GB1046012A - Process for the production of finely dispersed calcium silicate fillers - Google Patents

Process for the production of finely dispersed calcium silicate fillers

Info

Publication number
GB1046012A
GB1046012A GB2255963A GB2255963A GB1046012A GB 1046012 A GB1046012 A GB 1046012A GB 2255963 A GB2255963 A GB 2255963A GB 2255963 A GB2255963 A GB 2255963A GB 1046012 A GB1046012 A GB 1046012A
Authority
GB
United Kingdom
Prior art keywords
calcium silicate
sio2
cao
water glass
hcl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2255963A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer AG
Original Assignee
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer AG filed Critical Bayer AG
Publication of GB1046012A publication Critical patent/GB1046012A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/20Silicates
    • C01B33/24Alkaline-earth metal silicates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/20Silicates
    • C01B33/22Magnesium silicates
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09CTREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIESĀ ; PREPARATION OF CARBON BLACKĀ  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28Compounds of silicon
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/02Amorphous compounds
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/70Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)

Abstract

Finely dispersed calcium silicate filler is prepared by mixing a calcium silicate of composition CaO.SiO2.H2O having a tobermorite crystal structure, with a calcium silicate of composition CaO.2-5SiO2.nH2O which is amorphous to X-rays, both calcium silicates being in a moist condition from precipitation, until a SiO2 : CaO ratio of 1.5 : 1 to 2.5 : 1 is attained, followed by filtering, washing, drying and possibly grinding. The product has the disturbed crystal structure of synthetic tobermorite and X-ray diffraction lines at 3.06, 2.79, 1.83 and 1.66 <\>rA. The CaO.SiO2.H2O may be obtained by reacting milk of lime with (a) an unaged silica sol (obtained from water glass and HCl) or (b) silicate solution with HCl or CaCl2; then heating and stirring until the mixture becomes transparent, viscosity rises, and pH falls. The amorphous calcium silicate may be obtained by reacting CaCl2 with water glass solution, e.g. Na2O.3.3SiO2 or disilicates of lower SiO2 content, using high or low shearing force; SiO2 content may be increased by HCl treatment of the water glass or the calcium silicate.
GB2255963A 1962-06-06 1963-06-06 Process for the production of finely dispersed calcium silicate fillers Expired GB1046012A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEF37002A DE1184741B (en) 1962-06-06 1962-06-06 Process for the production of finely divided calcium silicate fillers

Publications (1)

Publication Number Publication Date
GB1046012A true GB1046012A (en) 1966-10-19

Family

ID=7096701

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2255963A Expired GB1046012A (en) 1962-06-06 1963-06-06 Process for the production of finely dispersed calcium silicate fillers

Country Status (2)

Country Link
DE (1) DE1184741B (en)
GB (1) GB1046012A (en)

Also Published As

Publication number Publication date
DE1184741B (en) 1965-01-07

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