FI71350C - Foerfarande foer aotervinning av vanadin - Google Patents

Foerfarande foer aotervinning av vanadin Download PDF

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Publication number
FI71350C
FI71350C FI812898A FI812898A FI71350C FI 71350 C FI71350 C FI 71350C FI 812898 A FI812898 A FI 812898A FI 812898 A FI812898 A FI 812898A FI 71350 C FI71350 C FI 71350C
Authority
FI
Finland
Prior art keywords
vanadium
solution
acid
hydrogen peroxide
oxidation
Prior art date
Application number
FI812898A
Other languages
English (en)
Finnish (fi)
Other versions
FI71350B (fi
FI812898L (fi
Inventor
Mark Elson Loveitt
David Barry Mobbs
Michael Edward Walton
Original Assignee
Interox Chemicals Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Interox Chemicals Ltd filed Critical Interox Chemicals Ltd
Publication of FI812898L publication Critical patent/FI812898L/fi
Publication of FI71350B publication Critical patent/FI71350B/fi
Application granted granted Critical
Publication of FI71350C publication Critical patent/FI71350C/fi

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Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/20Obtaining niobium, tantalum or vanadium
    • C22B34/22Obtaining vanadium
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G31/00Compounds of vanadium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/28Amines
    • C22B3/282Aliphatic amines
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Geology (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Claims (8)

1. Förfarande för oxidation av vanadin till ett oxidations-stadium V, där oxidationsmedlet tillsättes i en vattenhaltig syralösning av vanadinet i ett lägre oxidationsstadium än V vid en temperatur av 0 - 80° och oxidationsmedlet hälles i lösning ända tills ätminstone nägot vanadin oxiderats tili oxidationsstadiet V, kännetecknat därav, att san oxidationsmedel användes en vattenhaltig syralösning av peroxo-monosvavelsyra, som innehäller mindre än 1 mol väteperoxid per mol peroxomonosvave1syra.
2. Förfarande enligt patentkrav 1, kännetecknat därav, att peroxcmonosvavelsyra användes i en vattenhaltig syralös-ning, som innehäller mindre än 1 mol väteperoxid per 6 mol per-oxomono svave1syra.
3. Förfarande enligt patentkrav 1 eller 2, kännetecknat därav, att peroxomonosvavelsyralösningen erhälles genom att utföra reaktion mellan vattenhaltig väteperoxid med en stvr-ka av 60 - 75 viktprocent och svavelsyra med en styrka av ätminstone 90 viktprocent, varvid molförhällandet H^SO^ : ^2^2 är i omrädet 2,5 : 1 - 4 : 1.
4. Förfarande enligt nägot av patentkraven 1-3, kännetecknat därav, att vanadinlösningen hailes i pH-omrädet 1-3.
5. Förfarande enligt patentkrav 4, kännetecknat därav, att vanadinlösningen innehäller järn och dess pH hälles i pH-omrädet 1-2.
6. Förfarande enligt nägot av föregäende patentkrav, kännetecknat därav, att vanadinets elektriska spanning kon-trolleras under oxidationen och tillsättes med detta reagerande peroxomonosvavelsyra ända tills den förutbestämda avbrottspunk-ten uppnäs.
FI812898A 1980-09-27 1981-09-16 Foerfarande foer aotervinning av vanadin FI71350C (fi)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB8031308 1980-09-27
GB8031308 1980-09-27

Publications (3)

Publication Number Publication Date
FI812898L FI812898L (fi) 1982-03-28
FI71350B FI71350B (fi) 1986-09-09
FI71350C true FI71350C (fi) 1986-12-19

Family

ID=10516348

Family Applications (1)

Application Number Title Priority Date Filing Date
FI812898A FI71350C (fi) 1980-09-27 1981-09-16 Foerfarande foer aotervinning av vanadin

Country Status (13)

Country Link
EP (1) EP0049064B1 (sv)
JP (1) JPS5792150A (sv)
AR (1) AR225969A1 (sv)
AT (1) ATE12524T1 (sv)
AU (1) AU531834B2 (sv)
BR (1) BR8106174A (sv)
CA (1) CA1178062A (sv)
DE (1) DE3169691D1 (sv)
ES (1) ES8307301A1 (sv)
FI (1) FI71350C (sv)
NO (1) NO156532C (sv)
OA (1) OA06909A (sv)
ZA (1) ZA816353B (sv)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT1199472B (it) * 1984-06-13 1988-12-30 Va Ni M S R L Procedimento per la produzione di pentossido di vanadio a partire da polveri e fanghi contenenti composti di vanadio
US4851199A (en) * 1985-01-03 1989-07-25 Union Oil Company Of California Methods for recovering vanadium from phosphoric acid and vanadium sources
US4978511A (en) * 1985-01-03 1990-12-18 Union Oil Company Of California Methods for selectively recovering vanadium from phosphoric acid and vanadium sources
CN102260792B (zh) * 2011-07-25 2012-12-05 张国茂 一种含钒石煤加浓硫酸及添加剂堆浸提钒的方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1020312A (en) * 1910-12-22 1912-03-12 American Vanadium Co Process for recovery of vanadium.
US3252756A (en) * 1962-07-12 1966-05-24 Kerr Mc Gee Oil Ind Inc Oxidation and recovery of vanadium values from acidic aqueous media
US3305322A (en) * 1963-12-23 1967-02-21 Hazen Research Vanadium recovery process employing so2 gas as the oxidizer
FR1602405A (sv) * 1968-06-11 1970-11-23
US3836476A (en) * 1971-10-04 1974-09-17 Kerr Mc Gee Chem Corp Simultaneous recovery of vanadium and uranium from oxidized wet process acid
GB1594851A (en) * 1977-05-16 1981-08-05 Interox Chemicals Ltd Extraction of zinc
US4212849A (en) * 1978-01-13 1980-07-15 Kerr-Mcgee Corporation Simultaneous extraction and recovery of uranium and vanadium from wet process acids
US4225396A (en) * 1978-10-10 1980-09-30 Kerr-Mcgee Corporation Vanadium and uranium oxidation by controlled potential electrolysis

Also Published As

Publication number Publication date
BR8106174A (pt) 1982-06-15
ATE12524T1 (de) 1985-04-15
FI71350B (fi) 1986-09-09
NO156532C (no) 1987-10-07
DE3169691D1 (en) 1985-05-09
CA1178062A (en) 1984-11-20
AU531834B2 (en) 1983-09-08
OA06909A (fr) 1983-05-31
EP0049064B1 (en) 1985-04-03
NO813264L (no) 1982-03-29
AU7551781A (en) 1982-07-15
JPS5792150A (en) 1982-06-08
ZA816353B (en) 1982-09-29
JPH0156129B2 (sv) 1989-11-29
EP0049064A1 (en) 1982-04-07
NO156532B (no) 1987-06-29
AR225969A1 (es) 1982-05-14
FI812898L (fi) 1982-03-28
ES505802A0 (es) 1983-06-16
ES8307301A1 (es) 1983-06-16

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Owner name: INTEROX CHEMICALS LIMITED