FR2382505A1 - NICKEL RECOVERY PROCESS - Google Patents

NICKEL RECOVERY PROCESS

Info

Publication number
FR2382505A1
FR2382505A1 FR7805540A FR7805540A FR2382505A1 FR 2382505 A1 FR2382505 A1 FR 2382505A1 FR 7805540 A FR7805540 A FR 7805540A FR 7805540 A FR7805540 A FR 7805540A FR 2382505 A1 FR2382505 A1 FR 2382505A1
Authority
FR
France
Prior art keywords
nickel
ammonia
gasification
precipitate
aqueous solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7805540A
Other languages
French (fr)
Other versions
FR2382505B1 (en
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tohoku University NUC
Original Assignee
Tohoku University NUC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tohoku University NUC filed Critical Tohoku University NUC
Publication of FR2382505A1 publication Critical patent/FR2382505A1/en
Application granted granted Critical
Publication of FR2382505B1 publication Critical patent/FR2382505B1/fr
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0407—Leaching processes
    • C22B23/0446—Leaching processes with an ammoniacal liquor or with a hydroxide of an alkali or alkaline-earth metal
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

Abstract

L'invention concerne un procédé de récupération du nickel dans un résidu contenant du nickel obtenu après gazéification d'une matière charbonneuse en présence d'un catalyseur contenant du nickel. Selon l'invention, on ajoute une solution aqueuse contenant de l'ammoniaque au résidu contenant du nickel en présence d'un gaz contenant de l'oxygène pour dissoudre et extraire le nickel sous forme d'un sel complexe d'ammine-nickel; on sépare le mélange en une solution aqueuse d'ammine-nickel et des matières insolubles; on ajoute encore de l'ammoniaque à la solution aqueuse d'ammine-nickel séparée pour augmenter la concentration d'ammoniaque libérée à une valeur suffisante pour précipiter l'ammine-nickel; et on sépare ce précipité. Le dessin joint montre la courbe de la solubilité du chlorure d'ammine-nickel. L'invention s'applique notamment à la récupération du nickel après gazéification de la houille.The invention relates to a process for recovering nickel from a nickel-containing residue obtained after gasification of a carbonaceous material in the presence of a nickel-containing catalyst. According to the invention, an aqueous solution containing ammonia is added to the residue containing nickel in the presence of a gas containing oxygen to dissolve and extract the nickel in the form of an ammonia-nickel complex salt; separating the mixture into an aqueous solution of ammonia-nickel and insoluble materials; further adding ammonia to the separated aqueous ammonia-nickel solution to increase the concentration of liberated ammonia to a value sufficient to precipitate ammonia-nickel; and this precipitate is separated. The accompanying drawing shows the solubility curve of ammonia-nickel chloride. The invention applies in particular to the recovery of nickel after gasification of the coal.

FR7805540A 1977-03-01 1978-02-27 NICKEL RECOVERY PROCESS Granted FR2382505A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2081077A JPS53106623A (en) 1977-03-01 1977-03-01 Method of recovering nickel from coal ash residue containing nickel

Publications (2)

Publication Number Publication Date
FR2382505A1 true FR2382505A1 (en) 1978-09-29
FR2382505B1 FR2382505B1 (en) 1981-04-10

Family

ID=12037385

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7805540A Granted FR2382505A1 (en) 1977-03-01 1978-02-27 NICKEL RECOVERY PROCESS

Country Status (8)

Country Link
JP (1) JPS53106623A (en)
AU (1) AU513480B2 (en)
CA (1) CA1097927A (en)
DE (1) DE2808263C2 (en)
FR (1) FR2382505A1 (en)
GB (1) GB1560873A (en)
IN (1) IN150307B (en)
NL (1) NL7802008A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1998037247A1 (en) * 1997-02-18 1998-08-27 Centro De Investigaciones Para La Industria Minero-Metalurgica, Cipimm Hydrometallurgical process for the recovery of nickel and cobalt by ammoniacal leaching

