GB1228727A - - Google Patents
Info
- Publication number
- GB1228727A GB1228727A GB1228727DA GB1228727A GB 1228727 A GB1228727 A GB 1228727A GB 1228727D A GB1228727D A GB 1228727DA GB 1228727 A GB1228727 A GB 1228727A
- Authority
- GB
- United Kingdom
- Prior art keywords
- diarylamino
- march
- absence
- solvent
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
Abstract
1,228,727. 2,5-Diarylamino terephthalic acids. FARBWERKE HOECHST A.G. 25 March, 1969 [26 March, 1968], No. 15546/69. Heading C2C. A process for the preparation of a 2,5-diarylamino terephthalic acid comprises condensing the dimethyl or diethyl ester of succinylsuccinic acid with an aromatic amine in the absence of a solvent, oxidizing the 2,5-diarylamino-dihydroterephthalic acid ester obtained with nitrobenzene in the absence of a solvent, saponifying the ester groups with an aqueous alkaline solution and extracting the dialkali metal salt obtained with water and, after separating from the organic phase, precipitating the 2,5-diarylamino terephthalic acid by acidifying the aqueous phase. Suitable arylamines are aniline, the chloro anilines, the toluidines, the chlorotoluidines, the anisidines and 1- and 2-naphthylamine.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE1768049A DE1768049B2 (en) | 1968-03-26 | 1968-03-26 | Process for the preparation of 2,5- (di-arylamino) -terephthalic acids |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1228727A true GB1228727A (en) | 1971-04-15 |
Family
ID=5699577
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1228727D Expired GB1228727A (en) | 1968-03-26 | 1969-03-25 |
Country Status (6)
Country | Link |
---|---|
JP (1) | JPS5116418B1 (en) |
BE (1) | BE730473A (en) |
CH (1) | CH502987A (en) |
DE (1) | DE1768049B2 (en) |
FR (1) | FR2004790A1 (en) |
GB (1) | GB1228727A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4435589A (en) | 1981-02-10 | 1984-03-06 | Bayer Aktiengesellschaft | Process for the preparation of dimethyl succinylosuccinate, the disodium salt thereof, dianilinodihydroterephthalic acids, the dimethyl esters and salts thereof, and dianilinoterephthalic acids, and the dimethyl esters and salts thereof |
US4981997A (en) * | 1988-10-12 | 1991-01-01 | Bayer Aktiengesellschaft | Process for the preparation of 2,5-diarylaminoterephthalic acids |
EP0648733A2 (en) * | 1993-10-19 | 1995-04-19 | DSM Chemie Linz GmbH | Quinacridone synthesis and process for preparation of intermediates |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2542494C3 (en) * | 1975-09-24 | 1981-04-30 | Hoechst Ag, 6000 Frankfurt | Process for the preparation of pure substituted 2,5 diarylaminoterephthalic acid esters and the corresponding free acids |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB918511A (en) * | 1960-05-23 | 1963-02-13 | Ciba Ltd | Process for the manufacture of 2:5-diarylamino-terephthalic acids |
US3285952A (en) * | 1962-11-20 | 1966-11-15 | Allied Chem | Oxidation of 2, 5-diarylamino-dihydro-terephthalates with nitrobenzene |
-
1968
- 1968-03-26 DE DE1768049A patent/DE1768049B2/en active Granted
-
1969
- 1969-03-24 CH CH442569A patent/CH502987A/en not_active IP Right Cessation
- 1969-03-25 GB GB1228727D patent/GB1228727A/en not_active Expired
- 1969-03-26 JP JP44022419A patent/JPS5116418B1/ja active Pending
- 1969-03-26 BE BE730473D patent/BE730473A/xx unknown
- 1969-03-26 FR FR6908960A patent/FR2004790A1/fr not_active Withdrawn
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4435589A (en) | 1981-02-10 | 1984-03-06 | Bayer Aktiengesellschaft | Process for the preparation of dimethyl succinylosuccinate, the disodium salt thereof, dianilinodihydroterephthalic acids, the dimethyl esters and salts thereof, and dianilinoterephthalic acids, and the dimethyl esters and salts thereof |
US4981997A (en) * | 1988-10-12 | 1991-01-01 | Bayer Aktiengesellschaft | Process for the preparation of 2,5-diarylaminoterephthalic acids |
EP0648733A2 (en) * | 1993-10-19 | 1995-04-19 | DSM Chemie Linz GmbH | Quinacridone synthesis and process for preparation of intermediates |
EP0648733A3 (en) * | 1993-10-19 | 1995-08-16 | Chemie Linz Gmbh | Quinacridone synthesis and process for preparation of intermediates. |
US5491255A (en) * | 1993-10-19 | 1996-02-13 | Chemie Linz Gmbh | Process for the transesterification of dimethyl succinylsuccinate |
US5659076A (en) * | 1993-10-19 | 1997-08-19 | Dsm Chemie Linz Gmbh | Process for the production of 2,5-dianilino-terephthalic acids |
Also Published As
Publication number | Publication date |
---|---|
BE730473A (en) | 1969-09-26 |
JPS5116418B1 (en) | 1976-05-24 |
DE1768049A1 (en) | 1971-11-18 |
DE1768049B2 (en) | 1974-06-20 |
FR2004790A1 (en) | 1969-11-28 |
DE1768049C3 (en) | 1975-02-13 |
CH502987A (en) | 1971-02-15 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed [section 19, patents act 1949] | ||
PCNP | Patent ceased through non-payment of renewal fee |