GB1097270A - Process for the preparation of methylene dioxybenzene, 1,3-benzoxathiole and derivatives thereof - Google Patents
Process for the preparation of methylene dioxybenzene, 1,3-benzoxathiole and derivatives thereofInfo
- Publication number
- GB1097270A GB1097270A GB43418/65A GB4341865A GB1097270A GB 1097270 A GB1097270 A GB 1097270A GB 43418/65 A GB43418/65 A GB 43418/65A GB 4341865 A GB4341865 A GB 4341865A GB 1097270 A GB1097270 A GB 1097270A
- Authority
- GB
- United Kingdom
- Prior art keywords
- methylene
- benzoxathiole
- preparation
- methyl
- formula
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000002360 preparation method Methods 0.000 title abstract 3
- FTNJQNQLEGKTGD-UHFFFAOYSA-N 1,3-benzodioxole Chemical compound C1=CC=C2OCOC2=C1 FTNJQNQLEGKTGD-UHFFFAOYSA-N 0.000 title abstract 2
- AIUOUEPKBRDPLG-UHFFFAOYSA-N 1,3-benzoxathiole Chemical compound C1=CC=C2SCOC2=C1 AIUOUEPKBRDPLG-UHFFFAOYSA-N 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 abstract 3
- NWRWWWMEZJKVCS-UHFFFAOYSA-N benzo[f][1,3]benzodioxole Chemical compound C1=CC=C2C=C(OCO3)C3=CC2=C1 NWRWWWMEZJKVCS-UHFFFAOYSA-N 0.000 abstract 2
- SATCULPHIDQDRE-UHFFFAOYSA-N piperonal Chemical compound O=CC1=CC=C2OCOC2=C1 SATCULPHIDQDRE-UHFFFAOYSA-N 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- -1 1-methyl-3,4-methylene Chemical group 0.000 abstract 1
- DMBGBAJZGAJGLD-UHFFFAOYSA-N 4-propan-2-yl-1,3-benzodioxole Chemical compound CC(C)C1=CC=CC2=C1OCO2 DMBGBAJZGAJGLD-UHFFFAOYSA-N 0.000 abstract 1
- XGHBMXNEBREDBN-UHFFFAOYSA-N CC1=C2C(=CC(=C1)C(CC(C)(C)C)(C)C)OCO2 Chemical compound CC1=C2C(=CC(=C1)C(CC(C)(C)C)(C)C)OCO2 XGHBMXNEBREDBN-UHFFFAOYSA-N 0.000 abstract 1
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 abstract 1
- FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 abstract 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical group [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract 1
- 150000001450 anions Chemical class 0.000 abstract 1
- 150000001491 aromatic compounds Chemical class 0.000 abstract 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 229960001760 dimethyl sulfoxide Drugs 0.000 abstract 1
- 229940113088 dimethylacetamide Drugs 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 abstract 1
- 125000000325 methylidene group Chemical group [H]C([H])=* 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- HXJUTPCZVOIRIF-UHFFFAOYSA-N sulfolane Chemical compound O=S1(=O)CCCC1 HXJUTPCZVOIRIF-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
- C07D317/44—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 ortho- or peri-condensed with carbocyclic rings or ring systems
- C07D317/46—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 ortho- or peri-condensed with carbocyclic rings or ring systems condensed with one six-membered ring
- C07D317/48—Methylenedioxybenzenes or hydrogenated methylenedioxybenzenes, unsubstituted on the hetero ring
- C07D317/50—Methylenedioxybenzenes or hydrogenated methylenedioxybenzenes, unsubstituted on the hetero ring with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to atoms of the carbocyclic ring
- C07D317/54—Radicals substituted by oxygen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
- C07D317/44—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 ortho- or peri-condensed with carbocyclic rings or ring systems
- C07D317/46—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 ortho- or peri-condensed with carbocyclic rings or ring systems condensed with one six-membered ring
- C07D317/48—Methylenedioxybenzenes or hydrogenated methylenedioxybenzenes, unsubstituted on the hetero ring
- C07D317/50—Methylenedioxybenzenes or hydrogenated methylenedioxybenzenes, unsubstituted on the hetero ring with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to atoms of the carbocyclic ring
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
Priority Applications (9)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB43418/65A GB1097270A (en) | 1965-10-13 | 1965-10-13 | Process for the preparation of methylene dioxybenzene, 1,3-benzoxathiole and derivatives thereof |
