FR3014441B1 - Procede de preparation de prepolymeres a terminaison isocyanate pour la preparation de polyurethanes - Google Patents

Procede de preparation de prepolymeres a terminaison isocyanate pour la preparation de polyurethanes

Info

Publication number
FR3014441B1
FR3014441B1 FR1362130A FR1362130A FR3014441B1 FR 3014441 B1 FR3014441 B1 FR 3014441B1 FR 1362130 A FR1362130 A FR 1362130A FR 1362130 A FR1362130 A FR 1362130A FR 3014441 B1 FR3014441 B1 FR 3014441B1
Authority
FR
France
Prior art keywords
preparation
isocyanate
polyurethanes
prepolymers
terminating
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR1362130A
Other languages
English (en)
Other versions
FR3014441A1 (fr
Inventor
Herve Trentesaux
Laure Rambahiniarison
Remi Buffard
Jean-Pierre Pascault
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Merylithe
Original Assignee
Merylithe
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Merylithe filed Critical Merylithe
Priority to FR1362130A priority Critical patent/FR3014441B1/fr
Priority to CN201480071822.7A priority patent/CN106133019A/zh
Priority to US15/101,681 priority patent/US20160304658A1/en
Priority to PCT/EP2014/076790 priority patent/WO2015082712A1/fr
Priority to EP14816152.4A priority patent/EP3077441A1/fr
Publication of FR3014441A1 publication Critical patent/FR3014441A1/fr
Application granted granted Critical
Publication of FR3014441B1 publication Critical patent/FR3014441B1/fr
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08Processes
    • C08G18/10Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
    • C08G18/12Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step using two or more compounds having active hydrogen in the first polymerisation step
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08Processes
    • C08G18/0895Manufacture of polymers by continuous processes
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30Low-molecular-weight compounds
    • C08G18/38Low-molecular-weight compounds having heteroatoms other than oxygen
    • C08G18/3819Low-molecular-weight compounds having heteroatoms other than oxygen having nitrogen
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30Low-molecular-weight compounds
    • C08G18/38Low-molecular-weight compounds having heteroatoms other than oxygen
    • C08G18/3819Low-molecular-weight compounds having heteroatoms other than oxygen having nitrogen
    • C08G18/3842Low-molecular-weight compounds having heteroatoms other than oxygen having nitrogen containing heterocyclic rings having at least one nitrogen atom in the ring
    • C08G18/3844Low-molecular-weight compounds having heteroatoms other than oxygen having nitrogen containing heterocyclic rings having at least one nitrogen atom in the ring containing one nitrogen atom in the ring
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30Low-molecular-weight compounds
    • C08G18/38Low-molecular-weight compounds having heteroatoms other than oxygen
    • C08G18/3855Low-molecular-weight compounds having heteroatoms other than oxygen having sulfur
    • C08G18/3863Low-molecular-weight compounds having heteroatoms other than oxygen having sulfur containing groups having sulfur atoms between two carbon atoms, the sulfur atoms being directly linked to carbon atoms or other sulfur atoms
    • C08G18/3865Low-molecular-weight compounds having heteroatoms other than oxygen having sulfur containing groups having sulfur atoms between two carbon atoms, the sulfur atoms being directly linked to carbon atoms or other sulfur atoms containing groups having one sulfur atom between two carbon atoms
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40High-molecular-weight compounds
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72Polyisocyanates or polyisothiocyanates
    • C08G18/74Polyisocyanates or polyisothiocyanates cyclic
    • C08G18/76Polyisocyanates or polyisothiocyanates cyclic aromatic
    • C08G18/7614Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72Polyisocyanates or polyisothiocyanates
    • C08G18/74Polyisocyanates or polyisothiocyanates cyclic
    • C08G18/76Polyisocyanates or polyisothiocyanates cyclic aromatic
    • C08G18/7614Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring
    • C08G18/7621Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring being toluene diisocyanate including isomer mixtures

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Polyurethanes Or Polyureas (AREA)

