FR2415299A1 - Procede analytique et dispositif pour la determination des teneurs totales en azote dans des systemes aqueux - Google Patents

Procede analytique et dispositif pour la determination des teneurs totales en azote dans des systemes aqueux

Info

Publication number
FR2415299A1
FR2415299A1 FR7900668A FR7900668A FR2415299A1 FR 2415299 A1 FR2415299 A1 FR 2415299A1 FR 7900668 A FR7900668 A FR 7900668A FR 7900668 A FR7900668 A FR 7900668A FR 2415299 A1 FR2415299 A1 FR 2415299A1
Authority
FR
France
Prior art keywords
aqueous systems
total nitrogen
nitrogen content
determining
analytical process
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7900668A
Other languages
English (en)
Other versions
FR2415299B1 (fr
Inventor
Naobumi Oi
Tadamasa Itoh
Yoshiaki Yasumasa
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sumitomo Chemical Co Ltd
Original Assignee
Sumitomo Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from JP506678A external-priority patent/JPS5498296A/ja
Priority claimed from JP1024378A external-priority patent/JPS54103394A/ja
Application filed by Sumitomo Chemical Co Ltd filed Critical Sumitomo Chemical Co Ltd
Publication of FR2415299A1 publication Critical patent/FR2415299A1/fr
Application granted granted Critical
Publication of FR2415299B1 publication Critical patent/FR2415299B1/fr
Expired legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/18—Water
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
    • G01N31/005—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods investigating the presence of an element by oxidation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/17—Nitrogen containing
    • Y10T436/176152—Total nitrogen determined
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/24—Nuclear magnetic resonance, electron spin resonance or other spin effects or mass spectrometry

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Pathology (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Molecular Biology (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

Procédé et dispositif pour la détermination de la teneur totale en azote dans des systèmes aqueux. Ce procédé consiste à faire passer un courant de gaz inerte, ne contenant sensiblement pas d'azote et d'anhydride carbonique, à travers une tube de réaction, qui est garni avec un catalyseur de décomposition et maintenu à une température de 700 à 1200 degrés C, un condenseur 8 et un tube 9 absorption d'humidité, dans cet ordre, à injecter un échantillon expérimental aqueux à analyser dans le tube de réaction et à envoyer les produits gazeux sortant du tube d'absorption d'humidite à un spectromètre de masse pour déterminer la teneur en azote. La présente invention est particulièrement utile pour déterminer la teneur en azote totale dans des composés azotés contenus dans des systèmes aqueux, de manière rapide et précise, et avec une grande sensibilité
FR7900668A 1978-01-19 1979-01-11 Procede analytique et dispositif pour la determination des teneurs totales en azote dans des systemes aqueux Expired FR2415299B1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP506678A JPS5498296A (en) 1978-01-19 1978-01-19 Method of analysing total nitrogen in water and its device
JP1024378A JPS54103394A (en) 1978-01-31 1978-01-31 Method of analysing total nitrogen in water and its device

Publications (2)

Publication Number Publication Date
FR2415299A1 true FR2415299A1 (fr) 1979-08-17
FR2415299B1 FR2415299B1 (fr) 1985-06-28

Family

ID=26338948

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7900668A Expired FR2415299B1 (fr) 1978-01-19 1979-01-11 Procede analytique et dispositif pour la determination des teneurs totales en azote dans des systemes aqueux

Country Status (6)

Country Link
US (1) US4332591A (fr)
CA (1) CA1129325A (fr)
DE (1) DE2902056A1 (fr)
FR (1) FR2415299B1 (fr)
GB (1) GB2012953B (fr)
NL (1) NL7900450A (fr)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0359158A2 (fr) * 1988-09-16 1990-03-21 Solvay Umweltchemie GmbH Appareil et procédé pour la détermination dans l'eau de gaz ou de substances gazéifiables
EP0437405A1 (fr) * 1990-01-12 1991-07-17 Societe Nationale Elf Aquitaine Procédé et appareil pour la détermination de l'azote total
WO1994007134A1 (fr) * 1992-09-14 1994-03-31 Rosemount Analytical Inc. Appareil et procede de mesure de la teneur en azote de systemes aqueux

