FR2396737A1 - Procede d'enlevement des groupes de protection du radical carboxy par traitement d'esters benzyliques avec un acide de lewis et nouveaux produits ainsi obtenus - Google Patents

Procede d'enlevement des groupes de protection du radical carboxy par traitement d'esters benzyliques avec un acide de lewis et nouveaux produits ainsi obtenus

Info

Publication number
FR2396737A1
FR2396737A1 FR7720919A FR7720919A FR2396737A1 FR 2396737 A1 FR2396737 A1 FR 2396737A1 FR 7720919 A FR7720919 A FR 7720919A FR 7720919 A FR7720919 A FR 7720919A FR 2396737 A1 FR2396737 A1 FR 2396737A1
Authority
FR
France
Prior art keywords
benzyl esters
lewis acid
treatment
new products
protection groups
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7720919A
Other languages
English (en)
French (fr)
Other versions
FR2396737B1 (enrdf_load_stackoverflow
Inventor
T Tsuji
M Yoshioka
T Kataoka
Y Sendo
S Hirai
T Maeda
W Nagata
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shionogi and Co Ltd
Original Assignee
Shionogi and Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to DE19772725519 priority Critical patent/DE2725519A1/de
Priority to NLAANVRAGE7707240,A priority patent/NL188749C/xx
Priority to CH814877A priority patent/CH637909A5/de
Priority to BE179054A priority patent/BE856444A/xx
Application filed by Shionogi and Co Ltd filed Critical Shionogi and Co Ltd
Priority to FR7720919A priority patent/FR2396737A1/fr
Publication of FR2396737A1 publication Critical patent/FR2396737A1/fr
Application granted granted Critical
Publication of FR2396737B1 publication Critical patent/FR2396737B1/fr
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D505/00—Heterocyclic compounds containing 5-oxa-1-azabicyclo [4.2.0] octane ring systems, i.e. compounds containing a ring system of the formula:, e.g. oxacephalosporins; Such ring systems being further condensed, e.g. 2,3-condensed with an oxygen-, nitrogen- or sulfur-containing hetero ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/09—Preparation of carboxylic acids or their salts, halides or anhydrides from carboxylic acid esters or lactones
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D205/00—Heterocyclic compounds containing four-membered rings with one nitrogen atom as the only ring hetero atom
    • C07D205/02—Heterocyclic compounds containing four-membered rings with one nitrogen atom as the only ring hetero atom not condensed with other rings
    • C07D205/06—Heterocyclic compounds containing four-membered rings with one nitrogen atom as the only ring hetero atom not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member
    • C07D205/08—Heterocyclic compounds containing four-membered rings with one nitrogen atom as the only ring hetero atom not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member with one oxygen atom directly attached in position 2, e.g. beta-lactams
    • C07D205/085—Heterocyclic compounds containing four-membered rings with one nitrogen atom as the only ring hetero atom not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member with one oxygen atom directly attached in position 2, e.g. beta-lactams with a nitrogen atom directly attached in position 3
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/58—One oxygen atom, e.g. butenolide
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/55—Design of synthesis routes, e.g. reducing the use of auxiliary or protecting groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Cephalosporin Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
FR7720919A 1977-06-06 1977-07-07 Procede d'enlevement des groupes de protection du radical carboxy par traitement d'esters benzyliques avec un acide de lewis et nouveaux produits ainsi obtenus Granted FR2396737A1 (fr)

Priority Applications (5)

Application Number Priority Date Filing Date Title
DE19772725519 DE2725519A1 (de) 1977-06-06 1977-06-06 Verfahren zur herstellung freier carbonsaeuren durch esterspaltung
NLAANVRAGE7707240,A NL188749C (nl) 1977-06-06 1977-06-29 Werkwijze voor het splitsen van esters van een desgewenst gesubstitueerde benzylalcohol.
CH814877A CH637909A5 (en) 1977-06-06 1977-07-01 Removal of carboxyl-protecting groups
BE179054A BE856444A (fr) 1977-06-06 1977-07-04 Elimination de radicaux protegeant la fonction carboxyle
FR7720919A FR2396737A1 (fr) 1977-06-06 1977-07-07 Procede d'enlevement des groupes de protection du radical carboxy par traitement d'esters benzyliques avec un acide de lewis et nouveaux produits ainsi obtenus

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
DE19772725519 DE2725519A1 (de) 1977-06-06 1977-06-06 Verfahren zur herstellung freier carbonsaeuren durch esterspaltung
NLAANVRAGE7707240,A NL188749C (nl) 1977-06-06 1977-06-29 Werkwijze voor het splitsen van esters van een desgewenst gesubstitueerde benzylalcohol.
CH814877A CH637909A5 (en) 1977-06-06 1977-07-01 Removal of carboxyl-protecting groups
BE856444 1977-07-04
BE179054A BE856444A (fr) 1977-06-06 1977-07-04 Elimination de radicaux protegeant la fonction carboxyle
FR7720919A FR2396737A1 (fr) 1977-06-06 1977-07-07 Procede d'enlevement des groupes de protection du radical carboxy par traitement d'esters benzyliques avec un acide de lewis et nouveaux produits ainsi obtenus

Publications (2)

Publication Number Publication Date
FR2396737A1 true FR2396737A1 (fr) 1979-02-02
FR2396737B1 FR2396737B1 (enrdf_load_stackoverflow) 1980-11-21

Family

ID=27543026

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7720919A Granted FR2396737A1 (fr) 1977-06-06 1977-07-07 Procede d'enlevement des groupes de protection du radical carboxy par traitement d'esters benzyliques avec un acide de lewis et nouveaux produits ainsi obtenus

Country Status (5)

Country Link
BE (1) BE856444A (enrdf_load_stackoverflow)
CH (1) CH637909A5 (enrdf_load_stackoverflow)
DE (1) DE2725519A1 (enrdf_load_stackoverflow)
FR (1) FR2396737A1 (enrdf_load_stackoverflow)
NL (1) NL188749C (enrdf_load_stackoverflow)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1993001165A3 (en) * 1991-07-10 1993-04-29 Merck Sharp & Dohme Aromatic compounds, compositions containing them and their use in therapy

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5302711A (en) * 1992-02-18 1994-04-12 Eli Lilly And Company Ester cleavage process for use with β-lactams
ES2128281T1 (es) * 1995-11-06 1999-05-16 Gist Brocades Bv Proceso de desesterificacion.
US5922861A (en) * 1995-11-06 1999-07-13 Gist-Brocades B.V. De-esterification process

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS52106891A (en) * 1976-03-03 1977-09-07 Shionogi & Co Ltd Removal of carboxyl protecting group

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1993001165A3 (en) * 1991-07-10 1993-04-29 Merck Sharp & Dohme Aromatic compounds, compositions containing them and their use in therapy
US5610183A (en) * 1991-07-10 1997-03-11 Merck, Sharp & Dohme Ltd. Phenylglycine derivatives pharmaceutical compositions containing them and their use in therapy

Also Published As

Publication number Publication date
NL188749B (nl) 1992-04-16
NL7707240A (nl) 1979-01-03
CH637909A5 (en) 1983-08-31
DE2725519C2 (enrdf_load_stackoverflow) 1989-11-09
NL188749C (nl) 1992-09-16
BE856444A (fr) 1977-10-31
DE2725519A1 (de) 1978-12-21
FR2396737B1 (enrdf_load_stackoverflow) 1980-11-21

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