NL6614265A NL6614265A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1965-10-13 | 1966-10-11 | |
SE13698/66A SE316782B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1965-10-13 | 1966-10-11 | |
DK525566AA DK111896B (da) | 1965-10-13 | 1966-10-11 | Fremgangsmåde til fremstilling af methylendioxybenzen eller 1,3-benzoxathiol eller derivater deraf. |
BE688089D BE688089A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1965-10-13 | 1966-10-11 | |
CH1472866A CH467769A (de) | 1965-10-13 | 1966-10-11 | Verfahren zur Herstellung aromatischer Verbindungen |
DE19661543880 DE1543880C3 (de) | 1965-10-13 | 1966-10-11 | Verfahren zur Herstellung von Benzo- oder Naphtho-dioxolen bzw. -oxathiolen |
FR79455A FR1502914A (fr) | 1965-10-13 | 1966-10-11 | Procédé de préparation de composés aromatiques contenant un système hétérocyclique |
US586036A US3436403A (en) | 1965-10-13 | 1966-10-12 | Methylenation method |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB43418/65A GB1097270A (en) | 1965-10-13 | 1965-10-13 | Process for the preparation of methylene dioxybenzene, 1,3-benzoxathiole and derivatives thereof |
GB4341866 | 1966-08-26 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1097270A true GB1097270A (en) | 1968-01-03 |
Family
ID=26265141
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB43418/65A Expired GB1097270A (en) | 1965-10-13 | 1965-10-13 | Process for the preparation of methylene dioxybenzene, 1,3-benzoxathiole and derivatives thereof |
Country Status (8)
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2000336086A (ja) * | 1999-04-30 | 2000-12-05 | Endura Spa | 5−アルキルベンゾジオキソールの合成法 |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3528992A (en) * | 1965-10-28 | 1970-09-15 | Weldon M Padgett | Naphthoxathioles |
US3922285A (en) * | 1971-03-26 | 1975-11-25 | Hoffmann La Roche | Process for the methylenation of catechols |
US4082774A (en) * | 1974-07-11 | 1978-04-04 | Eli Lilly And Company | Methylenedioxybenzene -- improved method of preparation |
US4031257A (en) * | 1975-07-08 | 1977-06-21 | International Flavors & Fragrances Inc. | Use in foodstuff flavoring compositions of five or six membered heterocylic oxathio compounds |
US4548951A (en) * | 1983-04-21 | 1985-10-22 | Syntex (U.S.A.) Inc. | Hypotensive benzoxathiole pyrrolidines |
IT1291320B1 (it) * | 1997-05-08 | 1999-01-07 | Borregaard Italia Spa | Procedimento per la preparazione di composti aromatici contenenti un sistema eterociclico |
IT1304513B1 (it) * | 1998-12-30 | 2001-03-19 | Endura Spa | Processo per la sintesi di 5-(alfa-idrossialchil)benzo(1,3)diossoli. |
WO2017158404A1 (en) * | 2016-03-12 | 2017-09-21 | Anthea Aromatics Private Limited | An improved method for the preparation of alkylenedioxybenzene compounds |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2979513A (en) * | 1957-06-10 | 1961-04-11 | Firestone Tire & Rubber Co | 2-mercaptohydroquinone condensation products |
-
1965
- 1965-10-13 GB GB43418/65A patent/GB1097270A/en not_active Expired
-
1966
- 1966-10-11 BE BE688089D patent/BE688089A/xx unknown
- 1966-10-11 DK DK525566AA patent/DK111896B/da unknown
- 1966-10-11 NL NL6614265A patent/NL6614265A/xx unknown
- 1966-10-11 CH CH1472866A patent/CH467769A/de unknown
- 1966-10-11 SE SE13698/66A patent/SE316782B/xx unknown
- 1966-10-11 FR FR79455A patent/FR1502914A/fr not_active Expired
- 1966-10-12 US US586036A patent/US3436403A/en not_active Expired - Lifetime
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2000336086A (ja) * | 1999-04-30 | 2000-12-05 | Endura Spa | 5−アルキルベンゾジオキソールの合成法 |
Also Published As
Publication number | Publication date |
---|---|
SE316782B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1969-11-03 |
DK111896B (da) | 1968-10-21 |
NL6614265A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1967-04-14 |
US3436403A (en) | 1969-04-01 |
DE1543880A1 (de) | 1970-01-02 |
FR1502914A (fr) | 1967-11-24 |
DE1543880B2 (de) | 1975-10-16 |
CH467769A (de) | 1969-01-31 |
BE688089A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1967-04-11 |
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