GB1117755A - Process for the preparation of sulphuric acid solutions of nitrosyl sulphuric acid - Google Patents

Process for the preparation of sulphuric acid solutions of nitrosyl sulphuric acid

Info

Publication number
GB1117755A
GB1117755A GB5085565A GB5085565A GB1117755A GB 1117755 A GB1117755 A GB 1117755A GB 5085565 A GB5085565 A GB 5085565A GB 5085565 A GB5085565 A GB 5085565A GB 1117755 A GB1117755 A GB 1117755A
Authority
GB
United Kingdom
Prior art keywords
sulphuric acid
sulphuric
nitrosyl
acid
mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB5085565A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Organico
Original Assignee
Organico
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Organico filed Critical Organico
Publication of GB1117755A publication Critical patent/GB1117755A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00Nitrogen; Compounds thereof
    • C01B21/082Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/086Compounds containing nitrogen and non-metals and optionally metals containing one or more sulfur atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/06Phosphorus compounds without P—C bonds
    • C07F9/16Esters of thiophosphoric acids or thiophosphorous acids
    • C07F9/165Esters of thiophosphoric acids
    • C07F9/18Esters of thiophosphoric acids with hydroxyaryl compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Inorganic Chemistry (AREA)
  • Cleaning Or Drying Semiconductors (AREA)

Abstract

A sulphuric acid solution of nitrosyl-sulphuric acid is produced by reacting preferably at -15 DEG to + 70 DEG C., in stoichiometric quantities, sulphurous anhydride with nitric acid, the reaction being conducted in a medium of sulphuric acid and in the presence of nitrosyl sulphuric acid and water as initiators, the initial quantity of water being such that the weight of sulphuric acid with respect to the sum of the weights of sulphuric acid and water comprises 70-97 per cent. The initiator nitrosyl sulphuric acid may be formed in situ by the addition of NO2, a mixture of NO2 and NO or a mixture of NO and molecular oxygen to a mixture of sulphuric and nitric acids. Alternatively the initiator may be formed by the addition to a mixture of sulphuric and nitric acids, mineral salts or organic esters of nitrous acid or sulphurous anhydride in the presence of air. In place of mixing sulphuric and nitric acids, a mixture containing the reaction components: sulphuric acid, nitric acid, water and nitrosyl sulphuric acid, may be obtained by the action of nitrogen peroxide on excess sulphuric acid.
GB5085565A 1964-11-30 1965-11-30 Process for the preparation of sulphuric acid solutions of nitrosyl sulphuric acid Expired GB1117755A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR996752A FR1431704A (en) 1964-11-30 1964-11-30 Manufacturing process of nitrosyl sulfuric acid

Publications (1)

Publication Number Publication Date
GB1117755A true GB1117755A (en) 1968-06-26

Family

ID=8843637

Family Applications (1)

Application Number Title Priority Date Filing Date
GB5085565A Expired GB1117755A (en) 1964-11-30 1965-11-30 Process for the preparation of sulphuric acid solutions of nitrosyl sulphuric acid

Country Status (7)

Country Link
BE (1) BE672508A (en)
CH (1) CH442252A (en)
DE (1) DE1567734A1 (en)
FR (1) FR1431704A (en)
GB (1) GB1117755A (en)
LU (1) LU49890A1 (en)
NL (1) NL6515527A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5955050A (en) * 1994-10-25 1999-09-21 Marsulex Inc. Nox destruction in sulphuric acid

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5955050A (en) * 1994-10-25 1999-09-21 Marsulex Inc. Nox destruction in sulphuric acid

Also Published As

Publication number Publication date
FR1431704A (en) 1966-03-18
CH442252A (en) 1967-08-31
NL6515527A (en) 1966-05-31
LU49890A1 (en) 1966-01-22
DE1567734A1 (en) 1970-09-17
BE672508A (en) 1966-03-16

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