GB1066938A - Process for drying heat-sensitive materials as well as drying apparatus for the performance of the afore-mentioned process - Google Patents
Process for drying heat-sensitive materials as well as drying apparatus for the performance of the afore-mentioned processInfo
- Publication number
- GB1066938A GB1066938A GB16598/65A GB1659865A GB1066938A GB 1066938 A GB1066938 A GB 1066938A GB 16598/65 A GB16598/65 A GB 16598/65A GB 1659865 A GB1659865 A GB 1659865A GB 1066938 A GB1066938 A GB 1066938A
- Authority
- GB
- United Kingdom
- Prior art keywords
- particles
- compartment
- wall
- vapours
- drying
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/24—Extraction of coffee; Coffee extracts; Making instant coffee
- A23F5/28—Drying or concentrating coffee extract
- A23F5/34—Drying or concentrating coffee extract by spraying into a gas stream
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C1/00—Concentration, evaporation or drying
- A23C1/04—Concentration, evaporation or drying by spraying into a gas stream
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C1/00—Concentration, evaporation or drying
- A23C1/06—Concentration by freezing out the water
- A23C1/08—Freeze-drying
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/24—Extraction of coffee; Coffee extracts; Making instant coffee
- A23F5/28—Drying or concentrating coffee extract
- A23F5/32—Drying or concentrating coffee extract by lyophilisation
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
- A23L2/08—Concentrating or drying of juices
- A23L2/12—Concentrating or drying of juices by freezing
- A23L2/14—Concentrating or drying of juices by freezing and sublimation
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/40—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by drying or kilning; Subsequent reconstitution
- A23L3/44—Freeze-drying
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/40—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by drying or kilning; Subsequent reconstitution
- A23L3/46—Spray-drying
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/16—Evaporating by spraying
- B01D1/18—Evaporating by spraying to obtain dry solids
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B17/00—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement
- F26B17/10—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement with movement performed by fluid currents, e.g. issuing from a nozzle, e.g. pneumatic, flash, vortex or entrainment dryers
- F26B17/101—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement with movement performed by fluid currents, e.g. issuing from a nozzle, e.g. pneumatic, flash, vortex or entrainment dryers the drying enclosure having the shape of one or a plurality of shafts or ducts, e.g. with substantially straight and vertical axis
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B3/00—Drying solid materials or objects by processes involving the application of heat
- F26B3/02—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air
- F26B3/10—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour carrying the materials or objects to be dried with it
- F26B3/12—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour carrying the materials or objects to be dried with it in the form of a spray, i.e. sprayed or dispersed emulsions or suspensions
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B5/00—Drying solid materials or objects by processes not involving the application of heat
- F26B5/04—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
- F26B5/048—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum in combination with heat developed by electro-magnetic means, e.g. microwave energy
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B5/00—Drying solid materials or objects by processes not involving the application of heat
- F26B5/04—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
- F26B5/06—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum the process involving freezing
- F26B5/065—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum the process involving freezing the product to be freeze-dried being sprayed, dispersed or pulverised
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S159/00—Concentrating evaporators
- Y10S159/06—Infrared
Landscapes
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Nutrition Science (AREA)
- Molecular Biology (AREA)
- Microbiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Drying Of Solid Materials (AREA)
- Freezing, Cooling And Drying Of Foods (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
