GB1189649A - Improvements in and relating to the Production of Oxide Materials. - Google Patents
Improvements in and relating to the Production of Oxide Materials.Info
- Publication number
- GB1189649A GB1189649A GB2440066A GB2440066A GB1189649A GB 1189649 A GB1189649 A GB 1189649A GB 2440066 A GB2440066 A GB 2440066A GB 2440066 A GB2440066 A GB 2440066A GB 1189649 A GB1189649 A GB 1189649A
- Authority
- GB
- United Kingdom
- Prior art keywords
- magnesium oxide
- take place
- lithium salt
- magnesium
- isopropanol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F5/00—Compounds of magnesium
- C01F5/02—Magnesia
- C01F5/06—Magnesia by thermal decomposition of magnesium compounds
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/03—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on magnesium oxide, calcium oxide or oxide mixtures derived from dolomite
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/10—Solid density
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
1,189,649. Dense magnesium oxide. THERMAL SYNDICATE Ltd. 31 Aug., 1967 [1 June, 1966], No. 24400/66. Heading C1A. A block of magnesium oxide of density not less than 3À50 gm./c.c. is made by intimately mixing magnesium oxide powder of surface area determined by nitrogen adsorption greater than 10 m<SP>2</SP>/g. (prepared by calcining a decomposable magnesium compound below 850‹ C.) with 0À1 to 10% by weight of finely divided lithium salt, e.g. lithium fluoride, sintering by heating in air at 700‹ C. or above, heating to 800‹ to 1400‹ C. while compressing in a die under 500 to 3000 p.s.i. pressure in a vacuum less than 0À5 torr, and firing at 1000‹ C. or above in a moving atmosphere. Calcination to produce magnesium oxide may take place in a rotary drum. The intimate mixture may be formed by mixing slurries of magnesium oxide and lithium fluoride in an inert organic liquid, e.g. isopropanol, grinding in a colloid mill and evaporating most of the solvent. Sintering may take place in a recrystallized alumina tube, and graphite dies are preferably used in the compression. Firing to remove excess lithium salt may take place in an atmosphere of air, argon, or oxygen. Specified decomposable magnesium compounds are the sulphate, hydroxide, oxalate and basic carbonate. Magnesium oxide and lithium salt may be prepared as suspensions in an inert organic liquid, e.g. isopropanol in order to minimize pick-up of CO 2 and water vapour.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB2440066A GB1189649A (en) | 1966-06-01 | 1966-06-01 | Improvements in and relating to the Production of Oxide Materials. |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB2440066A GB1189649A (en) | 1966-06-01 | 1966-06-01 | Improvements in and relating to the Production of Oxide Materials. |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1189649A true GB1189649A (en) | 1970-04-29 |
Family
ID=10211144
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB2440066A Expired GB1189649A (en) | 1966-06-01 | 1966-06-01 | Improvements in and relating to the Production of Oxide Materials. |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB1189649A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2166424A (en) * | 1984-11-01 | 1986-05-08 | Atomic Energy Authority Uk | Synthetic rock materials |
-
1966
- 1966-06-01 GB GB2440066A patent/GB1189649A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2166424A (en) * | 1984-11-01 | 1986-05-08 | Atomic Energy Authority Uk | Synthetic rock materials |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed |