FR2331379A1 - Separating salts from alkylate neutralisation with ammonia - in Friedel:Crafts reaction, after flocculating with water - Google Patents

Separating salts from alkylate neutralisation with ammonia - in Friedel:Crafts reaction, after flocculating with water

Info

Publication number
FR2331379A1
FR2331379A1 FR7534704A FR7534704A FR2331379A1 FR 2331379 A1 FR2331379 A1 FR 2331379A1 FR 7534704 A FR7534704 A FR 7534704A FR 7534704 A FR7534704 A FR 7534704A FR 2331379 A1 FR2331379 A1 FR 2331379A1
Authority
FR
France
Prior art keywords
friedel
crafts reaction
alkylate
water
salts
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7534704A
Other languages
French (fr)
Other versions
FR2331379B1 (en
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Orkem SA
Original Assignee
Chimique des Charbonnages SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chimique des Charbonnages SA filed Critical Chimique des Charbonnages SA
Priority to FR7534704A priority Critical patent/FR2331379A1/en
Priority to BR7601964A priority patent/BR7601964A/en
Priority to SE7612113A priority patent/SE428013B/en
Priority to PT65786A priority patent/PT65786B/en
Priority to MX765109U priority patent/MX4893E/en
Priority to FI763222A priority patent/FI61681C/en
Priority to SU762419860A priority patent/SU955854A3/en
Priority to NO763847A priority patent/NO150078C/en
Priority to DE2651698A priority patent/DE2651698C2/en
Priority to DK511776A priority patent/DK155593C/en
Priority to US05/741,488 priority patent/US4117023A/en
Publication of FR2331379A1 publication Critical patent/FR2331379A1/en
Application granted granted Critical
Publication of FR2331379B1 publication Critical patent/FR2331379B1/fr
Granted legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00Compounds of aluminium
    • C01F7/48Halides, with or without other cations besides aluminium
    • C01F7/56Chlorides
    • C01F7/62Purification
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D21/00Separation of suspended solid particles from liquids by sedimentation
    • B01D21/009Heating or cooling mechanisms specially adapted for settling tanks
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D21/00Separation of suspended solid particles from liquids by sedimentation
    • B01D21/01Separation of suspended solid particles from liquids by sedimentation using flocculating agents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/28Regeneration or reactivation
    • B01J27/32Regeneration or reactivation of catalysts comprising compounds of halogens
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/584Recycling of catalysts

Abstract

Salts, originating from neutralisationof alkylates of a Friedel-Crafts reaction with anhydrous NH3, are sepd. from the alkylate after flocculation with water (pref. 10-20 wt.% wrt flocculated salts). Process is used for separting AlCl3 catalytic residues from Friedel-Crafts reaction of olefines with aromatic hydrocarbons, esp. of C2H4 or C3H6 with benzenes. Flocculated salts are easily decanted.
FR7534704A 1975-11-13 1975-11-13 Separating salts from alkylate neutralisation with ammonia - in Friedel:Crafts reaction, after flocculating with water Granted FR2331379A1 (en)

Priority Applications (11)

Application Number Priority Date Filing Date Title
FR7534704A FR2331379A1 (en) 1975-11-13 1975-11-13 Separating salts from alkylate neutralisation with ammonia - in Friedel:Crafts reaction, after flocculating with water
BR7601964A BR7601964A (en) 1975-11-13 1976-03-31 SEPARATION PROCESS OF CATALYTIC WASTE ARISING FROM NEUTRALIZATION BY ANhydrous AMMONIAC, FROM ALCOHILATES OF A FRIEDEL-CRAFT REACTION
SE7612113A SE428013B (en) 1975-11-13 1976-11-01 PROCEDURE KIT FOR SEPARATION OF FLOCKULATION PRODUCTS BY ALKYLING OF AROMATIC CULVET MEDIUM OLEFINIC CULVET
PT65786A PT65786B (en) 1975-11-13 1976-11-03 PROCESS FOR SEPARATING CATALYTIC RESIDUES FROM ALUMINUM DUCHLORIDE
MX765109U MX4893E (en) 1975-11-13 1976-11-09 IMPROVED PROCEDURE TO SEPARATE SALTS FROM NEUTRALIZATION FROM RENTED FROM A FRIEDEL-CRAFT REACTION
FI763222A FI61681C (en) 1975-11-13 1976-11-10 FOERFARANDE FOER AVLAEGSNANDE AV KATALYSATORRESTER FRAON SURA ALKYLATER
SU762419860A SU955854A3 (en) 1975-11-13 1976-11-11 Process for purifying hydrocarbons
NO763847A NO150078C (en) 1975-11-13 1976-11-11 PROCEDURE FOR THE EXTRACTION OF SURE ALKYLATES CREATED BY THE ALKYLATION OF AROMATIC HYDROCARBONES IN THE PRESENT OF ALUMINUM CHLORIDE
DE2651698A DE2651698C2 (en) 1975-11-13 1976-11-12 Process for the separation of the salts resulting from the neutralization of the alkylates in a Friedel-Crafts reaction with anhydrous ammonia
DK511776A DK155593C (en) 1975-11-13 1976-11-12 PROCEDURES FOR PHARMACEUTICAL PREPARATION OF MINERAL SALTS FROM A FRIDEL-CRAFT CATALYST
US05/741,488 US4117023A (en) 1975-11-13 1976-11-12 Method of separation of catalytic residues derived from aluminum chloride

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR7534704A FR2331379A1 (en) 1975-11-13 1975-11-13 Separating salts from alkylate neutralisation with ammonia - in Friedel:Crafts reaction, after flocculating with water

Publications (2)

Publication Number Publication Date
FR2331379A1 true FR2331379A1 (en) 1977-06-10
FR2331379B1 FR2331379B1 (en) 1978-12-29

Family

ID=9162373

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7534704A Granted FR2331379A1 (en) 1975-11-13 1975-11-13 Separating salts from alkylate neutralisation with ammonia - in Friedel:Crafts reaction, after flocculating with water

Country Status (2)

Country Link
BR (1) BR7601964A (en)
FR (1) FR2331379A1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110078691A (en) * 2019-05-05 2019-08-02 山东盛华新材料科技股份有限公司 The recovery method of catalyst in a kind of heterocyclic Friedel-Crafts reaction

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110078691A (en) * 2019-05-05 2019-08-02 山东盛华新材料科技股份有限公司 The recovery method of catalyst in a kind of heterocyclic Friedel-Crafts reaction

Also Published As

Publication number Publication date
BR7601964A (en) 1977-05-10
FR2331379B1 (en) 1978-12-29

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