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US4432953A (en) * 1982-09-24 1984-02-21 Chevron Research Company Leaching cobalt from spent hydroprocessing catalysts with sulfur dioxide
GB2130566B (en) * 1982-09-24 1986-07-09 Chevron Res Recovering metals from spent hydroprocessing catalysts
JP5645661B2 (en) * 2007-08-01 2014-12-24 ナーガルジュナ エナジー プライベート リミテッド Process for preventing polymerization of cracked volatile products during pyrolysis and gasification
WO2009086407A2 (en) 2007-12-28 2009-07-09 Greatpoint Energy, Inc. Steam generating slurry gasifier for the catalytic gasification of a carbonaceous feedstock
WO2009111345A2 (en) 2008-02-29 2009-09-11 Greatpoint Energy, Inc. Catalytic gasification particulate compositions
US8297542B2 (en) 2008-02-29 2012-10-30 Greatpoint Energy, Inc. Coal compositions for catalytic gasification
US8361428B2 (en) 2008-02-29 2013-01-29 Greatpoint Energy, Inc. Reduced carbon footprint steam generation processes
US8286901B2 (en) 2008-02-29 2012-10-16 Greatpoint Energy, Inc. Coal compositions for catalytic gasification
US20090217575A1 (en) 2008-02-29 2009-09-03 Greatpoint Energy, Inc. Biomass Char Compositions for Catalytic Gasification
WO2009111342A2 (en) 2008-02-29 2009-09-11 Greatpoint Energy, Inc Carbonaceous fines recycle
AU2009293087B2 (en) 2008-09-19 2012-11-15 Sure Champion Investment Limited Processes for gasification of a carbonaceous feedstock
WO2010033846A2 (en) 2008-09-19 2010-03-25 Greatpoint Energy, Inc. Char methanation catalyst and its use in gasification processes
US8647402B2 (en) 2008-09-19 2014-02-11 Greatpoint Energy, Inc. Processes for gasification of a carbonaceous feedstock
WO2010078298A1 (en) 2008-12-30 2010-07-08 Greatpoint Energy, Inc. Processes for preparing a catalyzed coal particulate
KR101290453B1 (en) 2008-12-30 2013-07-29 그레이트포인트 에너지, 인크. Processes for preparing a catalyzed carbonaceous particulate
WO2010132551A2 (en) 2009-05-13 2010-11-18 Greatpoint Energy, Inc. Processes for hydromethanation of a carbonaceous feedstock
EP2430126A2 (en) 2009-05-13 2012-03-21 Greatpoint Energy, Inc. Processes for hydromethanation of a carbonaceous feedstock
CN102597417B (en) 2009-10-19 2014-10-01 格雷特波因特能源公司 Integrated enhanced oil recovery process
WO2011049858A2 (en) 2009-10-19 2011-04-28 Greatpoint Energy, Inc. Integrated enhanced oil recovery process
CN102639435A (en) 2009-12-17 2012-08-15 格雷特波因特能源公司 Integrated enhanced oil recovery process
US8669013B2 (en) 2010-02-23 2014-03-11 Greatpoint Energy, Inc. Integrated hydromethanation fuel cell power generation
US8652696B2 (en) 2010-03-08 2014-02-18 Greatpoint Energy, Inc. Integrated hydromethanation fuel cell power generation
WO2011139694A1 (en) 2010-04-26 2011-11-10 Greatpoint Energy, Inc. Hydromethanation of a carbonaceous feedstock with vanadium recovery
WO2011150217A2 (en) 2010-05-28 2011-12-01 Greatpoint Energy, Inc. Conversion of liquid heavy hydrocarbon feedstocks to gaseous products
KR101424941B1 (en) 2010-08-18 2014-08-01 그레이트포인트 에너지, 인크. Hydromethanation of carbonaceous feedstock
EP2635662A1 (en) 2010-11-01 2013-09-11 Greatpoint Energy, Inc. Hydromethanation of a carbonaceous feedstock
CN103391989B (en) * 2011-02-23 2015-03-25 格雷特波因特能源公司 Hydromethanation of a carbonaceous feedstock with nickel recovery
WO2012166879A1 (en) 2011-06-03 2012-12-06 Greatpoint Energy, Inc. Hydromethanation of a carbonaceous feedstock
WO2013052553A1 (en) 2011-10-06 2013-04-11 Greatpoint Energy, Inc. Hydromethanation of a carbonaceous feedstock
CN104704204B (en) 2012-10-01 2017-03-08 格雷特波因特能源公司 Method for producing steam from original low rank coal raw material
US9034058B2 (en) 2012-10-01 2015-05-19 Greatpoint Energy, Inc. Agglomerated particulate low-rank coal feedstock and uses thereof
KR101576781B1 (en) 2012-10-01 2015-12-10 그레이트포인트 에너지, 인크. Agglomerated particulate low-rank coal feedstock and uses thereof
CN104704089B (en) 2012-10-01 2017-08-15 格雷特波因特能源公司 Graininess low rank coal raw material of agglomeration and application thereof
JP5598778B2 (en) * 2013-01-25 2014-10-01 住友金属鉱山株式会社 Method for producing high-purity nickel sulfate and method for removing impurity element from solution containing nickel
US10464872B1 (en) 2018-07-31 2019-11-05 Greatpoint Energy, Inc. Catalytic gasification to produce methanol
US10344231B1 (en) 2018-10-26 2019-07-09 Greatpoint Energy, Inc. Hydromethanation of a carbonaceous feedstock with improved carbon utilization
US10435637B1 (en) 2018-12-18 2019-10-08 Greatpoint Energy, Inc. Hydromethanation of a carbonaceous feedstock with improved carbon utilization and power generation
US10618818B1 (en) 2019-03-22 2020-04-14 Sure Champion Investment Limited Catalytic gasification to produce ammonia and urea
CN114426889B (en) * 2020-10-29 2023-10-10 中国石油化工股份有限公司 Utilization method of hydrocracking molybdenum-containing tailings
CN113802001B (en) * 2021-08-13 2022-11-22 广东邦普循环科技有限公司 Method for recovering and purifying nickel from nickel iron
CN115821041A (en) * 2022-09-01 2023-03-21 广东邦普循环科技有限公司 Method for recovering nickel

