FR2414033A1 - PROCESS FOR PREPARING A COMPOSITE OF POLYCRYSTALLINE DIAMOND AND OF SILICON CARBIDE OR NITRIDE, AND COMPOSITE THUS OBTAINED - Google Patents

PROCESS FOR PREPARING A COMPOSITE OF POLYCRYSTALLINE DIAMOND AND OF SILICON CARBIDE OR NITRIDE, AND COMPOSITE THUS OBTAINED

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Publication number
FR2414033A1
FR2414033A1 FR7829913A FR7829913A FR2414033A1 FR 2414033 A1 FR2414033 A1 FR 2414033A1 FR 7829913 A FR7829913 A FR 7829913A FR 7829913 A FR7829913 A FR 7829913A FR 2414033 A1 FR2414033 A1 FR 2414033A1
Authority
FR
France
Prior art keywords
composite
mass
diamond
silicon
nitride
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7829913A
Other languages
French (fr)
Other versions
FR2414033B1 (en
Inventor
Minyoung Lee
Lawrence Edward Szala
Robert Charles Devries
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
General Electric Co
Original Assignee
General Electric Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by General Electric Co filed Critical General Electric Co
Publication of FR2414033A1 publication Critical patent/FR2414033A1/en
Application granted granted Critical
Publication of FR2414033B1 publication Critical patent/FR2414033B1/fr
Granted legal-status Critical Current

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    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/64Burning or sintering processes
    • C04B35/645Pressure sintering
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/06Processes using ultra-high pressure, e.g. for the formation of diamonds; Apparatus therefor, e.g. moulds or dies
    • B01J3/062Processes using ultra-high pressure, e.g. for the formation of diamonds; Apparatus therefor, e.g. moulds or dies characterised by the composition of the materials to be processed
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    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/12Both compacting and sintering
    • B22F3/14Both compacting and sintering simultaneously
    • B22F3/15Hot isostatic pressing
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    • B22F7/00Manufacture of composite layers, workpieces, or articles, comprising metallic powder, by sintering the powder, with or without compacting wherein at least one part is obtained by sintering or compression
    • B22F7/06Manufacture of composite layers, workpieces, or articles, comprising metallic powder, by sintering the powder, with or without compacting wherein at least one part is obtained by sintering or compression of composite workpieces or articles from parts, e.g. to form tipped tools
    • B22F7/08Manufacture of composite layers, workpieces, or articles, comprising metallic powder, by sintering the powder, with or without compacting wherein at least one part is obtained by sintering or compression of composite workpieces or articles from parts, e.g. to form tipped tools with one or more parts not made from powder
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23BTURNING; BORING
    • B23B27/00Tools for turning or boring machines; Tools of a similar kind in general; Accessories therefor
    • B23B27/14Cutting tools of which the bits or tips or cutting inserts are of special material
    • B23B27/148Composition of the cutting inserts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24DTOOLS FOR GRINDING, BUFFING OR SHARPENING
    • B24D18/00Manufacture of grinding tools or other grinding devices, e.g. wheels, not otherwise provided for
    • B24D18/0009Manufacture of grinding tools or other grinding devices, e.g. wheels, not otherwise provided for using moulds or presses
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24DTOOLS FOR GRINDING, BUFFING OR SHARPENING
    • B24D3/00Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents
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    • B24D3/06Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents the constituent being used as bonding agent and being essentially inorganic metallic or mixture of metals with ceramic materials, e.g. hard metals, "cermets", cements
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Abstract