1,066,938. Drying foods &c. F. ANDERWERT. April 20, 1965 [April 24, 1964], No. 16598/65. Heading A2D. [Also in Divisions B2 and F4] In apparatus for drying heat-sensitive, atomizable materials, e.g. milk, fruit juices, aroma-rich extracts, in particle form produced either by pre-freezing liquid material in apparatus described with reference to Fig. 4 (not shown), or by delivery through atomizer or sprayer means 18 into a compartment 1 evacuated by a pump 9 and having a heat radiating wall 2, the particles fall by gravity through the chamber and are prevented from contacting the wall 2 by a mesh cylinder 10 coaxially mounted within the compartment. A vortex is formed within the compart ment by an agitator 14 with vanes 14<SP>1</SP> so that the vapours sublimed or evaporated from the particles are caused to flow through a vapour conduit leading to the pump 9 and the dried particles separated therefrom are removed through a valved base 5. A temperature sensing device41 may control the quantity of radiant energy and/or the speed of delivery of the particles to the apparatus as a function of the temperature of the vapour stream. A portion of the vapours from the conduit or condenser 8 therein is delivered by a blower 12 to the annular compartment lb formed between the wall 2 and cylinder 10 and into the compartment 1 to prevent particles contacting the wall 2. In a modification, Fig. 2 (not shown) the agitator 14 is replaced by tangentially introducing the vapours from the blower 12 and the radiant walls in the embodiments of Figs. 2 and 3 may have areas at different temperatures.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH534764A CH408781A (en) | 1964-04-24 | 1964-04-24 | Process for drying atomizable material by sublimation and drying device for carrying out the process |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1066938A true GB1066938A (en) | 1967-04-26 |
Family
ID=4292049
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB16598/65A Expired GB1066938A (en) | 1964-04-24 | 1965-04-20 | Process for drying heat-sensitive materials as well as drying apparatus for the performance of the afore-mentioned process |
Country Status (6)
Country | Link |
---|---|
US (1) | US3300868A (en) |
CH (1) | CH408781A (en) |
DE (1) | DE1604768A1 (en) |
ES (1) | ES312609A1 (en) |
GB (1) | GB1066938A (en) |
NL (1) | NL6505303A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2270409A1 (en) * | 2008-03-19 | 2011-01-05 | Morimoto-Pharma Co., Ltd. | Freeze-drying method and freeze-drying apparatus |
RU2646998C1 (en) * | 2017-06-26 | 2018-03-13 | Олег Савельевич Кочетов | Suspended layer dryer with inert attachment |
RU2647001C1 (en) * | 2017-06-29 | 2018-03-13 | Олег Савельевич Кочетов | Suspended layer dryer with inert attachment |
Families Citing this family (29)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3620776A (en) * | 1968-06-28 | 1971-11-16 | Nestle Sa | Spray drying process |
GB1288766A (en) * | 1969-01-30 | 1972-09-13 | ||
US3731392A (en) * | 1971-02-25 | 1973-05-08 | H Gottfried | Continuous freeze dryer |
US3880668A (en) * | 1972-04-05 | 1975-04-29 | Western Consumers Ind Inc | Apparatus for producing molasses food product |
US3847714A (en) * | 1972-06-15 | 1974-11-12 | Dasi Industries | Method and apparatus for heat treating liqueform materials |
US3837491A (en) * | 1972-11-03 | 1974-09-24 | Pollution Control Inc | Liquid purification apparatus and process |
US4284495A (en) * | 1979-12-10 | 1981-08-18 | Newton William A | Coating apparatus and method |
BR8600564A (en) * | 1985-02-11 | 1986-10-21 | Falvourtech Pty Ltd | CONTRA-CURRENT CONTACT DEVICE OR DISTILLATION COLUMN, SYSTEM TO REDUCE THE ALCOHOLIC CONTENT OF A DRINK CONTAINING ALCOHOL, SYSTEM TO REDUCE THE ALCOHOLIC CONTENT OF WINE, SYSTEM FOR REMOVING AROMA AND / OR TASTE OF FRUIT JUICE, DE-DESULFURIZING A LIQUID AND PROCESS TO DISTILL, DISTILL BY FRACTIONATION OR REMOVE A SELECTED VOLATILE COMPONENT, OR COMPONENTS OF A LIQUID |
FR2635273B1 (en) * | 1988-07-21 | 1990-11-30 | Faddi Etienne | PROCESS AND PLANT FOR SEPARATING COMPONENTS OF PLANT OR ANIMAL MATERIAL |
DE3829013A1 (en) * | 1988-08-26 | 1990-03-08 | Heraeus Schott Quarzschmelze | Thickening apparatus for jelly-like material |
JP2571890B2 (en) * | 1992-06-09 | 1997-01-16 | 株式会社 佐藤鉄工所 | Vacuum drying method and apparatus for neat soap |
US5744008A (en) * | 1996-01-02 | 1998-04-28 | Oceanit Laboratories, Inc. | Hurricane tower water desalination device |
US6168141B1 (en) * | 1999-03-22 | 2001-01-02 | Artur G. Zimmer | Apparatus for treatment of fluent materials |
