GB1049351A - Method of preparing dry powdered poly-1-butene - Google Patents
Method of preparing dry powdered poly-1-buteneInfo
- Publication number
- GB1049351A GB1049351A GB946865A GB946865A GB1049351A GB 1049351 A GB1049351 A GB 1049351A GB 946865 A GB946865 A GB 946865A GB 946865 A GB946865 A GB 946865A GB 1049351 A GB1049351 A GB 1049351A
- Authority
- GB
- United Kingdom
- Prior art keywords
- temperature
- solvent
- polybutene
- butene
- powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/18—Homopolymers or copolymers of hydrocarbons having four or more carbon atoms
- C08L23/20—Homopolymers or copolymers of hydrocarbons having four or more carbon atoms having four to nine carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/06—Treatment of polymer solutions
- C08F6/12—Separation of polymers from solutions
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
Abstract
Solvent-free polybutene-1 is obtained by cooling a solution of 15 to 40% by weight of polybutene-1 in a liquid hydrocarbon solvent to a temperature of from 15 DEG to 35 DEG C., maintaining the solution within this temperature range until at least 75% of the polymer has precipitated, milling the wet mass, and then drying the wet flaky powder by progressively heating to 90 DEG C., the temperature of the powder during such heating being kept below the temperature at which the grains of the powder reagglomerate in the presence of the solvent that they still contain. In order to increase the isotactic content of the polymer part of the solvent containing atactic polybutene may be removed after cooling but before milling.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR966351 | 1964-03-06 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1049351A true GB1049351A (en) | 1966-11-23 |
Family
ID=8824859
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB946865A Expired GB1049351A (en) | 1964-03-06 | 1965-03-05 | Method of preparing dry powdered poly-1-butene |
Country Status (4)
Country | Link |
---|---|
BE (1) | BE660701A (en) |
DE (1) | DE1570502A1 (en) |
GB (1) | GB1049351A (en) |
NL (1) | NL6502842A (en) |
-
1965
- 1965-03-05 DE DE19651570502 patent/DE1570502A1/en active Pending
- 1965-03-05 BE BE660701D patent/BE660701A/xx unknown
- 1965-03-05 NL NL6502842A patent/NL6502842A/xx unknown
- 1965-03-05 GB GB946865A patent/GB1049351A/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
DE1570502A1 (en) | 1970-02-05 |
NL6502842A (en) | 1965-09-07 |
BE660701A (en) | 1965-07-01 |
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