GB1343969A - Process for preparing, 2,4,4, tetrachlorobutanol - Google Patents
Process for preparing, 2,4,4, tetrachlorobutanolInfo
- Publication number
- GB1343969A GB1343969A GB5709271A GB5709271A GB1343969A GB 1343969 A GB1343969 A GB 1343969A GB 5709271 A GB5709271 A GB 5709271A GB 5709271 A GB5709271 A GB 5709271A GB 1343969 A GB1343969 A GB 1343969A
- Authority
- GB
- United Kingdom
- Prior art keywords
- butyl
- tetrachlorobutanol
- dec
- catalyst
- preparing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- PNDXSZVXDBLZCY-UHFFFAOYSA-N 1,1,2,2-tetrachlorobutan-1-ol Chemical compound CCC(Cl)(Cl)C(O)(Cl)Cl PNDXSZVXDBLZCY-UHFFFAOYSA-N 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title 1
- OZAIFHULBGXAKX-UHFFFAOYSA-N 2-(2-cyanopropan-2-yldiazenyl)-2-methylpropanenitrile Chemical compound N#CC(C)(C)N=NC(C)(C)C#N OZAIFHULBGXAKX-UHFFFAOYSA-N 0.000 abstract 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 abstract 2
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 abstract 2
- PHPDBVLDVIRSHU-UHFFFAOYSA-N 2,4,4,4-tetrachlorobutan-1-ol Chemical compound OCC(Cl)CC(Cl)(Cl)Cl PHPDBVLDVIRSHU-UHFFFAOYSA-N 0.000 abstract 1
- MRBKEAMVRSLQPH-UHFFFAOYSA-N 3-tert-butyl-4-hydroxyanisole Chemical compound COC1=CC=C(O)C(C(C)(C)C)=C1 MRBKEAMVRSLQPH-UHFFFAOYSA-N 0.000 abstract 1
- NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 abstract 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 abstract 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 1
- 229910021578 Iron(III) chloride Inorganic materials 0.000 abstract 1
- 239000003963 antioxidant agent Substances 0.000 abstract 1
- 230000003078 antioxidant effect Effects 0.000 abstract 1
- 235000006708 antioxidants Nutrition 0.000 abstract 1
- 229910000019 calcium carbonate Inorganic materials 0.000 abstract 1
- 229960002089 ferrous chloride Drugs 0.000 abstract 1
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
- B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
- B01J31/0235—Nitrogen containing compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/26—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24
- B01J31/28—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24 of the platinum group metals, iron group metals or copper
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/26—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24
- B01J31/28—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24 of the platinum group metals, iron group metals or copper
- B01J31/30—Halides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
- B01J2231/30—Addition reactions at carbon centres, i.e. to either C-C or C-X multiple bonds
- B01J2231/32—Addition reactions to C=C or C-C triple bonds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/74—Iron group metals
- B01J23/745—Iron
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/06—Halogens; Compounds thereof
- B01J27/08—Halides
- B01J27/10—Chlorides
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10035170A | 1970-12-21 | 1970-12-21 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1343969A true GB1343969A (en) | 1974-01-16 |
Family
ID=22279312
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB5709271A Expired GB1343969A (en) | 1970-12-21 | 1971-12-08 | Process for preparing, 2,4,4, tetrachlorobutanol |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3723543A (enExample) |
| CA (1) | CA948216A (enExample) |
| DE (1) | DE2163273A1 (enExample) |
| FR (1) | FR2119403A5 (enExample) |
| GB (1) | GB1343969A (enExample) |
| NL (1) | NL7117444A (enExample) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3969423A (en) * | 1973-06-21 | 1976-07-13 | Olin Corporation | Continuous preparation of 2,4,4,4-tetrachlorobutanol |
| DE3148450A1 (de) * | 1981-12-08 | 1983-06-16 | Hoechst Ag, 6230 Frankfurt | Katalysatorgemisch und verfahren zur herstellung von 1,2-dichlorethan |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3309393A (en) * | 1962-01-25 | 1967-03-14 | Shionogi & Co | Telomerization of acrylonitrile |
| DE1207366B (de) * | 1963-05-02 | 1965-12-23 | Basf Ag | Verfahren zur Herstellung von 2, 4, 4, 4-Tetrachlorbutanol-(1) |
| US3399241A (en) * | 1964-02-26 | 1968-08-27 | Olin Mathieson | Process for preparing 2, 4, 4, 4-tetrachlorobutanol from allyl alcohol and ccl4 in the presence of powdered iron catalyst |
| US3399217A (en) * | 1964-03-04 | 1968-08-27 | Olin Mathieson | Catalyst system for reaction of an allyl alcohol and carbon tetrachloride to produce2, 4, 4, 4-tetrachlorobutanol |
-
1970
- 1970-12-21 US US00100351A patent/US3723543A/en not_active Expired - Lifetime
-
1971
- 1971-11-16 CA CA127,778A patent/CA948216A/en not_active Expired
- 1971-12-08 GB GB5709271A patent/GB1343969A/en not_active Expired
- 1971-12-13 FR FR7144744A patent/FR2119403A5/fr not_active Expired
- 1971-12-20 NL NL7117444A patent/NL7117444A/xx unknown
- 1971-12-20 DE DE19712163273 patent/DE2163273A1/de active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| NL7117444A (enExample) | 1972-06-23 |
| DE2163273A1 (de) | 1972-07-13 |
| US3723543A (en) | 1973-03-27 |
| CA948216A (en) | 1974-05-28 |
| FR2119403A5 (enExample) | 1972-08-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PLNP | Patent lapsed through nonpayment of renewal fees |