GB1246958A - Process for producing 2,4-dihydroxybenzophenone - Google Patents

Process for producing 2,4-dihydroxybenzophenone

Info

Publication number
GB1246958A
GB1246958A GB429270A GB429270A GB1246958A GB 1246958 A GB1246958 A GB 1246958A GB 429270 A GB429270 A GB 429270A GB 429270 A GB429270 A GB 429270A GB 1246958 A GB1246958 A GB 1246958A
Authority
GB
United Kingdom
Prior art keywords
dihydroxybenzophenone
alkoxybenzophenones
hydroxy
weight
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB429270A
Inventor
Hirohisa Shioda
Isamu Namiki
Hisako Hori
Yoshihisa Katsuyma
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Furukawa Electric Co Ltd
Original Assignee
Furukawa Electric Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Furukawa Electric Co Ltd filed Critical Furukawa Electric Co Ltd
Priority to GB429270A priority Critical patent/GB1246958A/en
Publication of GB1246958A publication Critical patent/GB1246958A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/45—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by condensation
    • C07C45/46—Friedel-Crafts reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/008—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with tri- or tetrahalomethyl compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/67—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
    • C07C45/68—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
    • C07C45/70—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction with functional groups containing oxygen only in singly bound form
    • C07C45/71—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction with functional groups containing oxygen only in singly bound form being hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/04—Oxygen-containing compounds
    • C08K5/07—Aldehydes; Ketones
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L27/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/04—Oxygen-containing compounds
    • C08K5/13—Phenols; Phenolates
    • C08K5/132—Phenols containing keto groups, e.g. benzophenones

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1,246,958. 2,4-Dihydroxybenzophenone; 2- hydroxy - 4 - alkoxybenzophenones. FURUKAWA DENKI KOGYO K.K. 29 Jan., 1970, No. 4292/70. Heading C2C. 2,4-Dihydroxybenzophenone is prepared by reacting resorcinol with benzotrichloride at 10-90‹ C. in a mixed solvent comprising 20- 90% by weight of water and 10-80% by weight of water-miscible organic solvent. The preferred organic solvents are C 1 -C 4 alkanols, especially methanol, ethylene glycol monoethyl ether, tetrahydrofuran, dioxane and acetic, propionic and butyric acids. Preferably an emulsifier is present in the reaction mixture. The 2,4-dihydroxybenzophenone so obtained may be converted to 2-hydroxy-4-alkoxybenzophenones by reacting with an alkyl halide or with an alkyl ester of benzene sulphonic or pmethyl benzene sulphonic acid in aqueous alkaline solution.
GB429270A 1970-01-29 1970-01-29 Process for producing 2,4-dihydroxybenzophenone Expired GB1246958A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB429270A GB1246958A (en) 1970-01-29 1970-01-29 Process for producing 2,4-dihydroxybenzophenone

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB429270A GB1246958A (en) 1970-01-29 1970-01-29 Process for producing 2,4-dihydroxybenzophenone

Publications (1)

Publication Number Publication Date
GB1246958A true GB1246958A (en) 1971-09-22

Family

ID=9774398

Family Applications (1)

Application Number Title Priority Date Filing Date
GB429270A Expired GB1246958A (en) 1970-01-29 1970-01-29 Process for producing 2,4-dihydroxybenzophenone

Country Status (1)

Country Link
GB (1) GB1246958A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2473506A1 (en) * 1980-01-11 1981-07-17 Solvay PROCESS FOR THE MANUFACTURE OF SUBSTITUTED 2-HYDROXYBENZOPHENONES
US4568429A (en) * 1984-03-02 1986-02-04 Gaf Corporation Process for the preparation of 2,4-dihydroxybenzophenones

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2473506A1 (en) * 1980-01-11 1981-07-17 Solvay PROCESS FOR THE MANUFACTURE OF SUBSTITUTED 2-HYDROXYBENZOPHENONES
EP0032275A2 (en) * 1980-01-11 1981-07-22 American Cyanamid Company Process for the preparation of substituted 2-hydroxy-benzophenones
EP0032275A3 (en) * 1980-01-11 1981-08-26 American Cyanamid Company Process for the preparation of substituted 2-hydroxy-benzophenones
US4568429A (en) * 1984-03-02 1986-02-04 Gaf Corporation Process for the preparation of 2,4-dihydroxybenzophenones

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