GB1204293A - Ammonium salt complexes of, and process for purifying, hexachlorophene and 2,4,5-trichlorophenol - Google Patents
Ammonium salt complexes of, and process for purifying, hexachlorophene and 2,4,5-trichlorophenolInfo
- Publication number
- GB1204293A GB1204293A GB652569A GB652569A GB1204293A GB 1204293 A GB1204293 A GB 1204293A GB 652569 A GB652569 A GB 652569A GB 652569 A GB652569 A GB 652569A GB 1204293 A GB1204293 A GB 1204293A
- Authority
- GB
- United Kingdom
- Prior art keywords
- trichlorophenol
- hexachlorophene
- complex
- ammonium salt
- salt complexes
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
- C07C37/86—Purification; separation; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
- C07C37/685—Processes comprising at least two steps in series
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
- C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
- C07C37/84—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by crystallisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
- C07C39/24—Halogenated derivatives
- C07C39/26—Halogenated derivatives monocyclic monohydroxylic containing halogen bound to ring carbon atoms
- C07C39/27—Halogenated derivatives monocyclic monohydroxylic containing halogen bound to ring carbon atoms all halogen atoms being bound to ring carbon atoms
- C07C39/32—Halogenated derivatives monocyclic monohydroxylic containing halogen bound to ring carbon atoms all halogen atoms being bound to ring carbon atoms the halogen being three chlorine atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
- C07C39/24—Halogenated derivatives
- C07C39/367—Halogenated derivatives polycyclic non-condensed, containing only six-membered aromatic rings as cyclic parts, e.g. halogenated poly-hydroxyphenylalkanes
Abstract
1,204,293. Ammonium salt complexes of and methods of purification of 2,4,5-trichlorophenol and hexachlorophene. E. B. MICHAELS and J. W. LEE. 6 Feb., 1969 [6 Feb., 1968], No. 6525/69. Heading C2C. The invention relates to a process for preparing a complex of hexachlorophene or 2,4,5-trichlorophenol which comprises adding to a solution of the hexachlorophene or 2,4,5-trichlorophenol in a solvent in which the complex is insoluble ammonia gas, aqueous ammonia, or ammonium carbonate in an amount sufficient to form a precipitate of solid complex. Pure hexachlorophene or 2,4,5-trichlorophenol may be obtained by heating the separated solid precipitated complex to free ammonia therefrom.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US70327168A | 1968-02-06 | 1968-02-06 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1204293A true GB1204293A (en) | 1970-09-03 |
Family
ID=24824721
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB652569A Expired GB1204293A (en) | 1968-02-06 | 1969-02-06 | Ammonium salt complexes of, and process for purifying, hexachlorophene and 2,4,5-trichlorophenol |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB1204293A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0017141A1 (en) * | 1979-03-30 | 1980-10-15 | L. Givaudan & Cie Société Anonyme | Process for the purification of trichlorophenol |
-
1969
- 1969-02-06 GB GB652569A patent/GB1204293A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0017141A1 (en) * | 1979-03-30 | 1980-10-15 | L. Givaudan & Cie Société Anonyme | Process for the purification of trichlorophenol |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PCNP | Patent ceased through non-payment of renewal fee |