GB1086782A - Process for manufacturing polyisocyanates - Google Patents

Process for manufacturing polyisocyanates

Info

Publication number
GB1086782A
GB1086782A GB740065A GB740065A GB1086782A GB 1086782 A GB1086782 A GB 1086782A GB 740065 A GB740065 A GB 740065A GB 740065 A GB740065 A GB 740065A GB 1086782 A GB1086782 A GB 1086782A
Authority
GB
United Kingdom
Prior art keywords
diisocyanate
manufacture
reaction
polyisocyanates
manufacturing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB740065A
Inventor
Adnan Abdul Rida Sayigh
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Pharmacia and Upjohn Co
Original Assignee
Upjohn Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Upjohn Co filed Critical Upjohn Co
Priority to GB740065A priority Critical patent/GB1086782A/en
Publication of GB1086782A publication Critical patent/GB1086782A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene

Abstract

In the manufacture of aliphatic, cycloaliphatic or araliphatic di- or poly-isocyanates by reaction of the corresponding amines or their hydrochlorides with phosgene in the presence of an inert solvent, the reaction is effected at 120-128 DEG C. and the proportion of solvent, by weight, to amine is 18-30 : 1. Specified solvents are chlorobenzene, o-dichlorobenzene, benzene, toluene, xylene, n-octane and anisole. Examples are given of the manufacture of m-xylylene diisocyanate, p-1,8-menthane diisocyanate, hexamethylene diisocyanate, 4,6-dimethyl-1,3 xylylene diisocyanate, pentamethylene diisocyanate, nonamethylene diisocyanate and decamethylene diisocyanate.
GB740065A 1965-02-19 1965-02-19 Process for manufacturing polyisocyanates Expired GB1086782A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB740065A GB1086782A (en) 1965-02-19 1965-02-19 Process for manufacturing polyisocyanates

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB740065A GB1086782A (en) 1965-02-19 1965-02-19 Process for manufacturing polyisocyanates

Publications (1)

Publication Number Publication Date
GB1086782A true GB1086782A (en) 1967-10-11

Family

ID=9832395

Family Applications (1)

Application Number Title Priority Date Filing Date
GB740065A Expired GB1086782A (en) 1965-02-19 1965-02-19 Process for manufacturing polyisocyanates

Country Status (1)

Country Link
GB (1) GB1086782A (en)

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0424836A1 (en) * 1989-10-23 1991-05-02 MITSUI TOATSU CHEMICALS, Inc. Preparation process of aliphatic isocyanates
US5136086A (en) * 1989-10-23 1992-08-04 Mitsui Toatsu Chemicals, Inc. Preparation process of aliphatic isocyanate
US8183407B2 (en) 2005-07-22 2012-05-22 Mitsui Chemicals, Inc. Process for production of isocyanate, isocyanate produced by the process, and use of the isocyanate
US8455695B2 (en) 2010-05-07 2013-06-04 Dow Global Technologies Llc Process for the production of aliphatic isocyanates
CN105218422A (en) * 2015-10-16 2016-01-06 万华化学集团股份有限公司 A kind of preparation method of isocyanic ester
CN106496073A (en) * 2016-09-27 2017-03-15 江苏嘉隆化工有限公司 A kind of preparation method of MXDI
CN107337615A (en) * 2016-08-09 2017-11-10 万华化学集团股份有限公司 A kind of preparation method of isocyanates
CN108586705A (en) * 2017-05-17 2018-09-28 Skc株式会社 Optical mirror slip with improved stability and reactive benzene dimethylene diisocyanate composition and use the composition
WO2018190290A1 (en) 2017-04-10 2018-10-18 三井化学株式会社 Xylylene diisocyanate composition, xylylene diisocyanate modification composition, two-component resin starting material, and resin
CN111132960A (en) * 2017-09-11 2020-05-08 韩华思路信(株) Process for preparing aliphatic isocyanates
US11254783B2 (en) 2017-04-10 2022-02-22 Mitsui Chemicals, Inc. Xylylenediisocyanate composition, xylylenediisocyanate-modified composition, two-component resin material, and resin

Cited By (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5136086A (en) * 1989-10-23 1992-08-04 Mitsui Toatsu Chemicals, Inc. Preparation process of aliphatic isocyanate
EP0424836A1 (en) * 1989-10-23 1991-05-02 MITSUI TOATSU CHEMICALS, Inc. Preparation process of aliphatic isocyanates
US8183407B2 (en) 2005-07-22 2012-05-22 Mitsui Chemicals, Inc. Process for production of isocyanate, isocyanate produced by the process, and use of the isocyanate
US9045395B2 (en) 2009-05-06 2015-06-02 Dow Global Technologies Llc Process for the production of aliphatic isocyanates
US8455695B2 (en) 2010-05-07 2013-06-04 Dow Global Technologies Llc Process for the production of aliphatic isocyanates
CN105218422A (en) * 2015-10-16 2016-01-06 万华化学集团股份有限公司 A kind of preparation method of isocyanic ester
CN107337615B (en) * 2016-08-09 2019-04-23 万华化学集团股份有限公司 A kind of preparation method of isocyanates
CN107337615A (en) * 2016-08-09 2017-11-10 万华化学集团股份有限公司 A kind of preparation method of isocyanates
CN106496073A (en) * 2016-09-27 2017-03-15 江苏嘉隆化工有限公司 A kind of preparation method of MXDI
US10640605B2 (en) 2017-04-10 2020-05-05 Mitsui Chemicals, Inc. Xylylenediisocyanate composition, xylylenediisocyanate-modified composition, two-component resin material, and resin
CN109153637A (en) * 2017-04-10 2019-01-04 三井化学株式会社 The modified compositions of xylylene diisocyanate composition, xylylene diisocyanate, two-liquid type resin raw material and resin
WO2018190290A1 (en) 2017-04-10 2018-10-18 三井化学株式会社 Xylylene diisocyanate composition, xylylene diisocyanate modification composition, two-component resin starting material, and resin
CN109153637B (en) * 2017-04-10 2020-12-08 三井化学株式会社 Xylylene diisocyanate composition, xylylene diisocyanate modified product composition, two-pack type resin raw material, and resin
CN112409569A (en) * 2017-04-10 2021-02-26 三井化学株式会社 Xylylene diisocyanate composition, xylylene diisocyanate modified product composition, two-pack type resin raw material, and resin
US11254783B2 (en) 2017-04-10 2022-02-22 Mitsui Chemicals, Inc. Xylylenediisocyanate composition, xylylenediisocyanate-modified composition, two-component resin material, and resin
CN108586705A (en) * 2017-05-17 2018-09-28 Skc株式会社 Optical mirror slip with improved stability and reactive benzene dimethylene diisocyanate composition and use the composition
CN111132960A (en) * 2017-09-11 2020-05-08 韩华思路信(株) Process for preparing aliphatic isocyanates

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