FI91974B - Förfarande för behandling av ett fluorescerande ämne - Google Patents
Förfarande för behandling av ett fluorescerande ämne Download PDFInfo
- Publication number
- FI91974B FI91974B FI880436A FI880436A FI91974B FI 91974 B FI91974 B FI 91974B FI 880436 A FI880436 A FI 880436A FI 880436 A FI880436 A FI 880436A FI 91974 B FI91974 B FI 91974B
- Authority
- FI
- Finland
- Prior art keywords
- phosphor
- lamps
- lamp
- suspension
- coated
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 21
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 title description 49
- 239000000725 suspension Substances 0.000 claims description 38
- 238000000576 coating method Methods 0.000 claims description 33
- 239000011248 coating agent Substances 0.000 claims description 31
- 239000007900 aqueous suspension Substances 0.000 claims description 22
- 238000010438 heat treatment Methods 0.000 claims description 19
- 239000011572 manganese Substances 0.000 claims description 13
- 230000008569 process Effects 0.000 claims description 11
- 239000000126 substance Substances 0.000 claims description 8
- 229910052748 manganese Inorganic materials 0.000 claims description 6
- 230000001681 protective effect Effects 0.000 claims description 6
- 230000002411 adverse Effects 0.000 claims description 5
- -1 manganese-activated zinc silicate Chemical class 0.000 claims description 5
- 239000010410 layer Substances 0.000 claims 2
- 239000011241 protective layer Substances 0.000 claims 2
- 229910019142 PO4 Inorganic materials 0.000 claims 1
- 239000000654 additive Substances 0.000 claims 1
- 230000000996 additive effect Effects 0.000 claims 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims 1
- OOBNORVQFIAGPT-UHFFFAOYSA-N antimony manganese Chemical group [Mn].[Sb] OOBNORVQFIAGPT-UHFFFAOYSA-N 0.000 claims 1
- 150000001669 calcium Chemical class 0.000 claims 1
- 150000004820 halides Chemical class 0.000 claims 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims 1
- 239000010452 phosphate Substances 0.000 claims 1
- 229910052782 aluminium Inorganic materials 0.000 description 23
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 22
- 238000012360 testing method Methods 0.000 description 13
- 239000000463 material Substances 0.000 description 9
- 238000003860 storage Methods 0.000 description 9
- 238000004020 luminiscence type Methods 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 239000011701 zinc Substances 0.000 description 8
- 229910004283 SiO 4 Inorganic materials 0.000 description 7
- 239000011230 binding agent Substances 0.000 description 7
- 238000002474 experimental method Methods 0.000 description 7
- 239000011521 glass Substances 0.000 description 7
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 6
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 6
- 230000006870 function Effects 0.000 description 5
- 239000002245 particle Substances 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 4
- 230000014759 maintenance of location Effects 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 3
- 229910052786 argon Inorganic materials 0.000 description 3
- 230000015556 catabolic process Effects 0.000 description 3
- 238000006731 degradation reaction Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 3
- 229910052753 mercury Inorganic materials 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 229910052698 phosphorus Inorganic materials 0.000 description 3
- 239000011574 phosphorus Substances 0.000 description 3
- 238000000197 pyrolysis Methods 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 2
- 238000004833 X-ray photoelectron spectroscopy Methods 0.000 description 2
- QVQLCTNNEUAWMS-UHFFFAOYSA-N barium oxide Chemical compound [Ba]=O QVQLCTNNEUAWMS-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 239000004020 conductor Substances 0.000 description 2
- 238000009792 diffusion process Methods 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- ZOIVSVWBENBHNT-UHFFFAOYSA-N dizinc;silicate Chemical class [Zn+2].[Zn+2].[O-][Si]([O-])([O-])[O-] ZOIVSVWBENBHNT-UHFFFAOYSA-N 0.000 description 2
- 230000036571 hydration Effects 0.000 description 2
- 238000006703 hydration reaction Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000003071 parasitic effect Effects 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
- 239000011253 protective coating Substances 0.000 description 2
