GB1197758A - Process for the Preparation of the Tetrasodium Salt of Reduced Nicotinamide-Adenine-Dinucleotide-Phosphate. - Google Patents
Process for the Preparation of the Tetrasodium Salt of Reduced Nicotinamide-Adenine-Dinucleotide-Phosphate.Info
- Publication number
- GB1197758A GB1197758A GB4080667A GB4080667A GB1197758A GB 1197758 A GB1197758 A GB 1197758A GB 4080667 A GB4080667 A GB 4080667A GB 4080667 A GB4080667 A GB 4080667A GB 1197758 A GB1197758 A GB 1197758A
- Authority
- GB
- United Kingdom
- Prior art keywords
- phosphate
- tetrasodium salt
- reduced
- adenine
- dinucleotide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H19/00—Compounds containing a hetero ring sharing one ring hetero atom with a saccharide radical; Nucleosides; Mononucleotides; Anhydro-derivatives thereof
- C07H19/02—Compounds containing a hetero ring sharing one ring hetero atom with a saccharide radical; Nucleosides; Mononucleotides; Anhydro-derivatives thereof sharing nitrogen
- C07H19/04—Heterocyclic radicals containing only nitrogen atoms as ring hetero atom
- C07H19/16—Purine radicals
- C07H19/20—Purine radicals with the saccharide radical esterified by phosphoric or polyphosphoric acids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
1,197,758. Tetrasodium salt of reduced nicotinamide - adenine - dinucleotide phosphate. ARZNEIMITTELWERK DRESDEN VEB. 6 Sept., 1967, No. 40806/67. Heading C2C. The tetrasodium salt of reduced nicotinamideadeninedinucleotide phosphate is prepared by applying a solution of reduced nicotinamideadeninedinucleotide phosphate to a column of DEAE cellulose and eluting with a volatile buffer medium having a pH of less than 8 and having a linear increasing gradient of a sodium halide which is soluble in alcohol, the pH of the eluate being then adjusted to about 10 by adding a dilute aqueous solution of sodium hydroxide. The elution is preferably carried out at about 4‹ C. Good results are obtained by using the system pyridine-acetic acid or ethylene diamine-acetic acid at a pH below 8, e.g. 7À6-7À8, as the volatile buffer and using NaI or NaBr as the sodium halide.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB4080667A GB1197758A (en) | 1967-09-06 | 1967-09-06 | Process for the Preparation of the Tetrasodium Salt of Reduced Nicotinamide-Adenine-Dinucleotide-Phosphate. |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB4080667A GB1197758A (en) | 1967-09-06 | 1967-09-06 | Process for the Preparation of the Tetrasodium Salt of Reduced Nicotinamide-Adenine-Dinucleotide-Phosphate. |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1197758A true GB1197758A (en) | 1970-07-08 |
Family
ID=10416710
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB4080667A Expired GB1197758A (en) | 1967-09-06 | 1967-09-06 | Process for the Preparation of the Tetrasodium Salt of Reduced Nicotinamide-Adenine-Dinucleotide-Phosphate. |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB1197758A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4151349A (en) * | 1977-02-01 | 1979-04-24 | Boehringer Mannheim Gmbh | Crystalline potassium salt of β-nicotinamide adenine dinucleotide phosphoric acid and method for its preparation |
CN112774254A (en) * | 2021-01-09 | 2021-05-11 | 北京智飞绿竹生物制药有限公司 | Method for cleaning ion exchange chromatography medium |
-
1967
- 1967-09-06 GB GB4080667A patent/GB1197758A/en not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4151349A (en) * | 1977-02-01 | 1979-04-24 | Boehringer Mannheim Gmbh | Crystalline potassium salt of β-nicotinamide adenine dinucleotide phosphoric acid and method for its preparation |
CN112774254A (en) * | 2021-01-09 | 2021-05-11 | 北京智飞绿竹生物制药有限公司 | Method for cleaning ion exchange chromatography medium |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PLNP | Patent lapsed through nonpayment of renewal fees |