FR2060622A5 - Pure esters recovery - from a crude esterification mixture - Google Patents
Pure esters recovery - from a crude esterification mixtureInfo
- Publication number
- FR2060622A5 FR2060622A5 FR7029864A FR7029864A FR2060622A5 FR 2060622 A5 FR2060622 A5 FR 2060622A5 FR 7029864 A FR7029864 A FR 7029864A FR 7029864 A FR7029864 A FR 7029864A FR 2060622 A5 FR2060622 A5 FR 2060622A5
- Authority
- FR
- France
- Prior art keywords
- water
- mixt
- cpds
- esterification mixture
- esters
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000002148 esters Chemical class 0.000 title abstract 5
- 230000032050 esterification Effects 0.000 title 1
- 238000005886 esterification reaction Methods 0.000 title 1
- 239000000203 mixture Substances 0.000 title 1
- 238000011084 recovery Methods 0.000 title 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 5
- 150000008064 anhydrides Chemical class 0.000 abstract 1
- -1 aromatic dicarboxylic acids Chemical class 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000004014 plasticizer Substances 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- 229910052718 tin Inorganic materials 0.000 abstract 1
- 238000005292 vacuum distillation Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/10—Esters; Ether-esters
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/56—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/60—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19691945359 DE1945359B2 (de) | 1969-09-08 | 1969-09-08 | Verfahren zur gewinnung von estern |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| FR2060622A5 true FR2060622A5 (en) | 1971-06-18 |
Family
ID=5744854
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR7029864A Expired FR2060622A5 (en) | 1969-09-08 | 1970-08-13 | Pure esters recovery - from a crude esterification mixture |
Country Status (3)
| Country | Link |
|---|---|
| JP (1) | JPS5017043B1 (enExample) |
| DE (1) | DE1945359B2 (enExample) |
| FR (1) | FR2060622A5 (enExample) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10072133B2 (en) | 2014-01-09 | 2018-09-11 | Basf Se | Plasticizer composition containing furan derivatives and 1,2-cyclohexanedicarboxylic ester |
| US10273345B2 (en) | 2014-09-04 | 2019-04-30 | Basf Se | Plasticizer composition which contains a polymer dicarboxylic acid ester |
| US10287415B2 (en) | 2014-10-09 | 2019-05-14 | Basf Se | Plasticizer composition which comprises cycloalkyl esters of saturated dicarboxylic acids and terephthalic esters |
| US10329402B2 (en) | 2014-10-09 | 2019-06-25 | Basf Se | Plasticizer composition which comprises cycloalkyl esters of saturated dicarboxylic acids and 1,2-cyclohexanedicarboxylic esters |
Families Citing this family (35)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4007218A (en) * | 1973-12-07 | 1977-02-08 | Standard Oil Company (Indiana) | Esterification reaction |
| DE2604751A1 (de) * | 1976-02-06 | 1977-08-18 | Lentia Gmbh | Verfahren zur reinigung von rohen, hochsiedenden carbonsaeureestern |
| DE19721347B9 (de) * | 1997-05-22 | 2005-09-29 | Celanese Chemicals Europe Gmbh | Verfahren zur Herstellung von Esterweichmachern |
| DE10236279A1 (de) | 2002-08-08 | 2004-02-19 | Basf Ag | Verfahren zur Abtrennung von Veresterungskatalysator |
| US7291748B2 (en) | 2005-07-28 | 2007-11-06 | Basf Corporation | C10/C7 ester mixtures based on 2-propylheptanol |
| ES2422262T3 (es) * | 2008-12-16 | 2013-09-10 | Basf Se | Procedimiento para la elaboración de un éster crudo |
| JP2013510200A (ja) | 2009-11-05 | 2013-03-21 | ビーエーエスエフ ソシエタス・ヨーロピア | 2−プロピルヘプタノールを基礎とするエステルを含有する接着剤およびシーラント |
| WO2012084914A1 (de) | 2010-12-23 | 2012-06-28 | Basf Se | Thermoplastische elastomer-zusammensetzung und verfahren zu deren herstellung |
| DE102013015289A1 (de) | 2013-09-14 | 2015-03-19 | Oxea Gmbh | Verfahren zur Nachbehandlung von Polyolestern |
| US10030120B2 (en) | 2013-12-06 | 2018-07-24 | Basf Se | Softener composition which contains tetrahydrofuran derivatives and 1,2-cyclohexane dicarboxylic acid esters |
| DE102015207291A1 (de) | 2014-04-24 | 2016-03-10 | Basf Se | Weichmacher-Zusammensetzung, die Furanderivate und 1,2-Cyclohexandicarbonsäureester enthält |
| TW201609628A (zh) | 2014-07-08 | 2016-03-16 | 巴斯夫歐洲公司 | 包含脂族二羧酸二酯及對苯二甲酸二烷基酯之塑化劑組成物 |