PROCEDE UTILISANT DES PRESSIONS RELATIVEMENT PEU ELEVEES. IL CONSISTE A PLACER DANS UNE COUPELLE 13 UNE MASSE D'ALLIAGE SOLIDE EUTECTIFERE, RICHE EN SILICIUM 12, UNE MASSE DE CRISTAUX DE DIAMANT 13 ET UN SUBSTRAT DE CARBURE OU NITRURE DE SILICIUM 14; A DISPOSER L'ENSEMBLE DANS UN MILIEU EN POUDRE DE TRANSMISSION DE PRESSION; A EFFECTUER UN PRESSAGE A FROID DE L'ENSEMBLE POUR OBTENIR UN SYSTEME STABILISE EN DIMENSION, A PRESSER A CHAUD LE SYSTEME STABILISE EN DIMENSION POUR FAIRE S'INFILTRER L'ALLIAGE RICHE EN SILICIUM DANS LA MASSE DE DIAMANT ET A L'INTERFACE ENTRE LA MASSE DE DIAMANT ET LE SUBSTRAT, A MAINTENIR UNE PRESSION SUFFISANTE PENDANT LE REFROIDISSEMENT POUR CONSERVER LA STABILITE DE DIMENSION ET A RECUPERER LE COMPOSITE FORME. APPLICATION A LA FABRICATION D'OUTILS DE COUPE.PROCESS USING RELATIVELY LOW-HIGH PRESSURES. IT CONSISTS OF PLACING IN A CUP 13 A MASS OF SOLID EUTECTIFIER ALLOY, RICH IN SILICON 12, A MASS OF DIAMOND CRYSTALS 13 AND A SUBSTRATE OF CARBIDE OR SILICON NITRIDE 14; TO DISPOSE OF THE ASSEMBLY IN A PRESSURE TRANSMISSION POWDER MEDIUM; A COLD PRESSING OF THE ASSEMBLY TO OBTAIN A SYSTEM STABILIZED IN DIMENSION, A HOT PRESSING THE SYSTEM STABILIZED IN DIMENSION TO ENSURE THE SILICON-RICH ALLOY INTO THE DIAMOND GROUND AND AT THE INTERFACE BETWEEN THE DIAMOND MASS AND THE SUBSTRATE, TO MAINTAIN SUFFICIENT PRESSURE DURING COOLING TO KEEP SIZE STABILITY AND RECOVER THE COMPOSITE FORM. APPLICATION TO THE MANUFACTURING OF CUTTING TOOLS.

FR7829913A 1977-10-21 1978-10-20 PROCESS FOR PREPARING A COMPOSITE OF POLYCRYSTALLINE DIAMOND AND OF SILICON CARBIDE OR NITRIDE, AND COMPOSITE THUS OBTAINED Granted FR2414033A1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US84444977A 1977-10-21 1977-10-21
US84444777A 1977-10-21 1977-10-21

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FR2414033A1 true FR2414033A1 (en) 1979-08-03
FR2414033B1 FR2414033B1 (en) 1982-10-22

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FR7829913A Granted FR2414033A1 (en) 1977-10-21 1978-10-20 PROCESS FOR PREPARING A COMPOSITE OF POLYCRYSTALLINE DIAMOND AND OF SILICON CARBIDE OR NITRIDE, AND COMPOSITE THUS OBTAINED

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JP (1) JPS5473811A (en)
AT (1) AT371400B (en)
AU (1) AU525777B2 (en)
BR (1) BR7806957A (en)
CH (1) CH647487A5 (en)
DE (1) DE2845834A1 (en)
DK (1) DK153536C (en)
ES (1) ES474394A1 (en)
FR (1) FR2414033A1 (en)
GB (1) GB2006733B (en)
IE (1) IE48038B1 (en)
IL (1) IL55719A0 (en)
IT (1) IT1099392B (en)
NL (1) NL186311C (en)
SE (1) SE445838B (en)