- 235000012239 silicon dioxide Nutrition 0.000 description 2
- 229910052844 willemite Inorganic materials 0.000 description 2
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 1
- 239000001856 Ethyl cellulose Substances 0.000 description 1
- 239000000020 Nitrocellulose Substances 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000010891 electric arc Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 235000019325 ethyl cellulose Nutrition 0.000 description 1
- 229920001249 ethyl cellulose Polymers 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000004922 lacquer Substances 0.000 description 1
- 229910052754 neon Inorganic materials 0.000 description 1
- GKAOGPIIYCISHV-UHFFFAOYSA-N neon atom Chemical compound [Ne] GKAOGPIIYCISHV-UHFFFAOYSA-N 0.000 description 1
- 229920001220 nitrocellulos Polymers 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 150000002902 organometallic compounds Chemical class 0.000 description 1
- 244000045947 parasite Species 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000000375 suspending agent Substances 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J61/00—Gas-discharge or vapour-discharge lamps
- H01J61/02—Details
- H01J61/38—Devices for influencing the colour or wavelength of the light
- H01J61/42—Devices for influencing the colour or wavelength of the light by transforming the wavelength of the light by luminescence
- H01J61/46—Devices characterised by the binder or other non-luminescent constituent of the luminescent material, e.g. for obtaining desired pouring or drying properties
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/02—Use of particular materials as binders, particle coatings or suspension media therefor
- C09K11/025—Use of particular materials as binders, particle coatings or suspension media therefor non-luminescent particle coatings or suspension media
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
- C09K11/59—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing silicon
- C09K11/592—Chalcogenides
- C09K11/595—Chalcogenides with zinc or cadmium
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
- C09K11/74—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing arsenic, antimony or bismuth
- C09K11/75—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing arsenic, antimony or bismuth containing antimony
- C09K11/76—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing arsenic, antimony or bismuth containing antimony also containing phosphorus and halogen, e.g. halophosphates
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J61/00—Gas-discharge or vapour-discharge lamps
- H01J61/02—Details
- H01J61/38—Devices for influencing the colour or wavelength of the light
- H01J61/42—Devices for influencing the colour or wavelength of the light by transforming the wavelength of the light by luminescence
- H01J61/44—Devices characterised by the luminescent material
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Luminescent Compositions (AREA)
- Vessels And Coating Films For Discharge Lamps (AREA)
- Formation Of Various Coating Films On Cathode Ray Tubes And Lamps (AREA)
Claims (7)
1. Förfarande för behandling av ett fluorescerande ämne som är försett med ett skyddande skikt, innan det 5 inkluderas i en beläggningssuspension för en lampa, k ä n-netecknat därav, att det omfattar följande steg: steg 1: det fluorescerande ämnet som är försett med ett skyddande oxidskikt upphettas vid en temporatur pä 700 - 850 eC, under 15 minuter - 20 timmar, varvid man 10 förhindrar att oxidskiktet hos nämnda fluorescerande ämne förändras ogynnsamt vid den föjande vattenbaserade suspen-sionsbehandlingen, och varvid nämnda fluorescerande ämne ej förändras ogynnsamt; steg 2: man avkyler produkten frän steg 1; och 15 steg 3: man tillsätter produkten frän steg 2 tili en vattenbaserad suspension.
2. Förfarande enligt patentkrav 1, känne- t e c k n a t därav, att det fluorescerande ämnet utgörs av manganaktiverat zinksilikat. 20
3. Förfarande enligt patentkrav 1, k ä n n β ίε c k n a t därav, att det fluorescerande ämnet utgörs av antimonmanganaktiverat kalciumhalogenfosfat.
4. Förfarande enligt patentkrav 2 eller 3, kännetecknat därav, att nämnda skyddande skikt 25 innehäller närmast aluminiumoxid.
5. Förfarande enligt patentkrav 2 eller 3, kännetecknat därav, att nämnda upphettning sker vid en temperatur pä ca 750 °C under ca fyra timmar.