| TW201605945A (zh) | 2014-07-08 | 2016-02-16 | 巴斯夫歐洲公司 | 包含二羧酸的酯及1,2-環己烷二羧酸的酯之模製化合物 |
| PL3174845T3 (pl) | 2014-08-01 | 2020-11-16 | Basf Se | Sposób obróbki surowego estru, który zawiera produkt hydrolizy katalizatora estryfikacji w postaci zawieszonych cząstek |
| EP3183250B1 (en) | 2014-08-18 | 2023-10-04 | CLAP Co., Ltd. | Process for preparing crystalline organic semiconductor material |
| TWI706979B (zh) | 2014-08-19 | 2020-10-11 | 德商巴斯夫歐洲公司 | 包含聚合二羧酸酯的塑化劑組成物 |
| PL3250635T3 (pl) | 2015-01-30 | 2019-03-29 | Basf Se | Kompozycja plastyfikatora, która zawiera polimerowe estry kwasu dikarboksylowego i estry dialkilowe kwasu tereftalowego |
| JP2018516914A (ja) | 2015-05-29 | 2018-06-28 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | 環式エステルの製造方法 |
| RU2741299C1 (ru) | 2015-09-30 | 2021-01-25 | Басф Се | Пластифицирующая композиция, содержащая полимерные сложные эфиры дикарбоновых кислот и сложные эфиры 1, 2-циклогександикарбоновой кислоты |
| RU2743641C1 (ru) | 2015-09-30 | 2021-02-20 | Басф Се | Пластифицирующая композиция, содержащая полимерные сложные эфиры дикарбоновых кислот и сложные диалкиловые эфиры терефталевой кислоты |
| US20180282510A1 (en) | 2015-09-30 | 2018-10-04 | Basf Se | Plasticizer composition containing polymeric dicarboxylic acid esters and dicarboxylic acid diesters |
| EP3178908A1 (en) | 2015-12-11 | 2017-06-14 | Basf Se | The use of 2,5-furandicarboxylic acid esters as lubricants |
| CA3011907A1 (en) | 2016-01-20 | 2017-07-27 | Basf Se | Plasticiser composition containing aliphatic dicarboxylic acid esters and diesters selected from 1,2-cyclohexane dicarboxylic acid esters and terephthalic acid esters |
| RU2743230C2 (ru) | 2016-03-23 | 2021-02-16 | Басф Се | Полимерная композиция, содержащая циклоалкилалкилдикарбоновой кислоты сложный диэфир в качестве пластификатора |
| WO2018024597A1 (de) | 2016-08-01 | 2018-02-08 | Basf Se | Weichmacher-zusammensetzung |
| CA3032594A1 (en) | 2016-08-01 | 2018-02-08 | Basf Se | Plasticizer composition |
| RU2019105682A (ru) | 2016-08-01 | 2020-09-01 | Басф Се | Композиция пластификатора |
| WO2018024591A1 (de) | 2016-08-01 | 2018-02-08 | Basf Se | Weichmacher-zusammensetzung |
| WO2019185409A1 (de) | 2018-03-29 | 2019-10-03 | Basf Se | Pvc-zusammensetzung, enthaltend wenigstens einen weichmacher der wenigstens eine carbonsäureestergruppe aufweist und wenigstens eine carbodiimidverbindung |
| EP3747860B1 (de) | 2019-06-04 | 2023-07-26 | Basf Se | Neue weichmacher auf cyclohexanon-basis |
| WO2024133359A1 (de) | 2022-12-21 | 2024-06-27 | Basf Se | Weichmacher |
| EP4638409A1 (de) | 2022-12-21 | 2025-10-29 | Basf Se | Weichmacher-verbindung |
| WO2024153687A1 (de) | 2023-01-19 | 2024-07-25 | Basf Se | Verfahren zur herstellung von 1,2-cyclohexandicarbonsäuredialkylestern |
| WO2024256670A1 (de) | 2023-06-15 | 2024-12-19 | Basf Se | Weichmacher-zusammensetzung |
| WO2025125093A1 (de) | 2023-12-14 | 2025-06-19 | Basf Se | Weichmacher auf basis von sebacinsäure |
-
1969
- 1969-09-08 DE DE19691945359 patent/DE1945359B2/de active Granted
-
1970
- 1970-08-13 FR FR7029864A patent/FR2060622A5/fr not_active Expired
- 1970-09-07 JP JP7784470A patent/JPS5017043B1/ja active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10072133B2 (en) | 2014-01-09 | 2018-09-11 | Basf Se | Plasticizer composition containing furan derivatives and 1,2-cyclohexanedicarboxylic ester |
| US10273345B2 (en) | 2014-09-04 | 2019-04-30 | Basf Se | Plasticizer composition which contains a polymer dicarboxylic acid ester |
| US10287415B2 (en) | 2014-10-09 | 2019-05-14 | Basf Se | Plasticizer composition which comprises cycloalkyl esters of saturated dicarboxylic acids and terephthalic esters |
| US10329402B2 (en) | 2014-10-09 | 2019-06-25 | Basf Se | Plasticizer composition which comprises cycloalkyl esters of saturated dicarboxylic acids and 1,2-cyclohexanedicarboxylic esters |
Also Published As
| Publication number | Publication date |
|---|---|
| DE1945359B2 (de) | 1973-05-10 |
| DE1945359C3 (enExample) | 1973-12-13 |
| JPS5017043B1 (enExample) | 1975-06-18 |
| DE1945359A1 (de) | 1971-03-11 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ST | Notification of lapse |