Families Citing this family (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BR8108688A (en) * 1980-07-09 1982-05-25 Gen Electric PROCESS FOR THE PREPARATION OF AN ITEM COMPOSED OF SILICON CARBIDE AND COMPOUND PRODUCT RESULTING FROM THE PROCESS
US4453951A (en) * 1980-07-09 1984-06-12 General Electric Co. Process for the production of silicone carbide composite
JPS57501027A (en) * 1980-07-09 1982-06-10
JPS6059085B2 (en) * 1980-12-03 1985-12-23 住友電気工業株式会社 coated ceramic tools
JPS6059086B2 (en) * 1980-12-12 1985-12-23 住友電気工業株式会社 coated ceramic tools
US4448591A (en) * 1981-01-21 1984-05-15 General Electric Company Cutting insert having unique cross section
US4698070A (en) * 1981-12-16 1987-10-06 General Electric Company Cutting insert for interrupted heavy machining
US4544517A (en) * 1981-12-16 1985-10-01 General Electric Co. Automatic composite press technique for producing cutting inserts
US4497639A (en) * 1981-12-16 1985-02-05 General Electric Company Silicon carbide cutting insert with pre-pressed core center piece and sintered diamond envelope
US4460382A (en) * 1981-12-16 1984-07-17 General Electric Company Brazable layer for indexable cutting insert
US4483892A (en) * 1981-12-16 1984-11-20 General Electric Company Wear resistant annular insert and process for making same
US4465650A (en) * 1981-12-16 1984-08-14 General Electric Company Process for preparing nitrided superhard composite materials
DE3511284A1 (en) 1984-03-30 1985-10-10 De Beers Industrial Diamond Division (Proprietary) Ltd., Johannesburg, Transvaal GRINDING TOOL WITH GRINDING INSERT
FR2568933B1 (en) * 1984-08-13 1986-09-19 Combustible Nucleaire DIAMOND ROTARY DRILLING TOOL AND METHOD FOR MANUFACTURING SUCH A TOOL
FR2568810B1 (en) * 1984-08-13 1986-11-14 Combustible Nucleaire DIAMOND CUTTING ELEMENT AND METHOD FOR MANUFACTURING SUCH AN ELEMENT
WO1986001433A1 (en) * 1984-08-24 1986-03-13 The Australian National University Diamond compacts and process for making same
IE58714B1 (en) * 1985-06-07 1993-11-03 De Beers Ind Diamond Thermally stable diamond abrasive compact body
SE455277B (en) * 1986-03-21 1988-07-04 Uddeholm Tooling Ab SET FOR POWDER METAL SURGICAL PREPARING A FORM THROUGH HEAT COMPRESSION OF POWDER IN A CERAMIC FORM BY A PARTICULATED PRESSURE MEDIUM
FR2598644B1 (en) * 1986-05-16 1989-08-25 Combustible Nucleaire THERMOSTABLE DIAMOND ABRASIVE PRODUCT AND PROCESS FOR PRODUCING SUCH A PRODUCT
AU605996B2 (en) * 1988-08-31 1991-01-24 De Beers Industrial Diamond Division (Proprietary) Limited Manufacture of abrasive products
AU605994B2 (en) * 1988-08-31 1991-01-24 De Beers Industrial Diamond Division (Proprietary) Limited Manufacture of two-component products
AU605995B2 (en) * 1988-08-31 1991-01-24 De Beers Industrial Diamond Division (Proprietary) Limited Manufacture of abrasive products
US7647993B2 (en) * 2004-05-06 2010-01-19 Smith International, Inc. Thermally stable diamond bonded materials and compacts
DE102004056734A1 (en) * 2004-11-24 2006-06-01 Vatcharachai Buanatra Diamond molded article, useful as e.g. heat transmission medium, comprises multiplicity of diamond crystallites, whose boundary surfaces are connected with one another under the formation of an integral body structure
SE532992C2 (en) * 2007-11-08 2010-06-08 Alfa Laval Corp Ab Process for making a diamond composite, green body, diamond composite and use of the diamond composite
US9469918B2 (en) * 2014-01-24 2016-10-18 Ii-Vi Incorporated Substrate including a diamond layer and a composite layer of diamond and silicon carbide, and, optionally, silicon
CN111004033A (en) * 2019-11-28 2020-04-14 江苏禾吉新材料科技有限公司 Preparation method of polycrystalline diamond cutter for cutting straws
IT202100006182A1 (en) * 2021-03-16 2022-09-16 Willem Mirani PROCEDURE FOR THE PRODUCTION OF AN ABRASIVE TOOL.

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3913280A (en) * 1971-01-29 1975-10-21 Megadiamond Corp Polycrystalline diamond composites

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL129734C (en) * 1960-07-22
US3982911A (en) * 1972-11-01 1976-09-28 General Electric Company Process for the preparation of a composite cubic boron nitride layer abrasive body
US3853566A (en) * 1972-12-21 1974-12-10 Gen Electric Hot pressed silicon carbide
US4004934A (en) * 1973-10-24 1977-01-25 General Electric Company Sintered dense silicon carbide
US4042347A (en) * 1974-04-15 1977-08-16 Norton Company Method of making a resin-metal composite grinding wheel

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3913280A (en) * 1971-01-29 1975-10-21 Megadiamond Corp Polycrystalline diamond composites

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ATA754278A (en) 1982-11-15
AU4082578A (en) 1980-04-24
DK469278A (en) 1979-04-22
IT7828925A0 (en) 1978-10-19
FR2414033B1 (en) 1982-10-22
DK153536B (en) 1988-07-25
AU525777B2 (en) 1982-12-02
BR7806957A (en) 1979-05-08
DE2845834C2 (en) 1989-08-31
SE445838B (en) 1986-07-21
ES474394A1 (en) 1979-11-01
NL186311B (en) 1990-06-01
IT1099392B (en) 1985-09-18
IE48038B1 (en) 1984-09-05
GB2006733B (en) 1982-10-20
JPS5473811A (en) 1979-06-13
DE2845834A1 (en) 1979-04-26
CH647487A5 (en) 1985-01-31
IE782085L (en) 1979-04-21
IL55719A0 (en) 1978-12-17
GB2006733A (en) 1979-05-10
AT371400B (en) 1983-06-27
NL7810521A (en) 1979-04-24
JPS6213307B2 (en) 1987-03-25
DK153536C (en) 1988-12-19
NL186311C (en) 1990-11-01
SE7810975L (en) 1979-06-14

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