Abstract

Un procédé de préparation d'un prépolymère de polyuréthane à terminaison isocyanate comprenant une teneur en diisocyanates libres faible ainsi qu'un procédé de préparation de polyuréthanes, polyuréthane urée ou de granulés de polyuréthane thermoplastique sont décrits.
FR1362130A 2013-12-05 2013-12-05 Procede de preparation de prepolymeres a terminaison isocyanate pour la preparation de polyurethanes Expired - Fee Related FR3014441B1 (fr)

Priority Applications (5)

Application Number Priority Date Filing Date Title
FR1362130A FR3014441B1 (fr) 2013-12-05 2013-12-05 Procede de preparation de prepolymeres a terminaison isocyanate pour la preparation de polyurethanes
CN201480071822.7A CN106133019A (zh) 2013-12-05 2014-12-05 用于制备聚氨酯的具有异氰酸酯封端的预聚物的制备方法
US15/101,681 US20160304658A1 (en) 2013-12-05 2014-12-05 Method for producing prepolymers with an isocyanate termination for producing polyurethanes
PCT/EP2014/076790 WO2015082712A1 (fr) 2013-12-05 2014-12-05 Procede de preparation de prepolymeres a terminaison isocyanate pour la preparation de polyurethanes
EP14816152.4A EP3077441A1 (fr) 2013-12-05 2014-12-05 Procede de preparation de prepolymeres a terminaison isocyanate pour la preparation de polyurethanes

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1362130A FR3014441B1 (fr) 2013-12-05 2013-12-05 Procede de preparation de prepolymeres a terminaison isocyanate pour la preparation de polyurethanes

Publications (2)

Publication Number Publication Date
FR3014441A1 FR3014441A1 (fr) 2015-06-12
FR3014441B1 true FR3014441B1 (fr) 2016-01-08

Family

ID=50289888

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1362130A Expired - Fee Related FR3014441B1 (fr) 2013-12-05 2013-12-05 Procede de preparation de prepolymeres a terminaison isocyanate pour la preparation de polyurethanes

Country Status (5)

Country Link
US (1) US20160304658A1 (fr)
EP (1) EP3077441A1 (fr)
CN (1) CN106133019A (fr)
FR (1) FR3014441B1 (fr)
WO (1) WO2015082712A1 (fr)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108373528A (zh) * 2017-02-01 2018-08-07 胡海东 一种复合材料基体树脂
CN107383332B (zh) 2017-08-22 2020-07-03 广东电网有限责任公司电力科学研究院 一种聚氨酯聚合物及其制备方法和应用
CN114560991B (zh) * 2022-03-25 2023-10-20 华南理工大学 一种兼顾动态性能和阻尼性能的聚氨酯材料及其制备方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1993001222A1 (fr) * 1991-07-03 1993-01-21 Kanebo, Ltd. Elastomere de polyurethane thermoplastique, procede et dispositif de production, et fibre elastique realisee a partir de cet elastomere
DE4140660A1 (de) * 1991-12-10 1993-06-17 Bayer Ag Ether- und urethangruppen aufweisende polyisocyanate, ein verfahren zu ihrer herstellung und ihrer verwendung
DE19754885C1 (de) * 1997-12-10 1999-09-16 Basf Ag Verfahren zur kontinuierlichen Herstellung von Granulat aus thermoplastischen Polyurethan-Elastomeren
DE10229519A1 (de) * 2001-07-10 2003-01-30 Henkel Kgaa Reaktive Polyurethane mit einem geringen Gehalt an monomeren Diisocyanaten
DE102007025659A1 (de) * 2007-06-01 2008-12-11 Bayer Materialscience Ag NCO-Prepolymere mit niedrigem Gehalt an freiem monomerem Diisocyanat und ihre Herstellung
DE102011085944A1 (de) * 2010-11-10 2012-05-10 Bayer Materialscience Aktiengesellschaft Verfahren zur kontinuierlichen Herstellung von thermoplastisch verarbeitbaren Polyurethanen

Also Published As

Publication number Publication date
EP3077441A1 (fr) 2016-10-12
FR3014441A1 (fr) 2015-06-12
CN106133019A (zh) 2016-11-16
WO2015082712A1 (fr) 2015-06-11
US20160304658A1 (en) 2016-10-20

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Effective date: 20180831