6. Förfarande enligt patentkrav 2 eller 3, 30 kännetecknat därav, att nämnda upphettning sker vid en temperatur pä ca 850 °C under ca en timme.
7. Lysrör, kännetecknat därav, att däri användes ett tillsatsämne enligt patentkrav 2 eller 3. Il
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US07/010,078 US4803400A (en) | 1987-02-02 | 1987-02-02 | Pre-water-based suspension phosphor treatment process |
| US1007887 | 1987-02-02 |
Publications (4)
| Publication Number | Publication Date |
|---|---|
| FI880436A0 FI880436A0 (sv) | 1988-02-01 |
| FI880436A FI880436A (sv) | 1988-08-03 |
| FI91974B true FI91974B (sv) | 1994-05-31 |
| FI91974C FI91974C (sv) | 1994-09-12 |
Family
ID=21743716
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FI880436A FI91974C (sv) | 1987-02-02 | 1988-02-01 | Förfarande för behandling av ett fluorescerande ämne |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4803400A (sv) |
| EP (1) | EP0279254B1 (sv) |
| JP (1) | JP2660414B2 (sv) |
| CA (1) | CA1337674C (sv) |
| DE (1) | DE3870906D1 (sv) |
| FI (1) | FI91974C (sv) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5244750A (en) * | 1988-06-10 | 1993-09-14 | Gte Products Corporation | Coated electroluminescent phosphor |
| US4925703A (en) * | 1988-12-22 | 1990-05-15 | Gte Products Corporation | Firing and milling method for producing a manganese activated zinc silicate phosphor |
| US4956202A (en) * | 1988-12-22 | 1990-09-11 | Gte Products Corporation | Firing and milling method for producing a manganese activated zinc silicate phosphor |
| US4892757A (en) * | 1988-12-22 | 1990-01-09 | Gte Products Corporation | Method for a producing manganese activated zinc silicate phosphor |
| US5151215A (en) * | 1989-02-06 | 1992-09-29 | Gte Products Corporation | Pre-water-based suspension alumina coated phosphor treatment process |
| US4946707A (en) * | 1989-07-28 | 1990-08-07 | Gte Products Corporation | Method for producing an aluminum oxide coated manganese activated zinc silicate phosphor |
| US5049408A (en) * | 1989-11-07 | 1991-09-17 | Gte Laboratories Incorporated | Method for coating phosphor particles using aluminum isopropoxide precursors and an isothermal fluidized bed |
| US4999219A (en) * | 1989-11-07 | 1991-03-12 | Gte Laboratories Incorporated | Method for coating phosphor particles using aluminum isopropoxide precursors and an isothermal fluidized bed |
| US5087523A (en) * | 1990-01-22 | 1992-02-11 | Gte Laboratories Incorporated | Phosphors with improved lumen output and lamps made therefrom |
| US5113118A (en) * | 1991-03-11 | 1992-05-12 | Gte Laboratories Incorporated | Phosphors with improved lumen output and lamps made therefrom |
| US5051277A (en) * | 1990-01-22 | 1991-09-24 | Gte Laboratories Incorporated | Method of forming a protective bi-layer coating on phosphore particles |
| US5227207A (en) * | 1990-01-26 | 1993-07-13 | Matsushita Electric Works, Ltd. | Photoconverter |
| US5126166A (en) * | 1990-12-21 | 1992-06-30 | Gte Products Corporation | Method of reducing the degradation of the red phosphor, Y203:EU, in water base lamp suspensions |
| US5167982A (en) * | 1990-12-21 | 1992-12-01 | Gte Products Corporation | Method of detecting a degraded phosphor in a lamp phosphor suspension |
| US5223341A (en) * | 1991-05-23 | 1993-06-29 | Gte Products Corporation | Phosphor containing barium and lead |
| IL116092A (en) * | 1994-11-30 | 2000-06-29 | Honeywell Inc | Ultraviolet transparent binder for phosphor fluorescent light box |
