GB1242044A - Process for the production of aralkylmonohydroperoxides - Google Patents

Process for the production of aralkylmonohydroperoxides

Info

Publication number
GB1242044A
GB1242044A GB195669A GB195669A GB1242044A GB 1242044 A GB1242044 A GB 1242044A GB 195669 A GB195669 A GB 195669A GB 195669 A GB195669 A GB 195669A GB 1242044 A GB1242044 A GB 1242044A
Authority
GB
United Kingdom
Prior art keywords
aralkylmonohydroperoxides
hydrocarbon
oxidate
jan
absence
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB195669A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ineos Phenol GmbH
Original Assignee
Phenolchemie GmbH and Co KG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE19681668575 external-priority patent/DE1668575C/en
Application filed by Phenolchemie GmbH and Co KG filed Critical Phenolchemie GmbH and Co KG
Publication of GB1242044A publication Critical patent/GB1242044A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C409/00Peroxy compounds
    • C07C409/02Peroxy compounds the —O—O— group being bound between a carbon atom, not further substituted by oxygen atoms, and hydrogen, i.e. hydroperoxides
    • C07C409/04Peroxy compounds the —O—O— group being bound between a carbon atom, not further substituted by oxygen atoms, and hydrogen, i.e. hydroperoxides the carbon atom being acyclic
    • C07C409/08Compounds containing six-membered aromatic rings
    • C07C409/10Cumene hydroperoxide
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C407/00Preparation of peroxy compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C407/00Preparation of peroxy compounds
    • C07C407/003Separation; Purification; Stabilisation; Use of additives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1,242,044. Aralkyl monohydroperoxides. PHENOLCHEMIE G.m.b.H. 13 Jan., 1969 [13 Jan., 1968], No. 1956/69. Heading C2C. A process for the production of aralkylmonohydroperoxides of the general formula in which Ar is an aromatic hydrocarbon radical and R is an aliphatic hydrocarbon radical comprises oxidizing a hydrocarbon of the general formula in the liquid state with oxygen or oxygencontaining gases at a temperature in the range 40-135‹ C., in the absence of acid-fixing agents or of substances promoting the reaction, and in the absence of substantially any water and feeding the oxidate having a higher temperature direct and without intermediate processing into an apparatus in which unconverted hydrocarbon is under reduced pressure, the pressure conditions being such that substantially all the heat of formation of the aralkylmonohydroperoxides is used for the evaporation of the unconverted hydrocarbon. In an example cumene and oxygen are fed into an oxidation reactor to yield a 12% cumol hydroperoxide oxidate, which was then fed direct to a vacuum apparatus at 30-40 torr and a 20% cumene hydroperoxide solution obtained.
GB195669A 1968-01-13 1969-01-13 Process for the production of aralkylmonohydroperoxides Expired GB1242044A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19681668575 DE1668575C (en) 1968-01-13 1968-01-13 Process for the production of cumene hydroperoxide

Publications (1)

Publication Number Publication Date
GB1242044A true GB1242044A (en) 1971-08-11

Family

ID=5686113

Family Applications (1)

Application Number Title Priority Date Filing Date
GB195669A Expired GB1242044A (en) 1968-01-13 1969-01-13 Process for the production of aralkylmonohydroperoxides

Country Status (4)

Country Link
CH (1) CH510618A (en)
CS (1) CS150968B2 (en)
FR (1) FR1600006A (en)
GB (1) GB1242044A (en)

Also Published As

Publication number Publication date
FR1600006A (en) 1970-07-20
CS150968B2 (en) 1973-09-17
CH510618A (en) 1971-07-31

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