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR332596A (en) * 1903-05-06 1903-10-31 Miranda Malzac Wet desulphurization process of nickel, copper, zinc, etc. and hydroxidation of their metals, with a view to their extraction
FR460322A (en) * 1912-06-20 1913-11-28 Ernst Ellenberger Process for the treatment of cuttings from sheets coated with copper, nickel, zinc, tin, etc., or alloys of these metals by detaching the covering metals and by recovering the underlying metals
DE887871C (en) * 1941-03-05 1953-08-27 Kupferwerk Ilsenburg A G Process for separating copper-nickel-zinc alloys
NL88088C (en) * 1951-09-21 1958-05-16
DE1583911A1 (en) * 1967-11-11 1970-10-15 Ruhrchemie Ag Process for the recovery of nickel and / or cobalt from spent catalyst masses
US3967957A (en) * 1973-03-26 1976-07-06 Continental Oil Company Aqueous ammonia oxidative leach and recovery of metal values

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ZA731519B (en) * 1972-06-23 1973-11-28 Anaconda Co Recovery of nickel
CA970167A (en) * 1972-07-19 1975-07-01 Herman F. Bakker Selective precipitation of cobalt and nickel ammine complexes

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR332596A (en) * 1903-05-06 1903-10-31 Miranda Malzac Wet desulphurization process of nickel, copper, zinc, etc. and hydroxidation of their metals, with a view to their extraction
FR460322A (en) * 1912-06-20 1913-11-28 Ernst Ellenberger Process for the treatment of cuttings from sheets coated with copper, nickel, zinc, tin, etc., or alloys of these metals by detaching the covering metals and by recovering the underlying metals
DE887871C (en) * 1941-03-05 1953-08-27 Kupferwerk Ilsenburg A G Process for separating copper-nickel-zinc alloys
NL88088C (en) * 1951-09-21 1958-05-16
DE1583911A1 (en) * 1967-11-11 1970-10-15 Ruhrchemie Ag Process for the recovery of nickel and / or cobalt from spent catalyst masses
US3967957A (en) * 1973-03-26 1976-07-06 Continental Oil Company Aqueous ammonia oxidative leach and recovery of metal values

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1998037247A1 (en) * 1997-02-18 1998-08-27 Centro De Investigaciones Para La Industria Minero-Metalurgica, Cipimm Hydrometallurgical process for the recovery of nickel and cobalt by ammoniacal leaching
US6524367B1 (en) 1997-02-18 2003-02-25 Centro De Investigaciones Para La Industria Minero-Metalurgcia (Cipimm) Hydrometallurgical process for the recovery of nickel and cobalt by ammoniacal leaching

Also Published As

Publication number Publication date
JPS53106623A (en) 1978-09-16
NL7802008A (en) 1978-09-05
DE2808263A1 (en) 1978-09-07
CA1097927A (en) 1981-03-24
DE2808263C2 (en) 1983-10-27
JPS5536692B2 (en) 1980-09-22
IN150307B (en) 1982-09-04
FR2382505B1 (en) 1981-04-10
AU513480B2 (en) 1980-12-04
AU3334978A (en) 1979-08-23
GB1560873A (en) 1980-02-13

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