process for its production |
WO1997035806A1 (en) * | 1996-03-27 | 1997-10-02 | Solvay Interox (Societe Anonyme) | Process for producing a percarbonate |
US6231828B1 (en) * | 1997-03-26 | 2001-05-15 | Solvay Interox Sa | Process for producing sodium percarbonate |
KR100541269B1 (en) * | 1996-03-27 | 2006-04-12 | 솔베이인터록스(소시에떼아노님) | Method of manufacturing percarbonate |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
LU75466A1 (en) * | 1976-07-27 | 1978-02-08 | ||
DE2644148C3 (en) * | 1976-09-30 | 1983-05-11 | Degussa Ag, 6000 Frankfurt | Continuous process for the production of a compact, coarse-grained sodium percarbonate |
DE2644147C3 (en) * | 1976-09-30 | 1983-05-19 | Degussa Ag, 6000 Frankfurt | Process for the production of a compact, coarse-grained sodium percarbonate |
AT356627B (en) * | 1976-10-22 | 1980-05-12 | Treibacher Chemische Werke Ag | METHOD FOR PRODUCING SODIUM PERCARBONATE |
DE2800760C2 (en) * | 1978-01-09 | 1983-01-27 | Degussa Ag, 6000 Frankfurt | Process for the production of sodium percarbonate from a soda solution or suspension |
DE4338401A1 (en) * | 1993-11-10 | 1995-05-11 | Degussa | Process for the production of abrasion-resistant sodium percarbonate with high dissolving speed |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB549841A (en) * | 1941-09-12 | 1942-12-09 | Laporte Ltd B | Manufacture of sodium percarbonate |
BE463513A (en) * | 1943-08-09 |
-
1973
- 1973-06-06 DE DE19732328803 patent/DE2328803C3/en not_active Expired
-
1974
- 1974-05-29 ES ES426733A patent/ES426733A1/en not_active Expired
- 1974-05-31 FR FR7419470A patent/FR2232508B1/fr not_active Expired
- 1974-05-31 NL NL7407414A patent/NL7407414A/xx not_active Application Discontinuation
- 1974-06-04 BE BE145028A patent/BE815864A/en not_active IP Right Cessation
- 1974-06-06 IT IT2367374A patent/IT1014827B/en active
- 1974-06-06 GB GB2518174A patent/GB1469352A/en not_active Expired
Cited By (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4428914A (en) | 1977-12-23 | 1984-01-31 | Interox | Process for making sodium percarbonate granules |
JPH04227693A (en) * | 1990-04-09 | 1992-08-17 | Unilever Nv | Granular bleaching detergent composition |
US5346680A (en) * | 1992-10-16 | 1994-09-13 | Solvay Interox Gmbh | Sodium percarbonate stabilized by coating |
US5478488A (en) * | 1993-05-08 | 1995-12-26 | Solvay Interox Gmbh | Detergent composition containing alkali metal peroxysalt stabilized with alkali metal sulfate and chloride |
US5560896A (en) * | 1993-08-31 | 1996-10-01 | Degussa Aktiengesellschaft | Method for producing granulated sodium percarbonate |
EP0748764A1 (en) * | 1995-06-08 | 1996-12-18 | AUSIMONT S.p.A. | Process for producing sodium percarbonate in granular form |
US6340452B1 (en) | 1996-03-19 | 2002-01-22 | Solvay | Sodium percarbonate and process for producing it |
EP0796817A2 (en) * | 1996-03-19 | 1997-09-24 | Elf Atochem S.A. | Sodium percarbonate and process for its production |
EP0796817A3 (en) * | 1996-03-19 | 1997-10-01 | Elf Atochem S.A. | Sodium percarbonate and process for its production |
AU714881B2 (en) * | 1996-03-19 | 2000-01-13 | Solvay (Societe Anonyme) | Novel sodium percarbonate and process for producing it |
KR100244785B1 (en) * | 1996-03-19 | 2000-02-15 | 엘프 아토켐 소시에떼아노님 | Novel sodium percarbonate and process for producing it |
CN1055448C (en) * | 1996-03-19 | 2000-08-16 | 索尔维公司 | Novel sodium percarbonate and process for producing it |
WO1997035806A1 (en) * | 1996-03-27 | 1997-10-02 | Solvay Interox (Societe Anonyme) | Process for producing a percarbonate |
AU733834B2 (en) * | 1996-03-27 | 2001-05-24 | Solvay Interox (Societe Anonyme) | Process for producing a percarbonate |
US6482385B2 (en) * | 1996-03-27 | 2002-11-19 | Solvay Interox (Societe Anonyme) | Sodium percarbonate and process for producing sodium percarbonate |
KR100541269B1 (en) * | 1996-03-27 | 2006-04-12 | 솔베이인터록스(소시에떼아노님) | Method of manufacturing percarbonate |
US6231828B1 (en) * | 1997-03-26 | 2001-05-15 | Solvay Interox Sa | Process for producing sodium percarbonate |
Also Published As
Publication number | Publication date |
---|---|
FR2232508B1 (en) | 1980-04-11 |
DE2328803C3 (en) | 1982-11-25 |
DE2328803B2 (en) | 1978-06-22 |
FR2232508A1 (en) | 1975-01-03 |
BE815864A (en) | 1974-12-04 |
ES426733A1 (en) | 1976-07-01 |
IT1014827B (en) | 1977-04-30 |
NL7407414A (en) | 1974-12-10 |
DE2328803A1 (en) | 1975-01-09 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
429A | Application made for amendment of specification (sect. 29/1949) | ||
429H | Application (made) for amendment of specification now open to opposition (sect. 29/1949) | ||
429D | Case decided by the comptroller ** specification amended (sect. 29/1949) | ||
SP | Amendment (slips) printed | ||
PCNP | Patent ceased through non-payment of renewal fee |
Effective date: 19930606 |