FR2102898A5 - Pyrocatechol manufacture from a chloro - phenol - Google Patents
Pyrocatechol manufacture from a chloro - phenolInfo
- Publication number
- FR2102898A5 FR2102898A5 FR7031444A FR7031444A FR2102898A5 FR 2102898 A5 FR2102898 A5 FR 2102898A5 FR 7031444 A FR7031444 A FR 7031444A FR 7031444 A FR7031444 A FR 7031444A FR 2102898 A5 FR2102898 A5 FR 2102898A5
- Authority
- FR
- France
- Prior art keywords
- pyrocatechol
- weight
- chloro
- phenol
- manufacture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/01—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by replacing functional groups bound to a six-membered aromatic ring by hydroxy groups, e.g. by hydrolysis
- C07C37/02—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by replacing functional groups bound to a six-membered aromatic ring by hydroxy groups, e.g. by hydrolysis by substitution of halogen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Pyrocatechol is prepared by treating o-chlorophenol with 4-8 mole equivalents of alkali-metal hydroxide in aqueous solution at 60-85% Concentration by weight, in the presence of a copper hydrolysis catalyst (0.5% by weight of Cu relative to the weight of o-chlorophenol) at 160-240 degrees C. Preferably the alkali concentration is maintained at the above level throughout the reaction. This method minimizes the production of resorcinol and polynuclear products, and gives good yields in reasonable reaction times.
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
BE755540D BE755540A (en) | 1967-04-06 | Pyrocatechol manufacture from a chloro - phenol | |
FR7031444A FR2102898A5 (en) | 1970-08-28 | 1970-08-28 | Pyrocatechol manufacture from a chloro - phenol |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7031444A FR2102898A5 (en) | 1970-08-28 | 1970-08-28 | Pyrocatechol manufacture from a chloro - phenol |
Publications (1)
Publication Number | Publication Date |
---|---|
FR2102898A5 true FR2102898A5 (en) | 1972-04-07 |
Family
ID=9060665
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7031444A Expired FR2102898A5 (en) | 1967-04-06 | 1970-08-28 | Pyrocatechol manufacture from a chloro - phenol |
Country Status (1)
Country | Link |
---|---|
FR (1) | FR2102898A5 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2022200701A1 (en) | 2021-03-23 | 2022-09-29 | Psa Automobiles Sa | Reversible air conditioning device for a motor vehicle and method for installing such a device |
-
1970
- 1970-08-28 FR FR7031444A patent/FR2102898A5/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2022200701A1 (en) | 2021-03-23 | 2022-09-29 | Psa Automobiles Sa | Reversible air conditioning device for a motor vehicle and method for installing such a device |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
ST | Notification of lapse |