GB1363937A - Nitrosubstituted phenylene diamine compounds and compositions containing them - Google Patents
Nitrosubstituted phenylene diamine compounds and compositions containing themInfo
- Publication number
- GB1363937A GB1363937A GB5194371A GB5194371A GB1363937A GB 1363937 A GB1363937 A GB 1363937A GB 5194371 A GB5194371 A GB 5194371A GB 5194371 A GB5194371 A GB 5194371A GB 1363937 A GB1363937 A GB 1363937A
- Authority
- GB
- United Kingdom
- Prior art keywords
- reacting
- group
- amino
- acid
- nitrosubstituted
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- -1 Nitrosubstituted phenylene Chemical group 0.000 title abstract 2
- 150000001875 compounds Chemical class 0.000 title 1
- 239000000203 mixture Substances 0.000 title 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 3
- NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical compound CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 abstract 2
- DPLJNTWBXCKJOL-UHFFFAOYSA-N 3-bromo-4,5-diethoxybenzonitrile Chemical compound CCOC1=CC(C#N)=CC(Br)=C1OCC DPLJNTWBXCKJOL-UHFFFAOYSA-N 0.000 abstract 2
- ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 2
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 abstract 2
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 2
- QJDSLDWVMCWWCO-UHFFFAOYSA-N 6-(1,3-dioxoisoindol-2-yl)hexanoic acid Chemical compound C1=CC=C2C(=O)N(CCCCCC(=O)O)C(=O)C2=C1 QJDSLDWVMCWWCO-UHFFFAOYSA-N 0.000 abstract 1
- VYZAHLCBVHPDDF-UHFFFAOYSA-N Dinitrochlorobenzene Chemical compound [O-][N+](=O)C1=CC=C(Cl)C([N+]([O-])=O)=C1 VYZAHLCBVHPDDF-UHFFFAOYSA-N 0.000 abstract 1
- LGRFSURHDFAFJT-UHFFFAOYSA-N Phthalic anhydride Natural products C1=CC=C2C(=O)OC(=O)C2=C1 LGRFSURHDFAFJT-UHFFFAOYSA-N 0.000 abstract 1
- 125000003277 amino group Chemical group 0.000 abstract 1
- JHIWVOJDXOSYLW-UHFFFAOYSA-N butyl 2,2-difluorocyclopropane-1-carboxylate Chemical compound CCCCOC(=O)C1CC1(F)F JHIWVOJDXOSYLW-UHFFFAOYSA-N 0.000 abstract 1
- QKIUAMUSENSFQQ-UHFFFAOYSA-N dimethylazanide Chemical compound C[N-]C QKIUAMUSENSFQQ-UHFFFAOYSA-N 0.000 abstract 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- IENQDRALNOEFHD-UHFFFAOYSA-N methyl 3-(2,4-dinitroanilino)propanoate Chemical compound COC(=O)CCNC1=CC=C([N+]([O-])=O)C=C1[N+]([O-])=O IENQDRALNOEFHD-UHFFFAOYSA-N 0.000 abstract 1
- UHZYTMXLRWXGPK-UHFFFAOYSA-N phosphorus pentachloride Chemical compound ClP(Cl)(Cl)(Cl)Cl UHZYTMXLRWXGPK-UHFFFAOYSA-N 0.000 abstract 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 abstract 1
- 238000010992 reflux Methods 0.000 abstract 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/418—Amines containing nitro groups
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/06—Preparations for styling the hair, e.g. by temporary shaping or colouring
- A61Q5/065—Preparations for temporary colouring the hair, e.g. direct dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B51/00—Nitro or nitroso dyes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S8/00—Bleaching and dyeing; fluid treatment and chemical modification of textiles and fibers
- Y10S8/916—Natural fiber dyeing
- Y10S8/917—Wool or silk
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S8/00—Bleaching and dyeing; fluid treatment and chemical modification of textiles and fibers
- Y10S8/92—Synthetic fiber dyeing
- Y10S8/924—Polyamide fiber
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Cosmetics (AREA)
Abstract
