GB1153364A - Process for the Production of Epsilon-Caprolactone. - Google Patents
Process for the Production of Epsilon-Caprolactone.Info
- Publication number
- GB1153364A GB1153364A GB361267A GB361267A GB1153364A GB 1153364 A GB1153364 A GB 1153364A GB 361267 A GB361267 A GB 361267A GB 361267 A GB361267 A GB 361267A GB 1153364 A GB1153364 A GB 1153364A
- Authority
- GB
- United Kingdom
- Prior art keywords
- epsilon
- caprolactone
- basic
- acetate
- carbonate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D315/00—Heterocyclic compounds containing rings having one oxygen atom as the only ring hetero atom according to more than one of groups C07D303/00 - C07D313/00
Abstract
1,153,364. Epsilon-caprolactone. UGINE KUHLMANN. 24 Jan., 1967 [12 Feb., 1966], No. 3612/67. Heading C2C. Epsilon-caprolactone is prepared by heating esters or self-polyesters of epsilon-hydroxycaproic acid between approximately 150‹ and 350‹ C. in the presence of a basic compound as catalyst. Reduced pressure is preferred and the reaction products may be distilled as they are formed, or the alkanol first in the case of an alkyl ester. The basic compound may be a hydroxide, oxide, carbonate, cyanide, alcoholate, acetate or propionate of an alkali or alkaline earth metal, Mg, Zn, Cd, Al, Ti, Pb, Sn, or Sb, or a basic salt such as a Cu or Ag basic carbonate or acetate.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR49397A FR1474903A (en) | 1966-02-12 | 1966-02-12 | Process for preparing epsiloncaprolactone |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1153364A true GB1153364A (en) | 1969-05-29 |
Family
ID=8601219
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB361267A Expired GB1153364A (en) | 1966-02-12 | 1967-01-24 | Process for the Production of Epsilon-Caprolactone. |
Country Status (10)
| Country | Link |
|---|---|
| JP (1) | JPS4819640B1 (en) |
| AT (1) | AT265231B (en) |
| BE (1) | BE693971A (en) |
| CH (1) | CH468374A (en) |
| DE (1) | DE1643147B2 (en) |
| ES (1) | ES336114A1 (en) |
| FR (1) | FR1474903A (en) |
| GB (1) | GB1153364A (en) |
| LU (1) | LU52952A1 (en) |
| NL (1) | NL6702054A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5068361A (en) * | 1988-07-08 | 1991-11-26 | Basf Aktiengesellschaft | Preparation of caprolactone |
| US5100435A (en) * | 1990-12-04 | 1992-03-31 | Kimberly-Clark Corporation | Meltblown nonwoven webs made from epoxy/pcl blends |
| US5250707A (en) * | 1990-04-25 | 1993-10-05 | Ube Industries, Ltd. | Process for preparing ε-caprolactone |
| EP0940396A1 (en) * | 1998-03-03 | 1999-09-08 | Hüls Aktiengesellschaft | Process for the preparation of lactones |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3546251A (en) * | 1966-05-25 | 1970-12-08 | Chisso Corp | Process for producing caprolactone |
| DE2714564C2 (en) * | 1977-04-01 | 1986-01-02 | Chemische Werke Hüls AG, 4370 Marl | Process for the preparation of cyclic diesters of undecanedioic acid |
| GB8621094D0 (en) * | 1986-09-01 | 1986-10-08 | Ici Plc | Loading of polymer additives |
| US6838577B2 (en) | 2000-08-24 | 2005-01-04 | Union Carbide Chemicals & Plastics Technology Corporation | Processes for the manufacture of lactones |
-
1966
- 1966-02-12 FR FR49397A patent/FR1474903A/en not_active Expired
-
1967
- 1967-01-24 GB GB361267A patent/GB1153364A/en not_active Expired
- 1967-01-26 ES ES336114A patent/ES336114A1/en not_active Expired
- 1967-01-28 JP JP554967A patent/JPS4819640B1/ja active Pending
- 1967-01-31 DE DE19671643147 patent/DE1643147B2/en active Granted
- 1967-02-08 LU LU52952D patent/LU52952A1/xx unknown
- 1967-02-08 CH CH185767A patent/CH468374A/en unknown
- 1967-02-10 NL NL6702054A patent/NL6702054A/xx unknown
- 1967-02-10 AT AT128567A patent/AT265231B/en active
- 1967-02-13 BE BE693971D patent/BE693971A/xx unknown
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5068361A (en) * | 1988-07-08 | 1991-11-26 | Basf Aktiengesellschaft | Preparation of caprolactone |
| US5250707A (en) * | 1990-04-25 | 1993-10-05 | Ube Industries, Ltd. | Process for preparing ε-caprolactone |
| US5100435A (en) * | 1990-12-04 | 1992-03-31 | Kimberly-Clark Corporation | Meltblown nonwoven webs made from epoxy/pcl blends |
| EP0940396A1 (en) * | 1998-03-03 | 1999-09-08 | Hüls Aktiengesellschaft | Process for the preparation of lactones |
Also Published As
| Publication number | Publication date |
|---|---|
| NL6702054A (en) | 1967-08-14 |
| JPS4819640B1 (en) | 1973-06-14 |
| DE1643147A1 (en) | 1972-04-06 |
| DE1643147B2 (en) | 1973-06-14 |
| ES336114A1 (en) | 1968-01-01 |
| BE693971A (en) | 1967-07-17 |
| DE1643147C3 (en) | 1974-01-24 |
| LU52952A1 (en) | 1967-04-10 |
| CH468374A (en) | 1969-02-15 |
| AT265231B (en) | 1968-10-10 |
| FR1474903A (en) | 1967-03-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PE | Patent expired |