FR2757842B1 - PROCESS AND PLANT FOR THE MANUFACTURE OF NITRATE OF POROUS AMMONIA - Google Patents

PROCESS AND PLANT FOR THE MANUFACTURE OF NITRATE OF POROUS AMMONIA

Info

Publication number
FR2757842B1
FR2757842B1 FR9616297A FR9616297A FR2757842B1 FR 2757842 B1 FR2757842 B1 FR 2757842B1 FR 9616297 A FR9616297 A FR 9616297A FR 9616297 A FR9616297 A FR 9616297A FR 2757842 B1 FR2757842 B1 FR 2757842B1
Authority
FR
France
Prior art keywords
nitrate
manufacture
plant
ammonium nitrate
porous
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR9616297A
Other languages
French (fr)
Other versions
FR2757842A1 (en
Inventor
Edmond Vogel
Jacques Monsterleet
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kaltenbach Thuring SA
Original Assignee
Kaltenbach Thuring SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR9616297A priority Critical patent/FR2757842B1/en
Application filed by Kaltenbach Thuring SA filed Critical Kaltenbach Thuring SA
Priority to PT97403033T priority patent/PT850878E/en
Priority to EP97403033A priority patent/EP0850878B1/en
Priority to ES97403033T priority patent/ES2160912T3/en
Priority to AT97403033T priority patent/ATE205810T1/en
Priority to DK97403033T priority patent/DK0850878T3/en
Priority to DE69706822T priority patent/DE69706822T2/en
Priority to CA002221717A priority patent/CA2221717C/en
Priority to AU48376/97A priority patent/AU729196B2/en
Priority to NO19976096A priority patent/NO319746B1/en
Priority to US09/000,549 priority patent/US6022386A/en
Publication of FR2757842A1 publication Critical patent/FR2757842A1/en
Application granted granted Critical
Publication of FR2757842B1 publication Critical patent/FR2757842B1/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C06—EXPLOSIVES; MATCHES
    • C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B31/00—Compositions containing an inorganic nitrogen-oxygen salt
    • C06B31/28—Compositions containing an inorganic nitrogen-oxygen salt the salt being ammonium nitrate
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/12—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic in rotating drums
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/16—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by suspending the powder material in a gas, e.g. in fluidised beds or as a falling curtain
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/18—Nitrates of ammonium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Fertilizers (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Compounds Of Unknown Constitution (AREA)
  • Manufacturing Of Micro-Capsules (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
  • Hydroponics (AREA)
  • Medicinal Preparation (AREA)
  • Glanulating (AREA)

Abstract

A process is claimed for the manufacture of porous ammonium nitrate granules using a rotary drum granulator with a fluidised bed. Caps of solid ammonium nitrate are introduced and a solution of 94 - 98% ammonium nitrate is sprayed at 135 - 170 degrees C. Part of the water in the course of granulation is removed by the heat of crystallisation of the nitrate and an airflow blown under the bed.The remaining water is eliminated in a drying operation after granulation. Also claimed is the installation for the process.
FR9616297A 1996-12-31 1996-12-31 PROCESS AND PLANT FOR THE MANUFACTURE OF NITRATE OF POROUS AMMONIA Expired - Fee Related FR2757842B1 (en)

Priority Applications (11)

Application Number Priority Date Filing Date Title
FR9616297A FR2757842B1 (en) 1996-12-31 1996-12-31 PROCESS AND PLANT FOR THE MANUFACTURE OF NITRATE OF POROUS AMMONIA
EP97403033A EP0850878B1 (en) 1996-12-31 1997-12-12 Process and installation for the production of porous ammonium nitrate
ES97403033T ES2160912T3 (en) 1996-12-31 1997-12-12 PROCEDURE AND INSTALLATION FOR THE PRODUCTION OF POROUS AMMONIA NITRATE.
AT97403033T ATE205810T1 (en) 1996-12-31 1997-12-12 METHOD AND PLANT FOR PRODUCING POROUS AMMONIUM NITRATE
DK97403033T DK0850878T3 (en) 1996-12-31 1997-12-12 Process and plant for the production of porous ammonium nitrate
DE69706822T DE69706822T2 (en) 1996-12-31 1997-12-12 Process and plant for the production of porous ammonium nitrate
PT97403033T PT850878E (en) 1996-12-31 1997-12-12 PROCESS AND INSTALLATION FOR THE MANUFACTURE OF POROUS AMMONIA NITRATE
CA002221717A CA2221717C (en) 1996-12-31 1997-12-16 Procedure and installation for the manufacture of porous ammonium nitrate
AU48376/97A AU729196B2 (en) 1996-12-31 1997-12-16 Process and plant for producing porous ammonium nitrate
NO19976096A NO319746B1 (en) 1996-12-31 1997-12-29 Process for the preparation of porous granules of ammonium nitrate
US09/000,549 US6022386A (en) 1996-12-31 1997-12-30 Process for producing porous ammonium nitrate and ammonium nitrates produced

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9616297A FR2757842B1 (en) 1996-12-31 1996-12-31 PROCESS AND PLANT FOR THE MANUFACTURE OF NITRATE OF POROUS AMMONIA

Publications (2)

Publication Number Publication Date
FR2757842A1 FR2757842A1 (en) 1998-07-03
FR2757842B1 true FR2757842B1 (en) 1999-11-19

Family

ID=9499370

Family Applications (1)

