GB1412477A - Perfluoroalkylamindalkanols process for their manufacture and their use - Google Patents

Perfluoroalkylamindalkanols process for their manufacture and their use

Info

Publication number
GB1412477A
GB1412477A GB5469973A GB5469973A GB1412477A GB 1412477 A GB1412477 A GB 1412477A GB 5469973 A GB5469973 A GB 5469973A GB 5469973 A GB5469973 A GB 5469973A GB 1412477 A GB1412477 A GB 1412477A
Authority
GB
United Kingdom
Prior art keywords
perfluorooctyl
amine
general formula
radical
perfluoroalkylaminoalkanols
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB5469973A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Novartis AG
Original Assignee
Ciba Geigy AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ciba Geigy AG filed Critical Ciba Geigy AG
Publication of GB1412477A publication Critical patent/GB1412477A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/08—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms
    • C07D295/084—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms with the ring nitrogen atoms and the oxygen or sulfur atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings
    • C07D295/088—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms with the ring nitrogen atoms and the oxygen or sulfur atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings to an acyclic saturated chain
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D203/00—Heterocyclic compounds containing three-membered rings with one nitrogen atom as the only ring hetero atom
    • C07D203/04—Heterocyclic compounds containing three-membered rings with one nitrogen atom as the only ring hetero atom not condensed with other rings
    • C07D203/06—Heterocyclic compounds containing three-membered rings with one nitrogen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members
    • C07D203/08—Heterocyclic compounds containing three-membered rings with one nitrogen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to the ring nitrogen atom
    • C07D203/10—Radicals substituted by singly bound oxygen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Materials Applied To Surfaces To Minimize Adherence Of Mist Or Water (AREA)

Abstract

1412477 Perfluoroalkylaminoalkanols CIBAGEIGY AG 26 Nov 1973 [28 Sept 1972] 54699/73 Heading C2C Perfluoroalkylaminoalkanols of general formula where R f is a C 4-14 perfluorinated hydrocarbon radical; R is H or CH 3 ; R 1 and R 2 are each H, C 1-18 alkyl, C 5-6 cycloalkyl, C 1-10 hydroxyalkyl or alkoxyalkyl or the radical or R 1 and R 2 , together with the N-atom to which they are attached, form a heterocyclic ring of 3-6 members, are prepared by reacting an epoxide of general formula or a chlorohydrin of general formula with an amine R 1 R 2 NH, preferably at 20- 150‹ C. in an inert solvent in the presence of an alkali. Preferred compounds have R f as C 6 F 13 to C 12 F 25 radical, and R 1 and R 2 representing H, C 1-6 alkyl, C 2-6 hydroxyalkyl or together forming an aziridine, piperidine, morpholine or piperazine ring. Amongst the examples the following compounds are prepared:-1-perfluorooctyl - 2 - piperidinoethanol, 1 - perfluorooctyl - 2 - butylaminoethanol, bis - (perfluorooctyl - diethanol) amine and tris - (perfluorooctyl-triethanol)amine.
GB5469973A 1972-11-28 1973-11-26 Perfluoroalkylamindalkanols process for their manufacture and their use Expired GB1412477A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CH1729472A CH576936A5 (en) 1972-11-28 1972-11-28

Publications (1)

Publication Number Publication Date
GB1412477A true GB1412477A (en) 1975-11-05

Family

ID=4424294

Family Applications (1)

Application Number Title Priority Date Filing Date
GB5469973A Expired GB1412477A (en) 1972-11-28 1973-11-26 Perfluoroalkylamindalkanols process for their manufacture and their use

Country Status (8)

Country Link
JP (1) JPS4982612A (en)
BE (1) BE807848A (en)
CA (1) CA1018976A (en)
CH (1) CH576936A5 (en)
DE (1) DE2357780A1 (en)
FR (1) FR2207907B1 (en)
GB (1) GB1412477A (en)
SU (1) SU510993A3 (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7468236B2 (en) * 2005-10-14 2008-12-23 Shin-Etsu Chemical Co., Ltd. Amine compound, chemically amplified resist composition and patterning process
CN102796014A (en) * 2012-09-07 2012-11-28 山东大学 Preparation method of perfluorohexyl-containing tribasic alcohol

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6020425B2 (en) * 1976-06-28 1985-05-22 ダイキン工業株式会社 Polishing composition
EP0002004B1 (en) * 1977-11-07 1982-03-24 Ciba-Geigy Ag Process for the manufacture of fluorinated cationic compounds and their use as surfactants

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2023562A1 (en) * 1968-11-18 1970-08-21 Daikin Ind Ltd

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7468236B2 (en) * 2005-10-14 2008-12-23 Shin-Etsu Chemical Co., Ltd. Amine compound, chemically amplified resist composition and patterning process
CN102796014A (en) * 2012-09-07 2012-11-28 山东大学 Preparation method of perfluorohexyl-containing tribasic alcohol

Also Published As

Publication number Publication date
CH576936A5 (en) 1976-06-30
CA1018976A (en) 1977-10-11
SU510993A3 (en) 1976-04-15
JPS4982612A (en) 1974-08-08
BE807848A (en) 1974-05-27
FR2207907B1 (en) 1978-03-10
FR2207907A1 (en) 1974-06-21
DE2357780A1 (en) 1974-05-30

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Legal Events

Date Code Title Description
PS Patent sealed
PCNP Patent ceased through non-payment of renewal fee