GB1443393A - Method of producing spherical active alumina pellets of high mechanical strength - Google Patents
Method of producing spherical active alumina pellets of high mechanical strengthInfo
- Publication number
- GB1443393A GB1443393A GB779274A GB779274A GB1443393A GB 1443393 A GB1443393 A GB 1443393A GB 779274 A GB779274 A GB 779274A GB 779274 A GB779274 A GB 779274A GB 1443393 A GB1443393 A GB 1443393A
- Authority
- GB
- United Kingdom
- Prior art keywords
- mixture
- solution
- carbon black
- mechanical strength
- high mechanical
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 title abstract 5
- 239000008188 pellet Substances 0.000 title abstract 3
- 239000000203 mixture Substances 0.000 abstract 4
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 abstract 3
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 abstract 3
- 235000011114 ammonium hydroxide Nutrition 0.000 abstract 3
- 239000006229 carbon black Substances 0.000 abstract 3
- 239000003054 catalyst Substances 0.000 abstract 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- 239000008187 granular material Substances 0.000 abstract 2
- 239000012266 salt solution Substances 0.000 abstract 2
- 241000872198 Serjania polyphylla Species 0.000 abstract 1
- VXAUWWUXCIMFIM-UHFFFAOYSA-M aluminum;oxygen(2-);hydroxide Chemical compound [OH-].[O-2].[Al+3] VXAUWWUXCIMFIM-UHFFFAOYSA-M 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 238000001354 calcination Methods 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 230000003179 granulation Effects 0.000 abstract 1
- 238000005469 granulation Methods 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/06—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
- B01J20/08—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04 comprising aluminium oxide or hydroxide; comprising bauxite
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/86—Catalytic processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
- B01J35/51—Spheres
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Environmental & Geological Engineering (AREA)
- Analytical Chemistry (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Biomedical Technology (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Catalysts (AREA)
- Exhaust Gas Treatment By Means Of Catalyst (AREA)
Abstract
1443393 Exhaust gas purification catalysts KALI-CHEMIE AG 20 Feb 1974 7792/74 Heading B1E [Also in Division C1] Spherical pellets of active alumina having high mechanical strength suitable as supports for catalysts are made by granulating a mixture of hydrated alumina and carbon black with the addition of a solution of ammonia, drying the granules, heat-treating the granules at 250 to 500C and finally calcining at a temperature of 1000 to 1200C. The hydrated alumina is [preferably a pseudo-boehmite and it may optionally be dehydrated and ground before granulation,. The mixture preferably contains 0.01 to 1%, especially 0.05 to 0.5%, carbon black. The ammonia solution preferably has a concentration of 0.1 to 2% and is suitably introduced in an amount of 30 to 60% by weight based on the weight of the mixture. In a preferred embodiment the alumina/carbon black mixture is mixed with 25 to 45% of the ammonia solution to form a mass which is then granulated with the addition of the remainder of the ammonia solution. In Example 3, pellets are soaked with a Mn salt solution, dried, calcined at 1000C for 1 hour, soaked with a Pd salt solution, dried and calcined at 800C for 1 hour. The catalyst contained 2% Mn 2 O 3 and 0.2% Pd.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2308890A DE2308890C2 (en) | 1973-02-23 | 1973-02-23 | Process for the production of spherical particles from active alumina with high mechanical strength |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1443393A true GB1443393A (en) | 1976-07-21 |
Family
ID=5872791
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB779274A Expired GB1443393A (en) | 1973-02-23 | 1974-02-20 | Method of producing spherical active alumina pellets of high mechanical strength |
Country Status (3)
| Country | Link |
|---|---|
| FR (1) | FR2219115A1 (en) |
| GB (1) | GB1443393A (en) |
| IT (1) | IT1007455B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2473468C1 (en) * | 2011-05-31 | 2013-01-27 | Елена Арсеньевна Петрова | Method of obtaining active aluminium oxide |
| US10639616B2 (en) | 2014-09-12 | 2020-05-05 | Clariant International Ltd | Extruded Cu—Al—Mn hydrogenation catalyst |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2534828B1 (en) * | 1982-10-21 | 1986-12-26 | Pro Catalyse | ALUMINA, SILICA OR SILICA-ALUMINA-BASED CATALYSTS, THEIR PREPARATION AND THEIR USE IN THE FIELD OF HYDROPROCESSING OF HYDROCARBON OILS |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1438497A (en) * | 1965-03-31 | 1966-05-13 | Pechiney Saint Gobain | Alumina agglomerates |
| FR1597102A (en) * | 1968-02-26 | 1970-06-22 |
-
1974
- 1974-02-20 GB GB779274A patent/GB1443393A/en not_active Expired
- 1974-02-22 FR FR7406222A patent/FR2219115A1/en active Granted
- 1974-04-08 IT IT20715/74A patent/IT1007455B/en active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2473468C1 (en) * | 2011-05-31 | 2013-01-27 | Елена Арсеньевна Петрова | Method of obtaining active aluminium oxide |
| US10639616B2 (en) | 2014-09-12 | 2020-05-05 | Clariant International Ltd | Extruded Cu—Al—Mn hydrogenation catalyst |
Also Published As
| Publication number | Publication date |
|---|---|
| FR2219115B1 (en) | 1978-12-01 |
| FR2219115A1 (en) | 1974-09-20 |
| IT1007455B (en) | 1976-10-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 416 | Proceeding under section 16 patents act 1949 | ||
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |