FI20090090A - Menetelmä litiumbikarbonaatin puhdistamiseksi - Google Patents

Menetelmä litiumbikarbonaatin puhdistamiseksi Download PDF

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Publication number
FI20090090A
FI20090090A FI20090090A FI20090090A FI20090090A FI 20090090 A FI20090090 A FI 20090090A FI 20090090 A FI20090090 A FI 20090090A FI 20090090 A FI20090090 A FI 20090090A FI 20090090 A FI20090090 A FI 20090090A
Authority
FI
Finland
Prior art keywords
purification
lithium carbonate
lithium
carbonate
Prior art date
Application number
FI20090090A
Other languages
English (en)
Swedish (sv)
Other versions
FI121785B (fi
FI20090090A0 (fi
Inventor
Marika Tiihonen
Original Assignee
Outotec Oyj
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Outotec Oyj filed Critical Outotec Oyj
Publication of FI20090090A0 publication Critical patent/FI20090090A0/fi
Priority to FI20090090A priority Critical patent/FI121785B/fi
Priority to PT2010050158A priority patent/PT2010103173W/pt
Priority to AU2010223194A priority patent/AU2010223194B2/en
Priority to CA2755123A priority patent/CA2755123C/en
Priority to BRPI1009523-3A priority patent/BRPI1009523B1/pt
Priority to ES201150014A priority patent/ES2379423B1/es
Priority to EA201190148A priority patent/EA019279B9/ru
Priority to PCT/FI2010/050158 priority patent/WO2010103173A1/en
Priority to CN201080011083.4A priority patent/CN102348817B/zh
Priority to US13/255,099 priority patent/US9284626B2/en
Priority to ARP100100727A priority patent/AR075734A1/es
Publication of FI20090090A publication Critical patent/FI20090090A/fi
Application granted granted Critical
Publication of FI121785B publication Critical patent/FI121785B/fi
Priority to CL2011002230A priority patent/CL2011002230A1/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
    • C22B26/10—Obtaining alkali metals
    • C22B26/12—Obtaining lithium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction
    • B01D15/361—Ion-exchange
    • B01D15/362—Cation-exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/04—Processes using organic exchangers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/04—Processes using organic exchangers
    • B01J39/07—Processes using organic exchangers in the weakly acidic form
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/50—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents
    • B01J49/53—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents for cationic exchangers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/60—Cleaning or rinsing ion-exchange beds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/08—Carbonates; Bicarbonates
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/42—Treatment or purification of solutions, e.g. obtained by leaching by ion-exchange extraction
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Environmental & Geological Engineering (AREA)
  • Metallurgy (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Treatment Of Water By Ion Exchange (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Water Treatment By Electricity Or Magnetism (AREA)
  • Removal Of Specific Substances (AREA)
FI20090090A 2009-03-11 2009-03-11 Menetelmä litiumbikarbonaatin puhdistamiseksi FI121785B (fi)

Priority Applications (12)

Application Number Priority Date Filing Date Title
FI20090090A FI121785B (fi) 2009-03-11 2009-03-11 Menetelmä litiumbikarbonaatin puhdistamiseksi
EA201190148A EA019279B9 (ru) 2009-03-11 2010-03-01 Способ очистки бикарбоната лития
CN201080011083.4A CN102348817B (zh) 2009-03-11 2010-03-01 提纯碳酸氢锂的方法
CA2755123A CA2755123C (en) 2009-03-11 2010-03-01 Method for purifying lithium bicarbonate
BRPI1009523-3A BRPI1009523B1 (pt) 2009-03-11 2010-03-01 Method for the purification of lithium bicarbonate.
ES201150014A ES2379423B1 (es) 2009-03-11 2010-03-01 Método para purificar bicarbonato de litio.
PT2010050158A PT2010103173W (pt) 2009-03-11 2010-03-01 Processo para a purificação bicarbonato de lítio
PCT/FI2010/050158 WO2010103173A1 (en) 2009-03-11 2010-03-01 Method for purifying lithium bicarbonate
AU2010223194A AU2010223194B2 (en) 2009-03-11 2010-03-01 Method for purifying lithium bicarbonate
US13/255,099 US9284626B2 (en) 2009-03-11 2010-03-01 Method for purifying lithium bicarbonate
ARP100100727A AR075734A1 (es) 2009-03-11 2010-03-10 Metodo para purificar bicarbonato de litio
CL2011002230A CL2011002230A1 (es) 2009-03-11 2011-09-09 Metodo para purificar bicarbonato de litio impuro mediante una resina de intercambio ionico en donde ademas se incluye la regeneracion de metales enlazados a la resina que comprende lavar la resina con agua, eluir con solucion acida, lavado y neutralizacion con hidroxido de sodio.

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FI20090090 2009-03-11
FI20090090A FI121785B (fi) 2009-03-11 2009-03-11 Menetelmä litiumbikarbonaatin puhdistamiseksi

Publications (3)

Publication Number Publication Date
FI20090090A0 FI20090090A0 (fi) 2009-03-11
FI20090090A true FI20090090A (fi) 2010-09-12
FI121785B FI121785B (fi) 2011-04-15

Family

ID=40510167

Family Applications (1)

Application Number Title Priority Date Filing Date
FI20090090A FI121785B (fi) 2009-03-11 2009-03-11 Menetelmä litiumbikarbonaatin puhdistamiseksi

Country Status (12)

Country Link
US (1) US9284626B2 (fi)
CN (1) CN102348817B (fi)
AR (1) AR075734A1 (fi)
AU (1) AU2010223194B2 (fi)
BR (1) BRPI1009523B1 (fi)
CA (1) CA2755123C (fi)
CL (1) CL2011002230A1 (fi)
EA (1) EA019279B9 (fi)
ES (1) ES2379423B1 (fi)
FI (1) FI121785B (fi)
PT (1) PT2010103173W (fi)
WO (1) WO2010103173A1 (fi)

Families Citing this family (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8936770B2 (en) 2010-01-22 2015-01-20 Molycorp Minerals, Llc Hydrometallurgical process and method for recovering metals
CN103958412A (zh) 2011-09-15 2014-07-30 奥若可博有限公司 用于从浓锂卤水制备碳酸锂的方法
CN104245587A (zh) * 2012-03-19 2014-12-24 奥图泰(芬兰)公司 用于回收碳酸锂的方法
EP3824991B1 (en) 2012-04-23 2022-07-27 Nemaska Lithium Inc. Process for preparing lithium sulphate
WO2013177680A1 (en) 2012-05-30 2013-12-05 Nemaska Lithium Inc. Processes for preparing lithium carbonate
PT2971252T (pt) 2013-03-15 2021-04-06 Nemaska Lithium Inc Processos para preparar hidróxido de lítio
RU2564806C2 (ru) * 2013-08-28 2015-10-10 Общество с ограниченной ответственностью "Экостар-Наутех" (ООО"Экостар-Наутех") Способ получения ультрачистого карбоната лития из технического карбоната лития и установка для его осуществления
DK3060522T3 (da) 2013-10-23 2019-08-26 Nemaska Lithium Inc Processer til forberedelse af lithiumkarbonat
EP3492632B1 (en) 2014-02-24 2020-12-09 Nemaska Lithium Inc. Methods for treating lithium-containing materials
FI127782B (fi) 2014-12-02 2019-02-15 Keliber Oy Menetelmä litiummetallifosfaattien tuottamiseksi
EP3341330B1 (en) 2015-08-27 2020-08-19 Nemaska Lithium Inc. Methods for treating lithium-containing materials
CN105347364A (zh) * 2015-10-30 2016-02-24 华陆工程科技有限责任公司 一种碳酸锂生产中沉锂母液闭环回收的方法
FI128092B (fi) 2016-06-01 2019-09-13 Keliber Oy Menetelmä johtamattomien litiummetallifosfaattien tuottamiseksi
CA2940509A1 (en) 2016-08-26 2018-02-26 Nemaska Lithium Inc. Processes for treating aqueous compositions comprising lithium sulfate and sulfuric acid
CN107777712A (zh) * 2016-08-27 2018-03-09 湖南金源新材料股份有限公司 用粗制氟化锂制取工业级碳酸锂的方法及碳酸锂产品
CA3042432A1 (en) 2016-11-14 2018-05-17 Lilac Solutions, Inc. Lithium extraction with coated ion exchange particles
CN106892443B (zh) * 2017-03-30 2019-03-15 山西北斗星新材料有限公司 利用离子交换法制取高纯碳酸锂的工艺方法
AR112663A1 (es) 2017-08-02 2019-11-27 Lilac Solutions Inc Extracción de litio con perlas porosas de intercambio iónico
JP7194185B2 (ja) 2017-11-22 2022-12-21 ネマスカ リチウム インコーポレーテッド 様々な金属の水酸化物および酸化物ならびにそれらの誘導体の調製プロセス
AR114412A1 (es) 2018-02-28 2020-09-02 Lilac Solutions Inc Reactor de intercambio iónico con trampas de partículas para la extracción de litio
CA3166921A1 (en) 2020-01-09 2021-07-15 Lilac Solutions, Inc. Process for separating undesirable metals
CA3167773A1 (en) * 2020-01-17 2021-07-22 Bl Technologies, Inc. Ion exchange system and method for conversion of aqueous lithium solution
JP2023529444A (ja) 2020-06-09 2023-07-10 ライラック ソリューションズ，インク． スケール物質存在下におけるリチウム抽出
EP4247759A1 (en) 2020-11-20 2023-09-27 Lilac Solutions, Inc. Lithium production with volatile acid
CN112717468A (zh) * 2020-12-09 2021-04-30 西安蓝晓科技新材料股份有限公司 一种用于沉锂母液中锂回收的方法
KR20240014047A (ko) 2021-04-23 2024-01-31 리락 솔루션즈, 인크. 리튬 추출을 위한 이온 교환 장치

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Publication number Priority date Publication date Assignee Title
US5451383A (en) * 1993-12-23 1995-09-19 Praxair Technology, Inc. Lithium recovery
US5419819A (en) * 1994-03-17 1995-05-30 The United States Of America As Represented By The United States Department Of Energy Self-regenerating column chromatography
WO1997009274A1 (fr) * 1995-09-01 1997-03-13 Mizusawa Industrial Chemicals, Ltd. Composite forme d'un carbonate d'hydroxyde d'aluminium alcalin, son procede d'elaboration et son utilisation
FR2743798B1 (fr) * 1996-01-18 1998-02-27 Air Liquide Procede de purification d'une solution de sels de lithium contaminee par des cations metalliques et utilisation de ce procede dans la fabrication de zeolites echangees au lithium
US6048507A (en) * 1997-12-09 2000-04-11 Limtech Process for the purification of lithium carbonate
DE19809420A1 (de) * 1998-03-05 1999-09-09 Basf Ag Verfahren zur Herstellung von hochreinen Lithiumsalzen
JP4217292B2 (ja) 1998-03-17 2009-01-28 株式会社東芝 リチウム回収方法
CN1124985C (zh) * 2000-03-13 2003-10-22 南京大学 2－羟基－3－萘甲酸生产废水的治理和资源回收利用方法
US6514414B1 (en) * 2000-09-08 2003-02-04 Clariant Finance (Bvi) Limited Process for separation and removal of iron ions from basic zinc solution
RU2243157C2 (ru) * 2003-02-11 2004-12-27 Открытое акционерное общество "Новосибирский завод химконцентратов" Способ получения особочистого карбоната лития
CN1312040C (zh) * 2005-06-22 2007-04-25 广州锐鑫锂能新材料科技有限公司 工业级氢氧化锂生产高纯高清氢氧化锂的提纯方法
CN101177288B (zh) 2007-10-30 2010-08-11 中国科学院青海盐湖研究所 一种利用盐湖锂资源制取高纯碳酸锂的工艺方法

Also Published As

Publication number Publication date
AU2010223194A1 (en) 2011-09-08
BRPI1009523B1 (pt) 2017-08-01
US9284626B2 (en) 2016-03-15
ES2379423B1 (es) 2013-01-24
PT2010103173W (pt) 2014-08-11
WO2010103173A1 (en) 2010-09-16
FI121785B (fi) 2011-04-15
CN102348817A (zh) 2012-02-08
ES2379423A1 (es) 2012-04-26
BRPI1009523A2 (pt) 2016-03-15
EA019279B9 (ru) 2014-06-30
CL2011002230A1 (es) 2012-02-17
FI20090090A0 (fi) 2009-03-11
CA2755123C (en) 2016-08-23
CN102348817B (zh) 2014-10-08
CA2755123A1 (en) 2010-09-16
EA019279B1 (ru) 2014-02-28
EA201190148A1 (ru) 2012-03-30
AR075734A1 (es) 2011-04-20
US20110318253A1 (en) 2011-12-29
AU2010223194B2 (en) 2014-08-07

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