GB1453296A - Process for flameproofing organic fibre material and a preparatio for use therein - Google Patents
Process for flameproofing organic fibre material and a preparatio for use thereinInfo
- Publication number
- GB1453296A GB1453296A GB5345573A GB5345573A GB1453296A GB 1453296 A GB1453296 A GB 1453296A GB 5345573 A GB5345573 A GB 5345573A GB 5345573 A GB5345573 A GB 5345573A GB 1453296 A GB1453296 A GB 1453296A
- Authority
- GB
- United Kingdom
- Prior art keywords
- gpl
- urea
- optionally
- dicyandiamide
- thp
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K21/00—Fireproofing materials
- C09K21/06—Organic materials
- C09K21/12—Organic materials containing phosphorus
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/282—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
- D06M13/285—Phosphines; Phosphine oxides; Phosphine sulfides; Phosphinic or phosphinous acids or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/402—Amides imides, sulfamic acids
- D06M13/405—Acylated polyalkylene polyamines
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
- D06M13/47—Compounds containing quaternary nitrogen atoms derived from heterocyclic compounds
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
1453296 Flameproofing compositions CIBAGEIGY AG 16 Nov 1973 53455/73 Heading C3R [Also in Division D1] A flameproofing composition for organic fibres comprises (1) a tetramethylol phosphonium (THP) compound or a self-condensate thereof or a condensate thereof with a reactive nitrogen compound, (2) a soft-handle agent Q-A-D, wherein A is a C 2-3 alkylene radical, Q is R-CO-NH-A-NX- or and D is Q or is H, -OH, -NH 2 , -CO-NHR or -NH-CO-R, R being a C 9-23 alkyl or alkenyl radical, which may be quaternized with an alkyl halide of dialkyl sulphate having C 1-2 alkyl radicals or C 1-4 halocarboxylic acid ester of a C 1-22 alkanol or of an ether alcohol of up to 60 C atoms, (3) a watersoluble amino-1 : 3 : 5-triazine having 2-4 methylol groups, (4) optionally, an optionally methylolated, optionally etherified, cyanamide, urea, guanidine, dicyandiamide, cyanourea, biuret or guanylurea, and (5) optionally, an amine of molecular weight below 100. The compounds (2) may be prepared by heating a fatty acid with a polyalkylene polyamine in 1 : 1 molar ratio in a solvent, e.g. xylene or toluene, and eliminating water. Preferably the aqueous composition contains 200-750 gpl of (1), 3-20 gpl of (2), 20-200 gpl of (3), up to 120 gpl of (4) and up to 100 gpl of (5); other customary additives, listed, may be present. In Preparations 1-11 0À95-1À1 mols of water per mol are eliminated from THP chloride, the product optionally being etherified with methanol or dibromopropanol, and ca. 0À65 mols from THP hydroxide or bromide; in Preparations 12-15 minor amounts of urea, cyanamide, dicyandiamide or guanidine are condensed with the selfcondensates so obtained; in Preparations 16-63 THP chloride (or bromide or hydroxide) is cocondensed with 0À2-1 molar proportion of cyanamide, dicyandiamide, urea, ethyleneurea, propyleneurea, acetylenediurea, dihydroxyethyleneurea, dodecylamine, ethylene diamine, dimethylaminopropylamine, aminoethoxyethanol, ethanolamine, aniline, diethylene triamine, N aminopropylmorpholine, stearylamine, thiourea, biuret, guanidine HCl, guanylurea phosphate, dimethylol guanidine carbonate, the compounds oxalic diamide, hydroxyethyl carbamate, dimethylol methyl carbamate, methyl carbamate, nitrilo - tris - propionamide, melamine, diethylphosphono-ethylguanamine, acetoguanamine, trimethylolmelamine, triglycidyl isocyanurate, or the mono- or di-methylol derivatives of dicyandiamide, urea, thiourea and biuret. In the examples 1 : 1 or 2 : 1 polyestercotton fabric is treated with baths containing (1) 535-860 gpl of THP chloride or hydroxide, or a condensate of THP chloride alone or with urea, dimethylolurea or guanidine hydrochloride, (2) 30-35 gpl of a variety of the specified soft-handle agents, typically (3) 80-134 gpl of a di- and/or trimethylolmelamine, which may be methylated, or a dimethylol acetoguanamine, optionally with (4) 30-161 gpl of urea, dimethylourea, dimethoxymethylurea, cyanamide, biuret, or dicyandiamide and (5) 26-67 gpl of allylamine, piperidine or a variety of other amines.