GB1196509A - A process for Oxidizing Trichloroethylene to Dichloroacetyl Chloride - Google Patents

A process for Oxidizing Trichloroethylene to Dichloroacetyl Chloride

Info

Publication number
GB1196509A
GB1196509A GB4428868A GB4428868A GB1196509A GB 1196509 A GB1196509 A GB 1196509A GB 4428868 A GB4428868 A GB 4428868A GB 4428868 A GB4428868 A GB 4428868A GB 1196509 A GB1196509 A GB 1196509A
Authority
GB
United Kingdom
Prior art keywords
carbon atoms
dichloroacetyl chloride
trichloroethylene
oxidizing
amine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB4428868A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shell Internationale Research Maatschappij BV
Original Assignee
Shell Internationale Research Maatschappij BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shell Internationale Research Maatschappij BV filed Critical Shell Internationale Research Maatschappij BV
Publication of GB1196509A publication Critical patent/GB1196509A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/58Preparation of carboxylic acid halides

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1,196,509. Dichloroacetyl chloride. SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ N.V. 18 Sept., 1968 [20 Sept., 1967], No. 44288/68. Heading C2C. Dichloroacetyl chloride is obtained by oxidizing trichloroethylene with oxygen or an oxygen-containing gas at 50‹ to 250‹ C., at atmospheric pressure or above, in the presence of 20 to 2000 p.p.m. of an azo compound and 30 to 1000 p.p.m. of a secondary or tertiary amine, the azo compound having the formula where each R is a hydrogen atom or a cyano, -R1-CO-NH 2 , carbalkoxy or C 1-6 alkyl radical or two adjacent R groups complete an alicyclic ring, R<SP>1</SP> being a covalent bond or a C 1-6 alkylene radical, and the amine being a secondary amine with up to 12 carbon atoms, a tertiary alkylamine with up to 18 carbon atoms or a tertiary arylamine with up to 14 carbon atoms. Reference has been directed by the Comptroller to Specification 1,073.369.
GB4428868A 1967-09-20 1968-09-18 A process for Oxidizing Trichloroethylene to Dichloroacetyl Chloride Expired GB1196509A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US66926567A 1967-09-20 1967-09-20

Publications (1)

Publication Number Publication Date
GB1196509A true GB1196509A (en) 1970-06-24

Family

ID=24685741

Family Applications (1)

Application Number Title Priority Date Filing Date
GB4428868A Expired GB1196509A (en) 1967-09-20 1968-09-18 A process for Oxidizing Trichloroethylene to Dichloroacetyl Chloride

Country Status (6)

Country Link
BE (1) BE721017A (en)
CH (1) CH508573A (en)
DE (1) DE1793446A1 (en)
FR (1) FR1581376A (en)
GB (1) GB1196509A (en)
NL (1) NL6813397A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115504879A (en) * 2021-06-22 2022-12-23 联化科技股份有限公司 Method for continuously preparing dichloroacetyl chloride

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115504879A (en) * 2021-06-22 2022-12-23 联化科技股份有限公司 Method for continuously preparing dichloroacetyl chloride

Also Published As

Publication number Publication date
DE1793446A1 (en) 1972-01-27
CH508573A (en) 1971-06-15
FR1581376A (en) 1969-09-12
BE721017A (en) 1969-03-18
NL6813397A (en) 1969-03-24

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Legal Events

Date Code Title Description
PS Patent sealed
PLNP Patent lapsed through nonpayment of renewal fees