GB1068547A - Metal carbonate overbased lubricant detergent-dispersants - Google Patents
Metal carbonate overbased lubricant detergent-dispersantsInfo
- Publication number
- GB1068547A GB1068547A GB46348/64A GB4634864A GB1068547A GB 1068547 A GB1068547 A GB 1068547A GB 46348/64 A GB46348/64 A GB 46348/64A GB 4634864 A GB4634864 A GB 4634864A GB 1068547 A GB1068547 A GB 1068547A
- Authority
- GB
- United Kingdom
- Prior art keywords
- polyamine
- alkenyl succinic
- reaction product
- succinic anhydride
- dispersant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
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- C10M159/00—Lubricating compositions characterised by the additive being of unknown or incompletely defined constitution
- C10M159/12—Reaction products
- C10M159/20—Reaction mixtures having an excess of neutralising base, e.g. so-called overbasic or highly basic products
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- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/22—Organic compounds containing nitrogen
- C10L1/221—Organic compounds containing nitrogen compounds of uncertain formula; reaction products where mixtures of compounds are obtained
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- C10M2201/062—Oxides; Hydroxides; Carbonates or bicarbonates
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Abstract
An overbased detergent-dispersant suitable for oil compositions is obtained by the action of carbon dioxide on alkali metal oxides, alkali metal hydroxides, alkaline earth metal oxides or alkaline earth metal hydroxides in the presence of a dispersant, which is one of: the reaction product of an alkenyl succinic anhydride with a polyamine, the reaction product of an alkenyl succinic anhydride with a polyamine and a carboxylic acid, the reaction product of an alkenyl succinic anhydride with a polyhydric alcohol or an alkanolamine and subsequently with a polyamine or the product obtained by further reacting the reaction product of an alkenyl succinic anhydride and a polyamine and a carboxylic acid with a phosphosulphurized hydrocarbon or a dialkyl dithiophosphoric acid. The compositions may contain 10-35% by weight of metal carbonate and 5-50% of dispersant as above. In lubricating oil (mineral or synthetic) compositions from 0.001-10% of detergent-dispersant may be employed. Fuel compositions may be a major proportion of middle distillate fuel and 0.002 to 2% of the detergent dispersant. Other conventional ingredients are specified.ALSO:Compositions comprising colloidal alkali metal or alkaline earth metal carbonates are prepared by the action of carbon dioxide on alkali metal oxides, alkali metal hydroxides, alkaline earth metal oxides or alkaline earth metal hydroxides in the presence of a dispersant which is one of, the reaction product of an alkenyl succinic anhydride with a polyamine, the reaction product of an alkenyl succinic anhydride with a polyamine and a carboxylic acid, the reaction product of an alkenyl succinic anhydride with a polyhydric alcohol or an alkanolamine and subsequently with a polyamine, or the product obtained by further reacting the reaction product of an alkenyl succinic anhydride and a polyamine and a carboxylic acid with a phosphosulphurized hydrocarbon or a dialkyl dithiophosphoric acid. The alkenyl succinic anhydrides may contain alkenyl groups containing a total of 40-250 carbon atoms, such as polymers of C2 to C5 monoolefins with molecular weights of from 500-3,500, e.g. polymers of propylene or isobutylene of molecular weight 700-1,700. The aliphatic polyamine may be diethylene triamine, tetraethylene pentamine, octaethylene nonamine and tetrapropylene pentamine and may be of general formula <FORM:1068547/C1/1> where n is 2 or 3 and m is from 0 to 10. N-amino alkyl piperazines and mixtures of each of the above may be used. The carboxylic acid may be acetic, fumaric, adipic, lauric, oleic, linoleic or stearic acids. The polyhydric alcohols may be ethylene glycol, butanediol-1-4, pentanediol-1-5, octylene glycol and polyalkylene glycols such as polyethylene glycols and polypropylene glycols. The alkanolamines include triethanolamine and diethanolamine. The phosphosulphurized hydrocarbon may be polyisobutylene. The preparation is carried out in a mixture of dispersant and oil in the presence of a polar material, e.g. water. Auxiliary surface-active agents may be present in the preparation, such as, amyl phenol, octyl phenol, nonyl phenol, benzoic acid, oleic acid, tall oil fatty acids, isopropanolamine, ethylene diamine and diethylene triamine. Two methods are described. First, a high-speed mixing blend of the anhydride derivative and any auxiliary agent, 1-15 weight per cent, is prepared in hydrocarbon oil, e.g. light lubricating oil, 20-80 weight per cent, at 30-200 DEG F. and high-speed stirring is applied, the metal compound 10-50 weight per cent is added gradually and CO2 is passed at 400-500 DEG F. The mixture is dehydrated at 200-400 DEG F. and filtered at 100-400 DEG F. In a second method, a C1 to C3 aliphatic alcohol is dispersed in a liquid hydrocarbon at ambient temperature (droplets of smaller than 400 <\>pA), heated to 100-250 DEG F., the oxide or hydroxide is added, CO2 is passed at 125-300 DEG F. and water is removed by sparging with an inert gas such as nitrogen at 200-400 DEG F. Passage of CO2 takes 1.5 to 2.5 hours until exit gas shows unreacted CO2 exceeds 90%. The oxides and hydroxides may be those of sodium, potassium, lithium, barium, strontium, calcium and magnesium and mixtures thereof.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