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB5345573A GB1453296A (en) | 1973-11-16 | 1973-11-16 | Process for flameproofing organic fibre material and a preparatio for use therein |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB5345573A GB1453296A (en) | 1973-11-16 | 1973-11-16 | Process for flameproofing organic fibre material and a preparatio for use therein |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1453296A true GB1453296A (en) | 1976-10-20 |
Family
ID=10467875
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB5345573A Expired GB1453296A (en) | 1973-11-16 | 1973-11-16 | Process for flameproofing organic fibre material and a preparatio for use therein |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB1453296A (en) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2399433A1 (en) * | 1977-08-01 | 1979-03-02 | Ciba Geigy Ag | QUATERNARY AMMONIUM SALTS OF ANTISTATIC PRODUCTS OR TOUCH SOFTENING AGENTS WITH FATTY ACID REMAINS, THEIR PREPARATION PROCESS AND THEIR USE |
GB2244068A (en) * | 1990-04-12 | 1991-11-20 | Albright & Wilson | Flame retardants |
EP0709518A1 (en) * | 1994-10-25 | 1996-05-01 | Albright & Wilson Limited | Flame retardant and fabric softening treatment of textile materials |
EP2402416A1 (en) * | 2010-06-30 | 2012-01-04 | Huntsman Textile Effects (Germany) GmbH | Flame retardant compound for cotton wool items |
EP2524993A1 (en) * | 2011-05-17 | 2012-11-21 | Ctf 2000 N.V. | Textile fireproofing method |
CN110952320A (en) * | 2019-12-10 | 2020-04-03 | 山东芦氏阻燃纤维科技有限公司 | Continuous processing method of flame-retardant cellulose short fiber and flame-retardant cellulose short fiber obtained by same |
-
1973
- 1973-11-16 GB GB5345573A patent/GB1453296A/en not_active Expired
Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2399433A1 (en) * | 1977-08-01 | 1979-03-02 | Ciba Geigy Ag | QUATERNARY AMMONIUM SALTS OF ANTISTATIC PRODUCTS OR TOUCH SOFTENING AGENTS WITH FATTY ACID REMAINS, THEIR PREPARATION PROCESS AND THEIR USE |
GB2244068A (en) * | 1990-04-12 | 1991-11-20 | Albright & Wilson | Flame retardants |
GB2244068B (en) * | 1990-04-12 | 1994-01-19 | Albright & Wilson | Treatment of fabrics |
EP0709518A1 (en) * | 1994-10-25 | 1996-05-01 | Albright & Wilson Limited | Flame retardant and fabric softening treatment of textile materials |
AU686451B2 (en) * | 1994-10-25 | 1998-02-05 | Albright & Wilson Uk Limited | Flame retardant and fabric softening treatment of textile materials |
GB2294479B (en) * | 1994-10-25 | 1998-07-15 | Albright & Wilson Uk Ltd | Flame-retardant and fabric-softening treatment of textile materials |
EP2402416A1 (en) * | 2010-06-30 | 2012-01-04 | Huntsman Textile Effects (Germany) GmbH | Flame retardant compound for cotton wool items |
WO2012000756A1 (en) * | 2010-06-30 | 2012-01-05 | Huntsman Textile Effects (Germany) Gmbh | Flame retardant composition for cotton articles |
US8585813B2 (en) | 2010-06-30 | 2013-11-19 | Huntsman Textile Effects (Germany) Gmbh | Flame retardant composition for cotton articles |
EP2524993A1 (en) * | 2011-05-17 | 2012-11-21 | Ctf 2000 N.V. | Textile fireproofing method |
WO2012156190A1 (en) | 2011-05-17 | 2012-11-22 | Ctf 2000 Nv | Method for fireproofing textiles |
US9074316B2 (en) | 2011-05-17 | 2015-07-07 | Ctf 2000 Nv | Method for fireproofing textiles |
CN110952320A (en) * | 2019-12-10 | 2020-04-03 | 山东芦氏阻燃纤维科技有限公司 | Continuous processing method of flame-retardant cellulose short fiber and flame-retardant cellulose short fiber obtained by same |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PCNP | Patent ceased through non-payment of renewal fee |