GB1260996A - A process for the manufacture of phenazine derivatives - Google Patents
A process for the manufacture of phenazine derivativesInfo
- Publication number
- GB1260996A GB1260996A GB05635/70A GB1563570A GB1260996A GB 1260996 A GB1260996 A GB 1260996A GB 05635/70 A GB05635/70 A GB 05635/70A GB 1563570 A GB1563570 A GB 1563570A GB 1260996 A GB1260996 A GB 1260996A
- Authority
- GB
- United Kingdom
- Prior art keywords
- iodinin
- prepared
- alkali metal
- salt
- solvent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- 125000001791 phenazinyl group Chemical class C1(=CC=CC2=NC3=CC=CC=C3N=C12)* 0.000 title 1
- NBMOVCYIGUDQJE-UHFFFAOYSA-N iodinin Chemical compound C1=CC=C2[N+]([O-])=C3C(O)=CC=CC3=[N+]([O-])C2=C1O NBMOVCYIGUDQJE-UHFFFAOYSA-N 0.000 abstract 5
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 abstract 3
- 229910052783 alkali metal Inorganic materials 0.000 abstract 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 abstract 2
- -1 alkali metal salt Chemical class 0.000 abstract 2
- 229940100198 alkylating agent Drugs 0.000 abstract 2
- 239000002168 alkylating agent Substances 0.000 abstract 2
- 239000000010 aprotic solvent Substances 0.000 abstract 2
- GNOIPBMMFNIUFM-UHFFFAOYSA-N hexamethylphosphoric triamide Chemical group CN(C)P(=O)(N(C)C)N(C)C GNOIPBMMFNIUFM-UHFFFAOYSA-N 0.000 abstract 2
- 150000003839 salts Chemical class 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- YXZFFTJAHVMMLF-UHFFFAOYSA-N 1-bromo-3-methylbutane Chemical compound CC(C)CCBr YXZFFTJAHVMMLF-UHFFFAOYSA-N 0.000 abstract 1
- RBFXPOLOPNCHKW-UHFFFAOYSA-N 6-(3-methylbutoxy)-5,10-dioxidophenazine-5,10-diium-1-ol Chemical compound CC(CCOC1=C2[N+](=C3C=CC=C(C3=[N+](C2=CC=C1)[O-])O)[O-])C RBFXPOLOPNCHKW-UHFFFAOYSA-N 0.000 abstract 1
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 abstract 1
- 241000251748 Myxinidae Species 0.000 abstract 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract 1
- 125000003545 alkoxy group Chemical group 0.000 abstract 1
- 150000001351 alkyl iodides Chemical class 0.000 abstract 1
- 230000002152 alkylating effect Effects 0.000 abstract 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 1
- 230000003115 biocidal effect Effects 0.000 abstract 1
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- 238000004587 chromatography analysis Methods 0.000 abstract 1
- 229960001760 dimethyl sulfoxide Drugs 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 239000005457 ice water Substances 0.000 abstract 1
- 238000011065 in-situ storage Methods 0.000 abstract 1
- JIDVGUQUQSOHOL-UHFFFAOYSA-N myxin Chemical compound C1=CC=C2[N+]([O-])=C3C(OC)=CC=CC3=[N+]([O-])C2=C1O JIDVGUQUQSOHOL-UHFFFAOYSA-N 0.000 abstract 1
- 239000003495 polar organic solvent Substances 0.000 abstract 1
- 229910052700 potassium Inorganic materials 0.000 abstract 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 abstract 1
- 239000000741 silica gel Substances 0.000 abstract 1
- 229910002027 silica gel Inorganic materials 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D241/00—Heterocyclic compounds containing 1,4-diazine or hydrogenated 1,4-diazine rings
- C07D241/36—Heterocyclic compounds containing 1,4-diazine or hydrogenated 1,4-diazine rings condensed with carbocyclic rings or ring systems
- C07D241/50—Heterocyclic compounds containing 1,4-diazine or hydrogenated 1,4-diazine rings condensed with carbocyclic rings or ring systems with hetero atoms directly attached to ring nitrogen atoms
- C07D241/52—Oxygen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Saccharide Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US81844869A | 1969-04-22 | 1969-04-22 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1260996A true GB1260996A (en) | 1972-01-19 |
Family
ID=25225563
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB05635/70A Expired GB1260996A (en) | 1969-04-22 | 1970-04-02 | A process for the manufacture of phenazine derivatives |
Country Status (13)
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3681331A (en) * | 1970-04-02 | 1972-08-01 | Hoffmann La Roche | 1-hydroxy-6-amino alkoxy-phenazine 5,10-dioxides |
| GB201319363D0 (en) | 2013-11-01 | 2013-12-18 | Uni I Oslo | Compounds |
-
1970
- 1970-03-23 CH CH1728972A patent/CH546771A/xx not_active IP Right Cessation
- 1970-03-23 CH CH432670A patent/CH533628A/de not_active IP Right Cessation
- 1970-03-30 IL IL34193A patent/IL34193A0/xx unknown
- 1970-04-02 GB GB05635/70A patent/GB1260996A/en not_active Expired
- 1970-04-03 FI FI932/70A patent/FI54113C/fi active
- 1970-04-08 DE DE2016467A patent/DE2016467C3/de not_active Expired
- 1970-04-10 YU YU927/70A patent/YU34413B/xx unknown
- 1970-04-15 NL NL7005409A patent/NL7005409A/xx unknown
- 1970-04-20 IE IE498/70A patent/IE34101B1/xx unknown
- 1970-04-20 BE BE749172D patent/BE749172A/xx unknown
- 1970-04-21 FR FR707014385A patent/FR2060005B1/fr not_active Expired
- 1970-04-21 ES ES378852A patent/ES378852A1/es not_active Expired
- 1970-04-21 AT AT360770A patent/AT295544B/de not_active IP Right Cessation
- 1970-04-21 AT AT216371A patent/AT299219B/de not_active IP Right Cessation
- 1970-04-22 SE SE7005549A patent/SE376614B/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| AT299219B (de) | 1972-06-12 |
| IE34101L (en) | 1970-10-22 |
| NL7005409A (enrdf_load_stackoverflow) | 1970-10-26 |
| YU34413B (en) | 1979-07-10 |
| YU92770A (en) | 1978-12-31 |
| FI54113B (fi) | 1978-06-30 |
| DE2016467B2 (de) | 1979-05-10 |
| DE2016467A1 (de) | 1970-11-12 |
| BE749172A (fr) | 1970-10-20 |
| FR2060005A1 (enrdf_load_stackoverflow) | 1971-06-11 |
| CH533628A (de) | 1973-02-15 |
| CH546771A (de) | 1974-03-15 |
| FR2060005B1 (enrdf_load_stackoverflow) | 1973-03-16 |
| IL34193A0 (en) | 1970-05-21 |
| AT295544B (de) | 1972-01-10 |
| IE34101B1 (en) | 1975-02-05 |
| FI54113C (fi) | 1978-10-10 |
| DE2016467C3 (de) | 1980-01-24 |
| ES378852A1 (es) | 1973-01-16 |
| SE376614B (enrdf_load_stackoverflow) | 1975-06-02 |
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