Application Number Title Priority Date Filing Date
FR9616297A Expired - Fee Related FR2757842B1 (en) 1996-12-31 1996-12-31 PROCESS AND PLANT FOR THE MANUFACTURE OF NITRATE OF POROUS AMMONIA

Country Status (11)

Country Link
US (1) US6022386A (en)
EP (1) EP0850878B1 (en)
AT (1) ATE205810T1 (en)
AU (1) AU729196B2 (en)
CA (1) CA2221717C (en)
DE (1) DE69706822T2 (en)
DK (1) DK0850878T3 (en)
ES (1) ES2160912T3 (en)
FR (1) FR2757842B1 (en)
NO (1) NO319746B1 (en)
PT (1) PT850878E (en)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB9811824D0 (en) * 1998-06-03 1998-07-29 Cooper John Modified ammonium nitrate
US6365120B1 (en) * 2000-02-28 2002-04-02 Lobeco Products, Inc. Method for hardening granular inorganic salt compounds
EP1343578A2 (en) * 2000-12-19 2003-09-17 The Lubrizol Corporation Aminosulfonate product-treated nitrogen-containing salt particles
UA98306C2 (en) * 2006-08-02 2012-05-10 Омния Фертилайзер Лимитед Ammonium nitrate granules and methods for producing thereof
CN100586906C (en) * 2007-09-20 2010-02-03 兖矿鲁南化肥厂 Production process for high tower roller composite fertilizer
CN104311372B (en) * 2014-10-22 2016-09-07 安徽淮化股份有限公司 Multi-hole nitramines lumps in producing the recycling device of ammonium nitrate and using method thereof
RU2591947C1 (en) * 2014-12-25 2016-07-20 Федеральное государственное бюджетное образовательное учреждение высшего образования "Московский технологический университет" Method of porous granulated ammonium nitrate producing
RU2642669C1 (en) * 2016-03-02 2018-01-25 Федеральное государственное бюджетное образовательное учреждение высшего образования "Московский технологический университет" Method for production of porous granular ammonium nitrate
RU2643950C2 (en) * 2016-07-15 2018-02-06 Федеральное Государственное Бюджетное Учреждение Науки Институт Проблем Комплексного Освоения Недр Им. Академика Н.В. Мельникова Российской Академии Наук (Ипкон Ран) Device for producing porous granulated ammonium nitrate
CN107892310B (en) * 2017-12-12 2023-10-24 天脊煤化工集团股份有限公司 System and process for preventing porous ammonium nitrate from caking

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2416615A (en) * 1943-06-19 1947-02-25 Solvay Process Co Process for graining ammonium nitrate
US2798301A (en) * 1954-07-06 1957-07-09 Phillips Petroleum Co Process for drying ammonium nitrate prills
GB894773A (en) * 1958-05-30 1962-04-26 Chemical & Ind Corp Process for the production of pellets
GB990487A (en) * 1962-11-28 1965-04-28 Ici Ltd Improvements in and relating to granular ammonium nitrate compositions
ES456079A1 (en) * 1977-02-18 1978-02-01 Saez Diaz Jesus M Drying process of ammonium porous nitrate for explosive in "prilling" plants through fluidized beds. (Machine-translation by Google Translate, not legally binding)
NL173387C (en) * 1979-03-15 1984-01-16 Azote Sa Cie Neerlandaise METHOD FOR MAKING STABLE AMMONIUM NITRATE CONTAINING FERTILIZER GRAINS.
NL8102958A (en) * 1981-06-19 1983-01-17 Unie Van Kunstmestfab Bv PROCESS FOR PREPARING THERMALLY STABLE AMMONIUM NITRATE-CONTAINING HIGH DUMP WEIGHT GRANULES, AND GRANULES OBTAINED BY THIS PROCESS.
NL8102957A (en) * 1981-06-19 1983-01-17 Unie Van Kunstmestfab Bv METHOD FOR PREPARING AMMONIUM NITRATE-CONTAINING HIGH DUMP WEIGHT GRANULES, AND GRANULES OBTAINED BY THIS METHOD
NL8102959A (en) * 1981-06-19 1983-01-17 Unie Van Kunstmestfab Bv METHOD FOR PREPARING THERMALLY STABLE AMMONIUM NITRATE-CONTAINING GRANULES, AND GRANULES OBTAINED BY THIS METHOD
IE57463B1 (en) * 1985-08-07 1992-11-04 Kaltenbach Thuring Sa Granulating device
GB9209620D0 (en) * 1992-05-05 1992-06-17 Ici Plc Improvements in prill drying
JO1812B1 (en) * 1993-10-15 1995-07-05 ساسول كيميكال اندستريز ليمتد Porous prilled ammonium nitrate

Also Published As

Publication number Publication date
ATE205810T1 (en) 2001-10-15
FR2757842A1 (en) 1998-07-03
DK0850878T3 (en) 2001-11-19
PT850878E (en) 2002-02-28
US6022386A (en) 2000-02-08
EP0850878A1 (en) 1998-07-01
AU4837697A (en) 1998-07-02
CA2221717A1 (en) 1998-06-30
ES2160912T3 (en) 2001-11-16
EP0850878B1 (en) 2001-09-19
DE69706822T2 (en) 2002-03-28
NO319746B1 (en) 2005-09-12
AU729196B2 (en) 2001-01-25
NO976096D0 (en) 1997-12-29
NO976096L (en) 1998-07-01
CA2221717C (en) 2005-03-29
DE69706822D1 (en) 2001-10-25

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Legal Events

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ST Notification of lapse