| US5855583A (en) * | 1996-02-20 | 1999-01-05 | Computer Motion, Inc. | Method and apparatus for performing minimally invasive cardiac procedures |
| US6069441A (en) * | 1996-10-31 | 2000-05-30 | Honeywell Inc. | Method for producing phospher binding materials |
| US5891238A (en) * | 1997-12-29 | 1999-04-06 | Aos Holding Company | Curable pigmented silicate compositions |
| US6787980B2 (en) * | 2000-09-22 | 2004-09-07 | Matsushita Electric Industrial Co., Ltd. | Mercury-containing material, method for producing the same and fluorescent lamp using the same |
| US20030161944A1 (en) * | 2002-02-26 | 2003-08-28 | The Regents Of The University Of California | Vacuum deposition of powdered phosphor |
| DE102012203419A1 (de) | 2011-07-29 | 2013-01-31 | Osram Ag | Leuchtstoff und Leuchtstofflampe denselben enthaltend |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3249788A (en) * | 1961-11-08 | 1966-05-03 | Westinghouse Electric Corp | Electrode coating material and discharge device |
| US3310418A (en) * | 1963-10-31 | 1967-03-21 | Gen Electric | Fluorescent lamp coating |
| US3833398A (en) * | 1973-05-03 | 1974-09-03 | Gte Sylvania Inc | Method of providing an adherent phosphor coating on a fluorescent lamp |
| JPS5222583A (en) * | 1975-08-14 | 1977-02-19 | Fujitsu Ltd | Method for protective treatment of fluorescent substance |
| JPS5222580A (en) * | 1975-08-14 | 1977-02-19 | Fujitsu Ltd | Production process of fluorescent substance for gas discharge panel |
| JPS5222585A (en) * | 1975-08-14 | 1977-02-19 | Fujitsu Ltd | Method for protective treatment of fluorescent substance |
| JPS5222584A (en) * | 1975-08-14 | 1977-02-19 | Fujitsu Ltd | Method for protective treatment of fluorescent substance |
| US4396863A (en) * | 1980-08-21 | 1983-08-02 | Thorn Emi Limited | Synthetic willemite phosphors and fluorescent lamp containing the same |
| US4393330A (en) * | 1980-10-20 | 1983-07-12 | North American Philips Electric Corp. | Method for effectively contacting manganese-activated zinc silicate phosphor with antimony oxide during phosphor coating, and resulting lamp |
| US4585673A (en) * | 1984-05-07 | 1986-04-29 | Gte Laboratories Incorporated | Method for coating phosphor particles |
| EP0160856B1 (en) * | 1984-05-07 | 1990-07-11 | GTE Laboratories Incorporated | Method for coating phosphor particles, phosphor particle, fluorescent lamp, and manufacturing method |
-
1987
- 1987-02-02 US US07/010,078 patent/US4803400A/en not_active Expired - Lifetime
-
1988
- 1988-01-29 EP EP88101328A patent/EP0279254B1/en not_active Expired
- 1988-01-29 DE DE8888101328T patent/DE3870906D1/de not_active Expired - Lifetime
- 1988-02-01 FI FI880436A patent/FI91974C/sv not_active IP Right Cessation
- 1988-02-01 CA CA000557800A patent/CA1337674C/en not_active Expired - Lifetime
- 1988-02-01 JP JP63019719A patent/JP2660414B2/ja not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| EP0279254A2 (en) | 1988-08-24 |
| EP0279254B1 (en) | 1992-05-13 |
| JPS63264693A (ja) | 1988-11-01 |
| FI91974C (sv) | 1994-09-12 |
| FI880436A (sv) | 1988-08-03 |
| CA1337674C (en) | 1995-12-05 |
| US4803400A (en) | 1989-02-07 |
| EP0279254A3 (en) | 1989-03-15 |
| FI880436A0 (sv) | 1988-02-01 |
| DE3870906D1 (de) | 1992-06-17 |
| JP2660414B2 (ja) | 1997-10-08 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| BB | Publication of examined application | ||
| MM | Patent lapsed |
Owner name: GTE PRODUCTS CORPORATION |