GB1425669A - Electrolytic process for the preparation of dimethyl sebacate - Google Patents
Electrolytic process for the preparation of dimethyl sebacateInfo
- Publication number
- GB1425669A GB1425669A GB313374A GB313374A GB1425669A GB 1425669 A GB1425669 A GB 1425669A GB 313374 A GB313374 A GB 313374A GB 313374 A GB313374 A GB 313374A GB 1425669 A GB1425669 A GB 1425669A
- Authority
- GB
- United Kingdom
- Prior art keywords
- dimethyl sebacate
- sebacate
- preparation
- jan
- salt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- ALOUNLDAKADEEB-UHFFFAOYSA-N dimethyl sebacate Chemical compound COC(=O)CCCCCCCCC(=O)OC ALOUNLDAKADEEB-UHFFFAOYSA-N 0.000 title abstract 8
- 229940014772 dimethyl sebacate Drugs 0.000 title abstract 4
- 238000002360 preparation method Methods 0.000 title abstract 2
- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 abstract 5
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 abstract 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 abstract 2
- 150000002148 esters Chemical class 0.000 abstract 2
- 101100188552 Arabidopsis thaliana OCT3 gene Proteins 0.000 abstract 1
- 229920006310 Asahi-Kasei Polymers 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000009833 condensation Methods 0.000 abstract 1
- 230000005494 condensation Effects 0.000 abstract 1
- 230000003301 hydrolyzing effect Effects 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- UOBSVARXACCLLH-UHFFFAOYSA-N monomethyl adipate Chemical compound COC(=O)CCCCC(O)=O UOBSVARXACCLLH-UHFFFAOYSA-N 0.000 abstract 1
- 238000006386 neutralization reaction Methods 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B3/00—Electrolytic production of organic compounds
- C25B3/20—Processes
- C25B3/29—Coupling reactions
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1188373A JPS5323816B2 (enrdf_load_stackoverflow) | 1973-01-31 | 1973-01-31 | |
| JP48034863A JPS49117418A (enrdf_load_stackoverflow) | 1973-03-26 | 1973-03-26 | |
| JP11121873A JPS563434B2 (enrdf_load_stackoverflow) | 1973-10-03 | 1973-10-03 | |
| JP48141604A JPS5089317A (enrdf_load_stackoverflow) | 1973-12-17 | 1973-12-17 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1425669A true GB1425669A (en) | 1976-02-18 |
Family
ID=27455697
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB313374A Expired GB1425669A (en) | 1973-01-31 | 1974-01-23 | Electrolytic process for the preparation of dimethyl sebacate |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3896011A (enrdf_load_stackoverflow) |
| CA (1) | CA1057232A (enrdf_load_stackoverflow) |
| CH (1) | CH598176A5 (enrdf_load_stackoverflow) |
| DE (1) | DE2404560C3 (enrdf_load_stackoverflow) |
| FR (1) | FR2216261B1 (enrdf_load_stackoverflow) |
| GB (1) | GB1425669A (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113416969A (zh) * | 2021-06-18 | 2021-09-21 | 万华化学集团股份有限公司 | 一种癸二酸二甲酯电化学合成方法 |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4124453A (en) * | 1975-09-29 | 1978-11-07 | National Research Development Corporation | Electrochemical processes |
| GB2001312B (en) * | 1977-07-20 | 1982-03-10 | Asahi Chemical Ind | Process for producing sebacic acid |
| US4237317A (en) * | 1977-07-20 | 1980-12-02 | Asahi Kasei Kogyo Kabushiki Kaisha | Process for producing sebacic acid |
| WO1983002463A1 (en) * | 1982-01-12 | 1983-07-21 | Yamataka, Kazunori | Process for producing higher dibasic acid dimethyl ester |
| US5290404A (en) * | 1990-10-31 | 1994-03-01 | Reilly Industries, Inc. | Electro-synthesis of alcohols and carboxylic acids from corresponding metal salts |
| US8647492B2 (en) | 2009-07-23 | 2014-02-11 | Ceramatec, Inc. | Method of producing coupled radical products from biomass |
| US9957622B2 (en) * | 2009-07-23 | 2018-05-01 | Field Upgrading Limited | Device and method of obtaining diols and other chemicals using decarboxylation |
| US9493882B2 (en) | 2010-07-21 | 2016-11-15 | Ceramatec, Inc. | Custom ionic liquid electrolytes for electrolytic decarboxylation |
| KR101915824B1 (ko) | 2011-01-25 | 2018-11-06 | 필드 업그레이딩 리미티드 | 바이오매스 유래 화학물질로부터의 연료의 제조 |
| CN107326051B (zh) | 2017-08-02 | 2021-06-08 | 上海凯赛生物技术股份有限公司 | 一种微生物发酵法生产的癸二酸及其制备方法 |
| CN111850596B (zh) * | 2020-07-13 | 2021-04-20 | 万华化学(四川)有限公司 | 一种电化学合成癸二酸酯类化合物的连续生产方法 |
| CN116288424A (zh) * | 2023-01-03 | 2023-06-23 | 万华化学集团股份有限公司 | 一种电化学合成癸二酸二甲酯反应液的处理方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2439425A (en) * | 1946-04-01 | 1948-04-13 | Du Pont | Process for preparing dialkyl esters of dicarboxylic acids |
| US3589990A (en) * | 1968-02-29 | 1971-06-29 | Vnii Pi Monomerov | Process for the production of sebacic acid |
| DE2014985C3 (de) * | 1970-03-28 | 1978-06-08 | Basf Ag, 6700 Ludwigshafen | Verfahren zur elektrolytischen Kondensation von Carbonsäuren |
| DE2039991A1 (de) * | 1970-08-12 | 1972-02-17 | Basf Ag | Verfahren zur Herstellung von Sebacinsaeurediestern hoeherer Alkohole |
-
1974
- 1974-01-23 GB GB313374A patent/GB1425669A/en not_active Expired
- 1974-01-24 US US436275A patent/US3896011A/en not_active Expired - Lifetime
- 1974-01-29 CA CA191,139A patent/CA1057232A/en not_active Expired
- 1974-01-30 FR FR7403064A patent/FR2216261B1/fr not_active Expired
- 1974-01-31 CH CH135574A patent/CH598176A5/xx not_active IP Right Cessation
- 1974-01-31 DE DE2404560A patent/DE2404560C3/de not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113416969A (zh) * | 2021-06-18 | 2021-09-21 | 万华化学集团股份有限公司 | 一种癸二酸二甲酯电化学合成方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2404560A1 (de) | 1974-08-01 |
| FR2216261B1 (enrdf_load_stackoverflow) | 1978-07-13 |
| CA1057232A (en) | 1979-06-26 |
| DE2404560B2 (de) | 1981-07-23 |
| US3896011A (en) | 1975-07-22 |
| DE2404560C3 (de) | 1982-04-29 |
| FR2216261A1 (enrdf_load_stackoverflow) | 1974-08-30 |
| CH598176A5 (enrdf_load_stackoverflow) | 1978-04-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |
Effective date: 19930123 |