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US33361463A | 1963-12-26 | 1963-12-26 | |
US57597166A | 1966-08-30 | 1966-08-30 |
Publications (1)
Publication Number | Publication Date |
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GB1068547A true GB1068547A (en) | 1967-05-10 |
Family
ID=26988815
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB46348/64A Expired GB1068547A (en) | 1963-12-26 | 1964-11-13 | Metal carbonate overbased lubricant detergent-dispersants |
Country Status (2)
Country | Link |
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US (1) | US3451931A (en) |
GB (1) | GB1068547A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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EP0737736A2 (en) * | 1995-04-06 | 1996-10-16 | The Lubrizol Corporation | Non-conventional overbased materials |
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US3624115A (en) * | 1966-10-10 | 1971-11-30 | Mobil Oil Corp | Coordinated complexes of nitrogenous compounds |
US3525599A (en) * | 1967-10-25 | 1970-08-25 | Continental Oil Co | Barium-containing dispersion |
GB1121578A (en) * | 1967-11-06 | 1968-07-31 | Lubrizol Corp | Reaction products of high molecular weight hydrocarbon succinic acid compounds, amines and heavy metal compounds |
US3764536A (en) * | 1971-10-14 | 1973-10-09 | Texaco Inc | Overbased calcium salts of alkenylsuccinimide |
FR2271281B2 (en) * | 1974-03-29 | 1977-01-21 | Inst Francais Du Petrole | |
US4123368A (en) * | 1977-03-24 | 1978-10-31 | Rohm And Haas Company | Alkaline earth metal salt dispersions in acrylic polymers |
CA1118750A (en) * | 1978-08-01 | 1982-02-23 | Ernst L. Neustadter | Lubricating composition |
CA1143719A (en) * | 1978-12-26 | 1983-03-29 | Ronald J. Vaughan | Lubricating oil composition containing a metal salt |
US4306983A (en) * | 1979-03-26 | 1981-12-22 | Nalco Chemical Company | Process for preparing overbased magnesium sulfonates |
US4347147A (en) * | 1980-09-04 | 1982-08-31 | Nalco Chemical Company | Process for preparing overbased magnesium sulfonates |
US4388244A (en) * | 1981-06-09 | 1983-06-14 | Ashland Oil, Inc. | Petrolatum or hydrocarbon wax oxidate composition |
FR2521158A1 (en) * | 1982-02-05 | 1983-08-12 | Inst Francais Du Petrole | PROCESS FOR THE PREPARATION OF CALCIUM-ORGANO-SOLUBLE COMPLEXES, THE COMPLEXES OBTAINED AND THEIR USE, IN PARTICULAR AS ADDITIVES FOR IMPROVING THE COMBUSTION OF GASES AND FUEL OILS |
US4491535A (en) * | 1983-05-25 | 1985-01-01 | Ashland Oil, Inc. | Hydrocarbon oxidate composition |
US4647387A (en) * | 1985-04-11 | 1987-03-03 | Witco Chemical Corp. | Succinic anhydride promoter overbased magnesium sulfonates and oils containing same |
US4997594A (en) * | 1985-10-25 | 1991-03-05 | The Lubrizol Corporation | Compositions, concentrates, lubricant compositions, fuel compositions and methods for improving fuel economy of internal combustion engines |
US4866135A (en) * | 1986-10-07 | 1989-09-12 | Exxon Chemical Patents Inc. | Heterocyclic amine terminated, lactone modified, aminated viscosity modifiers of improved dispersancy |
US5652201A (en) * | 1991-05-29 | 1997-07-29 | Ethyl Petroleum Additives Inc. | Lubricating oil compositions and concentrates and the use thereof |
US7316522B2 (en) * | 2005-03-10 | 2008-01-08 | Guntert & Zimmerman Const. Div., Inc. | Concrete placer/spreader having roll in/roll out conveyor |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3321399A (en) * | 1961-10-20 | 1967-05-23 | Exxon Research Engineering Co | Preparation of oil dispersions of metal carbonates |
USRE26433E (en) * | 1963-12-11 | 1968-08-06 | Amide and imide derivatives of metal salts of substituted succinic acids | |
NL130536C (en) * | 1964-05-19 | |||
GB1052380A (en) * | 1964-09-08 | |||
US3342733A (en) * | 1964-10-05 | 1967-09-19 | Exxon Research Engineering Co | Preparation of colloidal carbonates in hydrocarbon media |
-
1964
- 1964-11-13 GB GB46348/64A patent/GB1068547A/en not_active Expired
-
1966
- 1966-08-30 US US575971A patent/US3451931A/en not_active Expired - Lifetime
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0737736A2 (en) * | 1995-04-06 | 1996-10-16 | The Lubrizol Corporation | Non-conventional overbased materials |
EP0737736A3 (en) * | 1995-04-06 | 1998-01-28 | The Lubrizol Corporation | Non-conventional overbased materials |
Also Published As
Publication number | Publication date |
---|---|
US3451931A (en) | 1969-06-24 |
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