FR2137100A1 - O,o-dimethylthionophosphoric acid prepn - from methanol and o,o - dimethyl-dithiophosphoric acid - Google Patents
O,o-dimethylthionophosphoric acid prepn - from methanol and o,o - dimethyl-dithiophosphoric acidInfo
- Publication number
- FR2137100A1 FR2137100A1 FR7117335A FR7117335A FR2137100A1 FR 2137100 A1 FR2137100 A1 FR 2137100A1 FR 7117335 A FR7117335 A FR 7117335A FR 7117335 A FR7117335 A FR 7117335A FR 2137100 A1 FR2137100 A1 FR 2137100A1
- Authority
- FR
- France
- Prior art keywords
- acid
- dimethyl
- methanol
- dimethylthionophosphoric
- prepn
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 title abstract 9
- CZGGKXNYNPJFAX-UHFFFAOYSA-N Dimethyldithiophosphate Chemical compound COP(S)(=S)OC CZGGKXNYNPJFAX-UHFFFAOYSA-N 0.000 title abstract 2
- 239000002253 acid Substances 0.000 title abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000002917 insecticide Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/16—Esters of thiophosphoric acids or thiophosphorous acids
- C07F9/165—Esters of thiophosphoric acids
- C07F9/17—Esters of thiophosphoric acids with hydroxyalkyl compounds without further substituents on alkyl
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
O,O-Dimethyl-thionophosphoric acid (I) is prepd by heating a mixt of MeOH and O,O-dimethyl-dithiophosphoric acid (II) in a molar ratio of >=1:2 at >75 degrees C. (II) may be replaced by the equiv amts of P2S5 and MeOH. (I) is an inter for insecticides.
Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7117335A FR2137100A1 (en) | 1971-05-13 | 1971-05-13 | O,o-dimethylthionophosphoric acid prepn - from methanol and o,o - dimethyl-dithiophosphoric acid |
NL7206118A NL7206118A (en) | 1971-05-13 | 1972-05-05 | |
DE19722223259 DE2223259A1 (en) | 1971-05-13 | 1972-05-12 | Process for the preparation of O, O-dimethylthionophosphoric acid |
BE783425A BE783425A (en) | 1971-05-13 | 1972-05-12 | PROCESS FOR PREPARING 0,0-DIMETHYL THIONOPHOSPHORIC ACID |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7117335A FR2137100A1 (en) | 1971-05-13 | 1971-05-13 | O,o-dimethylthionophosphoric acid prepn - from methanol and o,o - dimethyl-dithiophosphoric acid |
Publications (2)
Publication Number | Publication Date |
---|---|
FR2137100A1 true FR2137100A1 (en) | 1972-12-29 |
FR2137100B1 FR2137100B1 (en) | 1973-05-11 |
Family
ID=9076977
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7117335A Granted FR2137100A1 (en) | 1971-05-13 | 1971-05-13 | O,o-dimethylthionophosphoric acid prepn - from methanol and o,o - dimethyl-dithiophosphoric acid |
Country Status (4)
Country | Link |
---|---|
BE (1) | BE783425A (en) |
DE (1) | DE2223259A1 (en) |
FR (1) | FR2137100A1 (en) |
NL (1) | NL7206118A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111393472A (en) * | 2019-12-27 | 2020-07-10 | 安道麦股份有限公司 | Method for recycling by-products in production process of spermine |
-
1971
- 1971-05-13 FR FR7117335A patent/FR2137100A1/en active Granted
-
1972
- 1972-05-05 NL NL7206118A patent/NL7206118A/xx not_active Application Discontinuation
- 1972-05-12 DE DE19722223259 patent/DE2223259A1/en active Pending
- 1972-05-12 BE BE783425A patent/BE783425A/en unknown
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111393472A (en) * | 2019-12-27 | 2020-07-10 | 安道麦股份有限公司 | Method for recycling by-products in production process of spermine |
Also Published As
Publication number | Publication date |
---|---|
BE783425A (en) | 1972-11-13 |
DE2223259A1 (en) | 1972-11-23 |
FR2137100B1 (en) | 1973-05-11 |
NL7206118A (en) | 1972-11-15 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
ST | Notification of lapse |