GB1277282A - A process for the purification of 4,4-dihydroxy-diphenyl-2,2-propane or the phenol adduct thereof - Google Patents

A process for the purification of 4,4-dihydroxy-diphenyl-2,2-propane or the phenol adduct thereof

Info

Publication number
GB1277282A
GB1277282A GB4062669A GB4062669A GB1277282A GB 1277282 A GB1277282 A GB 1277282A GB 4062669 A GB4062669 A GB 4062669A GB 4062669 A GB4062669 A GB 4062669A GB 1277282 A GB1277282 A GB 1277282A
Authority
GB
United Kingdom
Prior art keywords
propane
dihydroxy
diphenyl
phenol
adduct
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB4062669A
Inventor
Hans Helmut Schwarz
Gunther Klotz
George Spott
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer AG
Original Assignee
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer AG filed Critical Bayer AG
Publication of GB1277282A publication Critical patent/GB1277282A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C07C37/84Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by crystallisation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1277282 Purification of 4,4-dihydroxy-diphenyl - 2,2 - propane or the phenol adduct thereof FARBENFABRIKEN BAYER AG 14 Aug 1969 [17 Sept 1968] 40626/69 Heading C2C A process for the purification of 4,41-dihydroxydiphenyl - 2,2 - propane or the phenol adduct thereof wherein a mixed melt of 4,4<SP>1</SP>- dihydroxy - diphenyl - 2,2 - propane, phenol and impurities is cooled and the resulting crystal-slurry is separated from the mother liquor and washed with a melt of pure 4,4<SP>1</SP>- dihydroxy - diphenyl - 2,2 - propane or of pure phenol-adduct thereof whose temperature is up to 25‹ C. above its solidification point, and purified crystals thus obtained are fused and run off, the temperature of the crystal-slurry being adjusted to from 90‹ to 120‹ C. for the preparation of 4,4<SP>1</SP>-dihydroxy-diphenyl-2,2-propane and to from 55‹ to 88‹ C. for the preparation of the phenol-adduct, whilst the run-off temperature of the mother liquor is adjusted to from 100‹ to 130‹ C. for the preparation of 4,4<SP>1</SP>- dihydroxy-diphenyl-2,2-propane and from 70‹ to 90‹ C. for the preparation of phenol adduct.
GB4062669A 1968-09-17 1969-08-14 A process for the purification of 4,4-dihydroxy-diphenyl-2,2-propane or the phenol adduct thereof Expired GB1277282A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19681793431 DE1793431A1 (en) 1968-09-17 1968-09-17 Process for the purification of 4,4'-dihydroxydiphenylpropane- (2,2) or the phenol adduct of these compounds

Publications (1)

Publication Number Publication Date
GB1277282A true GB1277282A (en) 1972-06-07

Family

ID=5707702

Family Applications (1)

Application Number Title Priority Date Filing Date
GB4062669A Expired GB1277282A (en) 1968-09-17 1969-08-14 A process for the purification of 4,4-dihydroxy-diphenyl-2,2-propane or the phenol adduct thereof

Country Status (6)

Country Link
JP (1) JPS5011909B1 (en)
BE (1) BE738962A (en)
DE (1) DE1793431A1 (en)
FR (1) FR2018276A1 (en)
GB (1) GB1277282A (en)
NL (1) NL6913707A (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT971366B (en) * 1972-11-30 1974-04-30 Sir Soc Italiana Resine Spa PROCEDURE FOR THE PRODUCTION OF 2 2 4 4 DIIDROXIDIPHENYL PROPANE
CN1050828C (en) * 1993-02-16 2000-03-29 中国石油化工总公司 Method of dephenolization for preparing high quality polycarbonic ester grade bisphenol A
CN1080914A (en) * 1993-02-17 1994-01-19 中国石油化工总公司 A kind of 2, the manufacture method of 2-two (4-hydroxy phenyl) propane
DE4413396A1 (en) * 1994-04-18 1995-10-19 Bayer Ag Process for the preparation of ultra-pure bisphenol-A and its use

Also Published As

Publication number Publication date
DE1793431A1 (en) 1971-07-01
BE738962A (en) 1970-03-02
JPS5011909B1 (en) 1975-05-07
FR2018276A1 (en) 1970-05-29
NL6913707A (en) 1970-03-19

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Legal Events

Date Code Title Description
PS Patent sealed
PLNP Patent lapsed through nonpayment of renewal fees