WO2001063191A1 (en) * | 2000-02-25 | 2001-08-30 | Glatt Gmbh | Method for producing particulate goods |
US7575761B2 (en) * | 2000-06-30 | 2009-08-18 | Novartis Pharma Ag | Spray drying process control of drying kinetics |
DE10112167C2 (en) * | 2001-03-12 | 2003-02-13 | Bionorica Ag | Process for the gentle extraction of dry extracts |
JP3824891B2 (en) * | 2001-07-06 | 2006-09-20 | 共和真空技術株式会社 | Dry bulk crushing equipment in freeze-drying equipment for foods and pharmaceuticals |
DE102005022154A1 (en) * | 2005-05-13 | 2006-11-16 | Degussa Ag | Reactor and method for gentle product drying |
GB2434195B (en) * | 2006-01-12 | 2010-11-24 | Dyson Technology Ltd | Drying apparatus |
EP2101131A1 (en) * | 2007-12-31 | 2009-09-16 | Terruzzi Fercalx S.p.A. | Lyophilization method and system therefor |
CN103069240B (en) * | 2010-08-04 | 2015-06-17 | Ima生命北美股份有限公司 | Bulk freeze drying system and method using spray freezing and stirred drying |
US9945611B2 (en) | 2010-08-04 | 2018-04-17 | Ima Life North America Inc. | Bulk freeze drying using spray freezing and agitated drying |
SE1100493A1 (en) * | 2011-06-23 | 2012-12-24 | Dragoljub Perunicic | Cyclone distillery / refinery which has steam duct connected impeller / turbine |
JP5837670B2 (en) * | 2014-10-24 | 2015-12-24 | アイエムエー ライフ ノース アメリカ インコーポレーテッド | Bulk freeze drying using spray freezing and stirring drying |
DK3303958T3 (en) | 2015-06-01 | 2020-01-02 | Ima Life North America Inc | Mass bulk freeze drying using spray freezing and drying under agitation with heat |
EP4378572A3 (en) * | 2019-12-09 | 2024-08-07 | Grant Prideco, Inc. | Method for continuous thermal separation of a multi-component substance |
CN112197550A (en) * | 2020-10-09 | 2021-01-08 | 马鞍山健鼎化工有限公司 | Efficient drying device for producing polyaluminium chloride and working method |
CN112268432B (en) * | 2020-10-22 | 2021-06-01 | 盐城市科瑞达科技咨询服务有限公司 | Industrial dust dryer |
WO2024178110A1 (en) | 2023-02-22 | 2024-08-29 | Ima Life North America, Inc. | Direct contact spray freezing system |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US996832A (en) * | 1907-10-02 | 1911-07-04 | Charles H Campbell | Desiccating milk. |
US1104920A (en) * | 1911-09-27 | 1914-07-28 | Osborne Patented Machinery Co Inc | Art of making ice. |
US1976204A (en) * | 1932-01-08 | 1934-10-09 | Standard Oil Co | Process of making ice |
US2020719A (en) * | 1934-06-12 | 1935-11-12 | Girdler Corp | Process and apparatus for solidifying material in finely subdivided form |
US2471035A (en) * | 1943-10-02 | 1949-05-24 | Frank E Hurd | Apparatus for the desiccation of organic substances |
US2515098A (en) * | 1945-08-01 | 1950-07-11 | Chain Belt Co | Continuous low-temperature dehydration |
US2533125A (en) * | 1946-02-16 | 1950-12-05 | Michael Reese Res Foundation | Apparatus for desiccation by ice sublimation |
US2751687A (en) * | 1952-05-21 | 1956-06-26 | Proctor Drying And Freezing Co | Process and apparatus for producing stabilized products |
US2800463A (en) * | 1953-05-14 | 1957-07-23 | Shawinigan Resins Corp | Polyvinyl acetate powder and process of making the same |
US2813350A (en) * | 1954-03-12 | 1957-11-19 | Commw Eugineering Company Of O | Process for concentration of solutions by sublimation |
US3024117A (en) * | 1958-11-17 | 1962-03-06 | Bar Rup Corp | Method of freezing citrus fruit juices |
-
1964
- 1964-04-24 CH CH534764A patent/CH408781A/en unknown
-
1965
- 1965-04-16 US US448668A patent/US3300868A/en not_active Expired - Lifetime
- 1965-04-20 DE DE19651604768 patent/DE1604768A1/en active Pending
- 1965-04-20 GB GB16598/65A patent/GB1066938A/en not_active Expired
- 1965-04-23 ES ES0312609A patent/ES312609A1/en not_active Expired
- 1965-04-26 NL NL6505303A patent/NL6505303A/xx unknown
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2270409A1 (en) * | 2008-03-19 | 2011-01-05 | Morimoto-Pharma Co., Ltd. | Freeze-drying method and freeze-drying apparatus |
EP2270409A4 (en) * | 2008-03-19 | 2012-08-08 | Morimoto Pharma Co Ltd | Freeze-drying method and freeze-drying apparatus |
RU2646998C1 (en) * | 2017-06-26 | 2018-03-13 | Олег Савельевич Кочетов | Suspended layer dryer with inert attachment |
RU2647001C1 (en) * | 2017-06-29 | 2018-03-13 | Олег Савельевич Кочетов | Suspended layer dryer with inert attachment |
Also Published As
Publication number | Publication date |
---|---|
US3300868A (en) | 1967-01-31 |
CH408781A (en) | 1966-02-28 |
ES312609A1 (en) | 1966-01-01 |
DE1604768A1 (en) | 1970-01-29 |
NL6505303A (en) | 1965-10-25 |
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