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS55155249A (en) * 1979-05-23 1980-12-03 Sumitomo Chem Co Ltd Method and apparatus of analysis of total nitrogen
US4622009A (en) * 1982-03-05 1986-11-11 Leco Corporation Carbon, hydrogen, and nitrogen analyzer
US4701306A (en) * 1984-06-05 1987-10-20 Canadian Patents & Development Ltd. Concentrator for detection of amine vapors
US5152963A (en) * 1986-08-04 1992-10-06 Wreyford Donald M Total sulfur analyzer system operative on sulfur/nitrogen mixtures
IT1256355B (it) * 1992-08-31 1995-12-01 Procedimento e apparecchiatura per la determinazione dell'azoto totale mediante analisi elementare
DE4437120C2 (de) * 1994-10-05 1998-02-12 Ufz Leipzighalle Gmbh Verfahren und Vorrichtung zur on-line gekoppelten Deuteriumbestimmung
US6627155B1 (en) * 1998-06-12 2003-09-30 Horiba, Ltd. Combustion furnace system for analyzing elements in a sample
US6830730B2 (en) 2001-09-11 2004-12-14 Spectrolanalytical Instruments Method and apparatus for the on-stream analysis of total sulfur and/or nitrogen in petroleum products
US7745226B2 (en) 2005-04-06 2010-06-29 Quest Diagnostics Investments Incorporated Methods for detecting vitamin D metabolites
US7972868B2 (en) 2007-11-28 2011-07-05 Quest Diagnostics Investments Incorporated Methods for detecting dihydroxyvitamin D metabolites by mass spectrometry
DE102008016583A1 (de) * 2008-03-31 2009-10-01 Thermo Fisher Scientific (Bremen) Gmbh Vorrichtung und Verfahren zur Bildung von CO2, N2 und/oder SO2 aus einer Probe
US7977117B2 (en) 2009-12-03 2011-07-12 Quest Diagnostics Investments Incorprated Vitamin D metabolite determination utilizing mass spectrometry following derivatization
US20120025067A1 (en) 2009-12-11 2012-02-02 Quest Diagnostics Investments Incorporated Mass spectrometric determination of non-derivatized, non-metabolized vitamin d
EP2510347B1 (fr) 2009-12-11 2019-03-20 Quest Diagnostics Investments Incorporated Spectrométrie de masse de composés stéroïdiens dans des échantillons multiplexes
JP2013160594A (ja) * 2012-02-03 2013-08-19 Horiba Ltd 元素分析装置
DE102017002627A1 (de) * 2017-03-20 2018-09-20 Taunus Instruments GmbH Verfahren zum Bestimmen eines Stickstoffgehaltes in festen oder flüssigen Proben

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3304159A (en) * 1963-01-28 1967-02-14 Hewlett Packard Co Gas chromatographic analysis method for c, h, and n content in solid organic compounds
US3565583A (en) * 1968-01-15 1971-02-23 Dohrmann Instr Co Method and apparatus for determination of nitrogen in water and in oxygenated hydrocarbon matrices
DE2621616A1 (de) * 1975-05-15 1976-12-02 Sumitomo Chemical Co Analytisches verfahren und vorrichtung zur bestimmung des gesamt-stickstoff- und/oder -kohlenstoffgehalts in waessrigen systemen
US4015936A (en) * 1975-08-26 1977-04-05 Hiryokagaku Kenkyusho Method for determination of total nitrogen and heavy nitrogen content
US4025309A (en) * 1976-02-26 1977-05-24 Hach Chemical Company Carbon nitrogen test system
CA1023969A (fr) * 1975-12-08 1978-01-10 Robert J. Flett Preparation et mesure d'infimes quantites d'azote

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3304159A (en) * 1963-01-28 1967-02-14 Hewlett Packard Co Gas chromatographic analysis method for c, h, and n content in solid organic compounds
US3565583A (en) * 1968-01-15 1971-02-23 Dohrmann Instr Co Method and apparatus for determination of nitrogen in water and in oxygenated hydrocarbon matrices
DE2621616A1 (de) * 1975-05-15 1976-12-02 Sumitomo Chemical Co Analytisches verfahren und vorrichtung zur bestimmung des gesamt-stickstoff- und/oder -kohlenstoffgehalts in waessrigen systemen
US4015936A (en) * 1975-08-26 1977-04-05 Hiryokagaku Kenkyusho Method for determination of total nitrogen and heavy nitrogen content
CA1023969A (fr) * 1975-12-08 1978-01-10 Robert J. Flett Preparation et mesure d'infimes quantites d'azote
US4025309A (en) * 1976-02-26 1977-05-24 Hach Chemical Company Carbon nitrogen test system

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0359158A2 (fr) * 1988-09-16 1990-03-21 Solvay Umweltchemie GmbH Appareil et procédé pour la détermination dans l'eau de gaz ou de substances gazéifiables
EP0359158A3 (en) * 1988-09-16 1990-05-09 Gutec Gmbh Apparatus and method for determining the presence of gases or gasifiable substances in water
EP0437405A1 (fr) * 1990-01-12 1991-07-17 Societe Nationale Elf Aquitaine Procédé et appareil pour la détermination de l'azote total
FR2657166A1 (fr) * 1990-01-12 1991-07-19 Elf Aquitaine Procede et appareil pour la determination de l'azote total.
WO1994007134A1 (fr) * 1992-09-14 1994-03-31 Rosemount Analytical Inc. Appareil et procede de mesure de la teneur en azote de systemes aqueux

Also Published As

Publication number Publication date
GB2012953A (en) 1979-08-01
GB2012953B (en) 1982-07-21
CA1129325A (fr) 1982-08-10
FR2415299B1 (fr) 1985-06-28
US4332591A (en) 1982-06-01
NL7900450A (nl) 1979-07-23
DE2902056A1 (de) 1979-08-02

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