GB1277282A - A process for the purification of 4,4-dihydroxy-diphenyl-2,2-propane or the phenol adduct thereof - Google Patents
A process for the purification of 4,4-dihydroxy-diphenyl-2,2-propane or the phenol adduct thereofInfo
- Publication number
- GB1277282A GB1277282A GB4062669A GB4062669A GB1277282A GB 1277282 A GB1277282 A GB 1277282A GB 4062669 A GB4062669 A GB 4062669A GB 4062669 A GB4062669 A GB 4062669A GB 1277282 A GB1277282 A GB 1277282A
- Authority
- GB
- United Kingdom
- Prior art keywords
- propane
- dihydroxy
- diphenyl
- phenol
- adduct
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
- C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
- C07C37/84—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by crystallisation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1277282 Purification of 4,4-dihydroxy-diphenyl - 2,2 - propane or the phenol adduct thereof FARBENFABRIKEN BAYER AG 14 Aug 1969 [17 Sept 1968] 40626/69 Heading C2C A process for the purification of 4,41-dihydroxydiphenyl - 2,2 - propane or the phenol adduct thereof wherein a mixed melt of 4,4<SP>1</SP>- dihydroxy - diphenyl - 2,2 - propane, phenol and impurities is cooled and the resulting crystal-slurry is separated from the mother liquor and washed with a melt of pure 4,4<SP>1</SP>- dihydroxy - diphenyl - 2,2 - propane or of pure phenol-adduct thereof whose temperature is up to 25‹ C. above its solidification point, and purified crystals thus obtained are fused and run off, the temperature of the crystal-slurry being adjusted to from 90‹ to 120‹ C. for the preparation of 4,4<SP>1</SP>-dihydroxy-diphenyl-2,2-propane and to from 55‹ to 88‹ C. for the preparation of the phenol-adduct, whilst the run-off temperature of the mother liquor is adjusted to from 100‹ to 130‹ C. for the preparation of 4,4<SP>1</SP>- dihydroxy-diphenyl-2,2-propane and from 70‹ to 90‹ C. for the preparation of phenol adduct.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19681793431 DE1793431A1 (en) | 1968-09-17 | 1968-09-17 | Process for the purification of 4,4'-dihydroxydiphenylpropane- (2,2) or the phenol adduct of these compounds |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1277282A true GB1277282A (en) | 1972-06-07 |
Family
ID=5707702
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB4062669A Expired GB1277282A (en) | 1968-09-17 | 1969-08-14 | A process for the purification of 4,4-dihydroxy-diphenyl-2,2-propane or the phenol adduct thereof |
Country Status (6)
Country | Link |
---|---|
JP (1) | JPS5011909B1 (en) |
BE (1) | BE738962A (en) |
DE (1) | DE1793431A1 (en) |
FR (1) | FR2018276A1 (en) |
GB (1) | GB1277282A (en) |
NL (1) | NL6913707A (en) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
IT971366B (en) * | 1972-11-30 | 1974-04-30 | Sir Soc Italiana Resine Spa | PROCEDURE FOR THE PRODUCTION OF 2 2 4 4 DIIDROXIDIPHENYL PROPANE |
CN1050828C (en) * | 1993-02-16 | 2000-03-29 | 中国石油化工总公司 | Method of dephenolization for preparing high quality polycarbonic ester grade bisphenol A |
CN1080914A (en) * | 1993-02-17 | 1994-01-19 | 中国石油化工总公司 | A kind of 2, the manufacture method of 2-two (4-hydroxy phenyl) propane |
DE4413396A1 (en) * | 1994-04-18 | 1995-10-19 | Bayer Ag | Process for the preparation of ultra-pure bisphenol-A and its use |
-
1968
- 1968-09-17 DE DE19681793431 patent/DE1793431A1/en active Pending
-
1969
- 1969-08-14 GB GB4062669A patent/GB1277282A/en not_active Expired
- 1969-09-09 NL NL6913707A patent/NL6913707A/xx unknown
- 1969-09-16 JP JP7283269A patent/JPS5011909B1/ja active Pending
- 1969-09-17 FR FR6931631A patent/FR2018276A1/fr not_active Withdrawn
- 1969-09-17 BE BE738962D patent/BE738962A/xx unknown
Also Published As
Publication number | Publication date |
---|---|
DE1793431A1 (en) | 1971-07-01 |
BE738962A (en) | 1970-03-02 |
JPS5011909B1 (en) | 1975-05-07 |
FR2018276A1 (en) | 1970-05-29 |
NL6913707A (en) | 1970-03-19 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PLNP | Patent lapsed through nonpayment of renewal fees |