1363937 Amino compounds GILLETTE CO 9 Nov 1971 [18 Nov 1970] 51943/71 Heading C2C [Also in Divisions C4 and D1] In Example 1, N<SP>1</SP>-[2-(N,N-dimethylcarboxamido)ethyl]-2-nitro-p-phenylenediamine is prepared by (a) reacting #-alanine with methanol and HCl gas to form methyl-3-aminopropionate hydrochloride, (b) reacting methyl-3-aminopropionate hydrochloride with 1-chloro-2,4- dinitro-benzene to form N-(2-carbomethoxyethyl)-2,4-dinitro-aniline, (c) converting the carboxymethoxy group to a dimethylcarboxamido group by reaction with methylamine, and (d) hydrogenating to convert the 4-nitro-group to an amino group. In Example 2, 6-amino-N,N-dimethyl-nhexamide is prepared by (a) reacting 6-amino-nhexanoic acid with phthalic anhydride to form 6-phthalimido-n-hexanoic acid, (b) converting the acid to the acid chloride using phosphorus pentachloride, (c) reacting the acid chloride with dimethylamine to form the dimethyl-amide and then refluxing with hydrazine in ethanol, followed by heating at 50 C. with HCl.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US00090825A US3836326A (en) | 1970-11-18 | 1970-11-18 | Dyeing hair with nitro-substituted phenylene compounds |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1363937A true GB1363937A (en) | 1974-08-21 |
Family
ID=22224501
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB5194371A Expired GB1363937A (en) | 1970-11-18 | 1971-11-09 | Nitrosubstituted phenylene diamine compounds and compositions containing them |
Country Status (3)
| Country | Link |
|---|---|
| US (1) | US3836326A (en) |
| CA (1) | CA1020952A (en) |
| GB (1) | GB1363937A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5171889A (en) * | 1990-10-31 | 1992-12-15 | Clairol Incorporated | Compositions containing nitroaniline dyes having a carbamide substituent group |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040200011A1 (en) * | 2002-12-06 | 2004-10-14 | Luc Nicolas-Morgantini | Composition for the oxidation dyeing of keratin fibers, comprising at least one oxidation dye, at least one fatty alcohol, at least one associative polymer, and at least one C14-C30 alkyl sulphate |
| US9417226B2 (en) * | 2011-06-28 | 2016-08-16 | Mistral Detection Ltd | Reagent, method and kit for the detection of nitro aliphatic compounds |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3121116A (en) * | 1961-03-31 | 1964-02-11 | Dow Chemical Co | Propynyl p-phenylene diamines |
| GB1053369A (en) * | 1963-11-26 | |||
| FR1310072A (en) * | 1964-06-12 | 1963-03-04 | ||
| FR1458155A (en) * | 1965-04-23 | 1966-03-04 | Oreal | New acidic nitrates |
| US3629330A (en) * | 1965-05-24 | 1971-12-21 | Clairol Inc | Components for hair dyeing compositions |
| US3658454A (en) * | 1969-05-16 | 1972-04-25 | American Cyanamid Co | Dyeing keratinaceous material with n-carbamoylethyl amines |
-
1970
- 1970-11-18 US US00090825A patent/US3836326A/en not_active Expired - Lifetime
-
1971
- 1971-11-09 GB GB5194371A patent/GB1363937A/en not_active Expired
- 1971-11-09 CA CA127,266A patent/CA1020952A/en not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5171889A (en) * | 1990-10-31 | 1992-12-15 | Clairol Incorporated | Compositions containing nitroaniline dyes having a carbamide substituent group |
Also Published As
| Publication number | Publication date |
|---|---|
| CA1020952A (en) | 1977-11-15 |
| US3836326A (en) | 1974-09-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PLNP | Patent lapsed through nonpayment of renewal fees |